一种双臂型低温导热带的性能研究

详细介绍了低温导热带的设计特点。从理论上分析了低温导热带的冷量传输性能和减振特性,得到通过利用高导热率材料可以有效地减小导热温差和降温时间。通过实验验证了低温导热带与制冷机和高温超导滤波器的耦合实验,耦合温差为2.5K。实验结果和理论值基本吻合,分析了造成温差的原因。根据实验结果,提出了新的改进和实施方案。     

基于STC89C51的新型液氮低温微创冷冻控制系统设计

设计了一种新型液氮低温微创冷冻控制系统,详述了系统的控制原理及各功能模块的实现.采用热流平衡原理、PID技术与STC89C51单片机及外围控制电路对冷冻冻结面范围、液氮瓶压力及冷刀刀头温度进行实时控制和显示.应用结果表明:该系统运行稳定,可靠性高,操作简单.     

Microwave Loss Reduction in Cryogenically Cooled Conductors

Measurements of microwave attenuation at room temperature and 4.2 K have been performed on some conductors commonly used in receiver input circuits. The reduction in loss on cooling is substantial, particularly for copper and plated gold, both of which showed a factor of 3 loss reduction. Copper passivated with benzotriazole shows the same loss as without passivation. The residual resistivity ratio between room temperature and 4.2 K, deduced from the measurements using the classical skin effect formula, was smaller than the measured DC value to a degree consistent with conduction in the extreme anomalous skin effect regime at cryogenic temperatures. The measurements were made in the 5–10 GHz range. The materials tested were: aluminum alloys 1100-T6 and 6061-O, C101 copper, benzotriazole treated C101 copper, and brass plated with electroformed copper, Pur-A-Gold 125-Au soft gold, and BDT200 bright gold.     

CH_4/N_2混合气体在CMS上的低温吸附分离实验研究

将煤层气液化后运往终端市场是一种十分有效的利用方式。与常规天然气不同,抽放煤层气含氮量高,采用有效的方式实现CH4/N2分离是煤层气液化流程中重要的环节。吸附分离是提高煤层气中甲烷浓度的可行方法。为了与低温液化过程紧密结合,探讨在低温下实现CH4/N2吸附分离的可行性,文中对CH4/N2在碳分子筛(CMS)上的低温分离特性进行了实验研究,并与常温下的实验结果进行了对比。实验结果表明,低温下CH4/N2吸附分离的特性与常温下有明显差别。     

反传热问题及其在深冷处理传热分析中的应用

深冷处理作为一种新的材料处理工艺,越来越受到人们的关注,目前深冷处理使材料性能提高的机理尤其是与升降温过程的耦合关系等还尚未完全清楚,需开展更深入的研究,而传热分析是此方面研究的基础。反传热分析方法是研究深冷处理传热问题的一种可行方法。较为详细地叙述了反传热问题的定义及其求解方法,介绍了反传热在深冷处理传热分析中的初步应用,并对深冷处理中应用反传热方法存在的问题进行了探讨。     

Cryogenic grinding pre-treatment improves extraction efficiency of fluoroquinolones for HPLC-MS/MS determination in animal tissue

An efficiency extraction of fluoroquinolones in chicken muscle was achieved by pulverizing it in a freezer mill before treatment with NaOH (10mM)/MeCN (1:1). The improvement of cryogenic grinding in the extraction was demonstrated for the same piece (whole leg) of four chickens treated with enrofloxacin in equal doses. A confirmatory method based on high-performance liquid chromatography tandem mass spectrometry (HPLC-MS/MS) was used to analyze the extracts. The chromatographic separation was achieved in 5min with a Synergi Fusion-RP 80A (50 x 2mm, 4μm) column filled with a hybrid polymer. The HPLC was coupled with a detector based in a quadrupole–linear ion trap Q-TRAP that allows a confirmatory detection according to the European legislation. The specificity of the method was assessed by testing a number of representative blank muscle samples (n = 10) to verify the absence of potential interfering compounds. The limits of detection and quantitation were 2 and 5ng g^-1 of quinolones in muscle samples, respectively. The chromatographic method was demonstrated to be linear for the range studied (5–500ng g^-1) with the P value for lack-of-fit in the ANOVA table greater or equal to 0.10 (calibration coefficient 0.9998 and 0.9996 for ciprofloxacin and enrofloxacin, respectively). The mean intra-day relative standard deviation (RSD) (n = 6, c = 50ng g^-1) was 6%; inter-day assay gave a RSD of 12%. The extraction and clean-up were carried out in one step with very satisfactory recovery data (between 65 and 101%).     

用低温光谱方法揭示氢键的结构特征

本文提出了一种利用红外光谱方法揭示晶态物质中分子的氢键结构的新方法。用ＫＢｒ压片和氟油研磨法制备于红光谱测量的样品。测得的光谱有时基本相同,有时同明显的差别。对此现象一直没有一个十分满意的解释。我们用低温红外光谱法证明压力诱导晶格中氢键网络的微细变化是造成不同产法测得的光谱不同的原因。具有平面氢键结构的晶体不能有效地的御加于样品上的应力,易一城较低的外力作用下发生结构畸变,因此,用ＫＢｒ压片和氟油     

场效应器件低温特性与低噪声放大器

高温超导滤波器与低噪声放大器(LNA)组成的射频接收机前端设备具有高选择性、高灵敏度和极低的噪声,因而展现出广阔的应用前景.本文研究了场效应器件的低温物理特性和电学参数,研制了一种适用于高温超导微波接收系统的低温低噪声放大器,在60K工作温度下,具有很好的噪声特性.包括高电子迁移率场效应晶体管在内的元件参数均在60K温度下进行了实际测量.放大器的各项指标与设计值吻合,工作频段为800MHz～850MHz,增益大于18dB,输入输出驻波比小于1.2,噪声系数小于0.22dB.     

低温液体管路输送中几个问题的分析

对低温液体传输过程中气体置换、预冷过程、竖直管道中间歇泉现象、盲支管填充时和阀门开启时的不稳定现象作了较详细分析,指出了其可能造成的危害,并提出了相应的解决方法。     

微重力下低温贮箱压力控制技术进展

针对微重力下低温贮箱压力升高的问题,简要介绍了几种常用的低温贮箱压力控制的方法及原理,讨论了它们各自存在的问题,并简要展望未来低温贮箱压力控制技术的发展方向。文章指出,未来研究重点在于将主动制冷与被动绝热相结合,实现零蒸发贮存的热转移技术。