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介绍了溯源至低温辐射计的紫外绝对光谱响应度测量装置,对硅陷阱探测器在三个激光波长点进行了绝对光谱响应度校准实验.测量了硅陷阱探测器的空间均匀性和非线性系数,分析了影响测量准确度的各不确定度分量.实验表明:硅陷阱探测器在紫外波段266、325、379 nm三个激光波长点处的绝对光谱响应度测量扩展不确定度分别为0.19%、0.14%、0.11%,可作为紫外波段光辐射功率基准保持和传递的标准探测器,用于提高紫外波段光谱辐射度的校准能力. 相似文献
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The influence of cryogenic mechanical milling on the structure and the thermal behavior of isotactic polypropylene was investigated by means of wide-angle X-ray scattering, differential scanning calorimetry and transmission electron microscopy. The results presented show that structural changes caused by mechanical milling at cryogenic temperatures are only partly reversible. The decrease in the degree of crystallinity as determined by differential scanning calorimetry with increasing milling time is attributed to a reversible transformation of the initial morphology into a nanostructured morphology, consisting of small fragments of the original isotactic polypropylene lamellae. During recrystallization from the molten state, there still exists an influence of the previous milling treatment, leading to significantly changed crystallization behavior. The reason for this behavior might be a decrease in the molecular weight or a change in the molecular weight distribution or the formation of long-chain branched polypropylene molecules induced by cryogenic mechanical milling.
相似文献
Michael StranzEmail: Phone: +49-231-7552579Fax: +49 231-7555978 |
187.
P. B. Bisht H. B. Tripathi D. D. Pant 《Journal of photochemistry and photobiology. A, Chemistry》1995,90(2-3):103-108
Cryogenic effects (10–293 K) on the photophysics of salicylic acid (SA) dimer have been using steady state and time-resolved spectroscopic techniques. SA dimer shows two emissions at approximately 390 nm (dimer, D) and approximately 430 nm (tautomer, T), formed by cyclic double proton transfer plus fast excited state intramolecular proton transfer (ESIPT), at low temperatures; a vibrational structure also develops which is due to C = O and OH stretches. On red edge excitation (REE), only the dimer-type (UV) emission is observed, which shifts with excitation energy resembling emission due to site selectivity. Due to the asymmetry of the double potential energy curves of D and T, all dimers can be trapped in the D minimum. The UV emission of the dimer is accompanied by the Stokes' shifted tautomer emission on excitation at 1050 cm−1 higher than the (0,0) band of D, which is interpreted as the barrier height of the double potential energy curves of D and T. Time-resolved studies at various temperatures have helped to clarify the photophysics of crystalline SA. 相似文献
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The strong paramagnetic susceptibility of liquid oxygen (LOX) has established it as a good candidate for a cryogenic magnetic fluid system. While its properties have been known for several decades, a fundamental understanding of the behavior of LOX in a magnetically controlled fluid system is needed for the development of a suitable space application that can operate reliably and efficiently. This study conducted quantitative experiments on the dynamics of a LOX slug in a tube when subjected to electrically-induced magnetic fields within a solenoid. The experiments used a quartz tube with an inner diameter of 1.9 mm and LOX slugs of 0.6, 1.3, 1.9, 2.5, and 3.2 mm length at various initial positions relative to the solenoid. The pressures generated by the motion of the LOX slug under the magnetic force were recorded to characterize the pressure differential generated and the breakdown of the slug. The highest attainable pressure differential was found to be 1.45 kPa, which correlated well to theoretical predictions once the analysis accounted for the resistance heating of the solenoid. The noted differences between experimental results and theory could also be attributed to impeded slug motion from shear and mass forces. Within the workable pressure range, however, an optimal slug length was found which appropriately balances the pressure, shear, and magnetic forces in the system. This paper presents the experimental data on the dynamics and the maximum pressure differential generated by a LOX slug in a magnetic field and discusses the viability of LOX in a magnetic fluid management system intended for space applications. 相似文献
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在传导冷却超导磁体系统中,超导磁体与系统其它部分的温度平衡过程是依靠固体间的热传导来实现热量传递的。由于超导磁体和冷屏等低温部件冷却条件的差异,将导致磁体内部各处和冷屏不同部位的温度分布不均匀。分析研究超导磁体系统的低温温度分布状况,对于低温系统的热设计和磁体的温度裕度设计具有重要意义。文中借助于ANSYS有限元分析软件,建立了一个大口径传导冷却超导磁体低温系统的稳态三维热分析模型,仿真了超导磁体和冷屏的空间温度场,得到了传导冷却超导磁体低温系统的热分布规律。该分析结果对于大口径传导冷却超导磁体的低温系统设计具有重要的参考价值。 相似文献