用LBS—16B型高速相机记录高温动态云纹干涉条纹

以３０ｍＷＨｅ－Ｎｅ激光作为相干光源，用ＬＢＳ—１６Ｂ型高速相机连续记录ＬＹ１２铝板试件在大电流快速加热条件下的动态云纹干涉条纹图像，获得了１０００幅／ｓ的有效拍摄频率，为将云纹干涉应用于高温动态变形测试提供了一种有效的方法。     

利用联合付里叶变换谱干涉法测量透镜焦距

本文提出了采用联合付里叶变换频谱干涉法测量透镜焦距的方法。输入面上两个分布完全相同的图像经光学付里叶变换在频谱面上得到二者付里叶变换频谱的干涉条纹，通过测量干涉条纹的间距即可得到透镜的焦距。该方法装置简单、操作调整方便；易于采用实时空间光调制器、ＣＣＤ及微机实现快速自动测量，且具有较高的精度。文中进行了原理分析和实验验证。     

基于微流控技术的磁流体载基液的太赫兹透射特性研究

太赫兹(THz)是指频率在0.1～10 THz的电磁波,其波长在30～3 000 μm范围内。由于自然界许多小分子的振动、转动等的频率均在太赫兹波段,并且太赫兹的低电子能特性使其在实验过程中不会对待测样品造成破坏,所以太赫兹技术被广泛地应用于无损检测、生物医学等领域。但是太赫兹在铁磁领域的相关报道还是较少的,因此本研究利用太赫兹时域光谱系统研究了一种新型磁性材料：磁流体的组成部分-载基液的太赫兹透射特性。磁流体是一种兼具液体流动性和固体磁性的新型功能材料,其打破了传统磁性材料的固体形态。磁流体由Fe₃O₄纳米级颗粒以及载基液构成。在前人的研究成果中发现磁性液体不仅具有良好的磁光效应,而且对于一定频率的太赫兹波具有高透射率;另外,在极低频电磁场作用下其可用于医学上的肿瘤治疗,可作为靶向治疗的载药系统。由于磁流体的组成部分-载基液成本较高,因此在实验中运用了微流控技术。微流控技术对检测样品的消耗少、检测速度快,并且可以根据实验需求自行设计沟道,因此是一种便捷的、灵活性好的检测方式。采用对太赫兹波具有高透过率的石英材料制成了夹心式的太赫兹微流控芯片。首先将两块3 cm×3 cm×2 mm的石英玻璃作为基片和盖片,再把强粘黏性双面胶剪刻成镂空样式,形成2 cm×2 cm的方形区域,然后把盖片和基片通过雕刻好的强粘黏性双面胶键合,其沟道厚度为50 μm,可以用于对少量液体的探测,并且可以使载基液呈薄膜状。之后将太赫兹技术和微流控技术相结合,利用太赫兹时域光谱(THz-TDS)系统研究了载基液的太赫兹透射特性,通过对太赫兹时域光谱以及频域光谱的研究发现,装有载基液的微流控芯片的信号强度高于空的微流控芯片,这一发现为载基液的应用和深入研究提供了技术支持。     

A facile synthesis of monodisperse CoFe2O4/SiO2 nanoparticles

Aminated-CoFe₂O₄/SiO₂ magnetic nanoparticles (NPs) were prepared from primary silica particles using modified StÖber method. By optimizing the preparation conditions, monodisperse CoFe₂O₄/SiO₂ NPs with high amino groups’ density were obtained, which is necessary for enzyme immobilization. TEM confirm that the sample is a core/shell structure. These aminated-CoFe₂O₄/SiO₂ NPs have narrow size distributions with a mean size of about 60 nm. Moreover, the aminated-CoFe₂O₄/SiO₂ NPs can be easily dispersed in aqueous medium. The experimental results also show that the NPs have superparamagnetism, indicating that the aminated-CoFe₂O₄/SiO₂ NPs can be used as an effective carrier for the enzyme immobilization.     

多肽自组装技术及其在生物医学上的应用

多肽分子自组装广泛存在于自然界中。多肽具有良好的生物相容性和可调控的降解性能,并且利用多肽自组装技术,可以在分子水平上设计并调控聚集态的形状和结构,这在生物医学材料方面具有巨大的应用潜力。近年来关于多肽自组装的研究成为材料学、医学等领域中研究热点之一,并且在药物缓释载体、组织工程支架研究方面取得进展。本文介绍多肽分子自组装技术的概念,综述了多肽自组装技术在药物缓释载体材料、组织工程支架材料方面的应用。     

天然高分子药物微球载体材料的研究进展

综述了国内外在天然高分子药物微球载体材料研究及应用中的进展状况,主要从天然高分子药物微球载体材料的分类、微球的制备方法及特点、载药微球的给药途径和应用等进行概括,并对目前所存在的问题进行了描述。     

Pyrene Derivate Functionalized with Acetylene for Organic Field Effect Transistors

A new X-shaped compound (SiPy) functionalized with acetylene bonds in the 1-, 3-, 6-, and 8-positions of the pyrene core has been synthesized by Sonogashira coupling reactions. Its photophysical, thermal, and organic field effect transistor (OFET) properties as well as the film morphologies have been investigated. SiPy exhibits high stability which is evidenced by thermal gravimetric analysis. The atomic force microscopy images reveal that the morphol-ogy of thin films depends on the substrate temperature. The film OFET devices based on SiPy were constructed and exhibited p-type performances.     

Electrochemical performance of a nano SnO2-modified LiNi1/3Co1/3Mn1/3O2 cathode material

The nano SnO₂-modified LiNi_1/3Co_1/3Mn_1/3O₂ was successfully prepared by a carrier transfer method. The pristine and modified samples were characterized with various techniques such as XRD, SEM, XPS and EDS. The results showed that the SnO₂ particles did not enter the crystal structure of LiNi1/3Co1/ 3Mn1/3O₂, many nano SnO₂ particles were uniformly covered on the surface of LiNi_1/3Co_1/3Mn_1/3O₂ and the modified thin layer could inhibit the dissolution of transition metal oxides. The electrochemical tests indicated that the existence of nano SnO₂ could improve the discharge capacity and rate capability owing to the decreased interfacial polarization. The cycling stability was remarkably improved at room temperature and 55 ℃. The XRD patterns of the fresh NCM electrode and after 50 cycles proved that the structural change of NCM was not so effective on the capacity fade.