微电渗流毛细管原位柱中流动相组成对电渗流的影响

采用原位聚合的方法合成了一种新型微电渗流毛细管电泳原位柱。考察了不同有机调节剂种类和浓度 ,pH对电渗流的影响 ,在 pH值 2 .3～ 9.8范围内 ,电渗流小于 19.6× 10 -10 m2 V-1s-1。当有机调节剂浓度从 6 0 %增加到 90 %时 ,电渗流仅从 6 .6× 10 -10 m2 V-1s-1增大到 4 8.9× 10 -10 m2 V-1s-1。结果表明 ,此类微电渗流柱在电色谱分离模式下电渗流保持在较低水平     

魔方矩阵的特征值分析

数值实验显示 :魔方矩阵的特征值除最大者为魔方值外 ,其余或为 0 ,或呈正负、共轭成对出现     

基于Samelson逆的向量值连分式的收敛准则

The aim of this work is to give some criteria on the convergence of vector valued continued fractions defined by Samelson inverse. We give a new approach to prove the convergence theory of continued fractions. First, by means of the modified classical backward recurrence relation, we obtain a formula between the m-th and n-th convergence of vector valued continued fractions. Second, using this formula, we give necessary and sufficient conditions for the convergence of vector valued continued fractions.     

全纯函数族涉及公共值的正规定则

研究涉及公共值的全纯函数正规族问题．设F为单位圆△内的全纯函数族,a,b为两个判别的有穷复数且b≠0．文中证明了若对每一个,f∈F,Ef(a)=Ef(a),E↑-f′（b)包含于E^-f(b),则F在单位圆△内正规．     

色谱法测定手性四面体金属簇合物对映体过量值

在自制的直链淀粉-三(苯基氨基甲酸酯)(ATPC)高效液相色谱手性固定相(HPLC-CSP)上,优化了手性四面体金属簇合物的手性分离条件,测定了不同合成条件下得到的手性四面体金属簇合物C0M0(CO)5C5H4C(O)CH3(μη^2-HC≡CCH2OH)的对映体过剩值(ee)。结果表明,高效液相色谱手性固定相法是拆分这类化合物的一种理想方法。     

多自由度线性微幅振动系统简正坐标的一般求法

给出了动能矩阵为对角矩阵,在A=aE和A≠aE(E为单位矩阵)两种情况下同时对角化势能矩阵求简正坐标的一般方法,并提出了先改变坐标标度,后对角化新势能矩阵或用频率特征矩阵的伴随矩阵的任一列求简正坐标的另两种方法．     

基于随机相位实值编码的光学图像加密

提出了一种用于图像加密的随机相位实值编码方法,待编码的纯相位图像与一个随机相位掩膜一起作傅里叶变换,取其实部作为编码图像.已编码的图像和随机相位掩膜的傅里叶变换相加作傅里叶反变换,反变换的光强可以准确地重建原图像.该编译码方法简单,编码图像是一个实值图像,便于计算机打印或显示输出.     

Influence of pH value on microstructure and thermal stability of Ni-P electroless coating prepared in acidic condition

Three kinds of Ni-P electroless coatings were prepared in nickel sulphate solution at different pH values of 4.5,5.5 and 6.5 with the purpose of ascertaining the influence of pH value on microstructure,internal stress statue and thermal stability of the coatings.Laser curvature(LC) method was used to measure the residual stress level in the coatings.Scanning electronic microscopy(SEM) and transmission electronic microscopy with energy dispersive spectrum(TEM/EDS) were used to examine the surface morpholo...     

CLASSIFICATION OF POSITIVE SOLUTIONS FOR NONLINEAR DIFFERENTIAL AND INTEGRAL SYSTEMS WITH CRITICAL EXPONENTS

We classify all positive solutions for the following integral system：{ui（x）=∫Rn1/│x-y│^n-α fi（u（y））dy,x∈R^n,i=1,…,m,0〈α〈n,and u（x）=（u1（x）,u2（x）…,um（x））.Here fi（u）, 1 ≤ i ≤m, monotone nondecreasing are real-valued functions of homogeneous degree n＋α/n-α and are monotone nondecreasing with respect to all the independent variables U1, u2, ..., urn.In the special case n ≥ 3 and α = 2. we show that the above system is equivalent to thefollowing elliptic PDE system：This system is closely related to the stationary SchrSdinger system with critical exponents for Bose-Einstein condensate     

马尔可夫过程H-值可加泛函的向前向后鞅分解

本文研究了马尔可夫H-值可加泛函的向前向后鞅分解.利用Lyons-Meyer-Zheng鞅分解得到了泛函数极限定理所必需的极大不等式和紧性结果,在最小条件限度内得到了马尔可夫过程经验测度的泛函中心极限定理,将该定理从实值情形推广到了希尔伯特值情形.