大口径宽视场双波段扫描红外相机光学设计

通过分析计算,设计了一种大口径宽视场折射式红外相机光学系统。该系统设计用于超长线阵扫描红外相机的地面演示成像,它能同时对短波2μm—3μm、中波3μm—4.5μm双波段成像,且同时具有24°的大视场和150mm的宽口径,成像质量接近衍射极限。该系统在航天遥感领域应用广泛。     

Ultrasound imaging and evaluation of lesion induced by High Intensity Focused Ultrasound

The present study was to investigate the differential imaging method for detecting HIFU (High Intensity Focused Ultrasound)-induced lesions and the estimation of variation of attenuation for lesion evaluation with log spectral difference algorithm. Experiment results of bovine muscle and liver in vitro were acquired. Several algorithms for lesion detection - Absolute Difference (AD), Sum Absolute Differences (SAD) and Sum Squared Differences (SSD) - were analyzed with several window sizes and threshold values. Then three attenuation parameters were compared to evaluate the degree of tissue damage. It was found that variation of the mean attenuation △α was an effective parameter to evaluate lesions.     

离子交换富集-导数火焰原子吸收法测定自来水中Cu,Fe和Zn

本文研究了用 2 0 1× 7阳离子交换树脂对自来水中的微量元素进行交换富集 ,采用微量脉冲进样 导数火焰原子吸收法测定富集后溶液中的Cu ,Fe和Zn ,该方法灵敏度分别为 0 2 9,0 5 9和 0 0 6 μg·L- 1 ,精密度分别为 4 2 8% ,1 95 %和 2 2 8% ,检测限分别为 1 2 8,5 85和 0 6 8μg·L- 1 ,回收率分别为 91 13% ,10 1 34%和99 84 % ,本方法大大减少了需样量 ,简便快速 ,灵敏度高。     

混合判断矩阵排序方法研究

本文介绍了混合判断矩阵及完全一致性混合判断矩阵的概念，提出了混合判断矩阵排序的一种最小偏差法，并给出了其收敛性迭代算法，最后通过算例说明了方法的可行性。     

多相体系中Ni-PMMA纳米复合材料的γ辐射制备

在多相体系中 ,运用γ射线辐射法 ,在常温常压下成功地一步合成了镍 聚甲基丙烯酸甲酯 (Ni PMMA)纳米复合材料 .XRD、TEM分析和IR光谱表明 ,在此实验条件下 ,镍离子和甲基丙烯酸甲酯已成功地被还原或聚合 ,镍粒子为面心立方 ,尺寸为 7.33nm .研究显示 ,用醋酸钠代替氢氧化钠或氨水作为碱性试剂 ,可以有效地控制体系的pH ,同时不影响单体的聚合 .     

AAS测定纸巾中的铅和镉

本文采用原子吸收光谱法测定纸巾中铅、镉的含量。结果表明，不同纸巾中的污染元素铅、镉的含量不同。同时还对一种纸巾的铅、镉元素进行了回收实验，回收率在92％-104％之间。     

一种高信噪比的双光束激光光声光谱仪原理及应用

作为一种新兴的检测手段 ,激光光声光谱技术与其他检测技术相比具有很多优点。本文设计的光声光谱仪用激光做光源 ,有两个光声池 ,分别用来放置参考样品和待测样品 ,输出结果为二者光声信号的比值。利用这一比值 ,可以由参考样品的性能参数方便地求出待测样品的相关性能参数。该光声光谱仪有效地减小了本底吸收噪声的影响 ,提高了信噪比 ,扩大了固体光声理论的应用范围。本文还阐述了该光声光谱仪在定性定量分析中的一些应用     

稀土甘氨酸咪唑配合物[RE(Gly)4(Im)(H2O)](ClO4)3的热化学研究

采用溶解-反应量热法在具有恒温环境的溶解-反应热量计内,测定了[Gd(Gly)4(Im)(H2O)](ClO4)3和[Y(Gly)4(Im)(H2O)](ClO4)3两种稀土甘氨酸咪唑配合物的标准生成焓分别为(-3 461.46 ±0.22) kJ·mol-1 和(-3 926.6±0.90) kJ·mol-1.     

A Facile Synthesis of Silver-Coated Composite Particles by Swelling Surface Method

We report a facile and rapid method for fabrication of composite particles consisting of a polystyrene (PS) core and a uniform silver shell. The process involves the PS colloid surface swelling, the anchoring of silver ions and nanoparticles onto the surfaces, and the subsequent growth of metal seeds in a short period. The present approach has the advantages of simplicity and high efficiency. The TEM images show the morphology of the obtained PS core-silver shell particles, and their chemical composition and crystallinity are analysed by x-ray diffraction. To our knowledge, this is the first study based on swelling PS surface for synthesis of silver-coated PS particles and may be implemented for preparing other metal-coated PS particles.