SPECTRO光电直读光谱仪的取样与使用

直读光谱仪分析快速、准确,操作简单,方便实用,已得到了广泛应用。本文介绍了光电直读光谱仪的取样及操作。     

An optical fiber methane gas sensing film sensor based on core diameter mismatch

<正>An optical fiber evanescent wave methane gas sensor based on core diameter mismatch is reported.The sensor consists of a multimode fiber in which a short section of standard single-mode fiber,coated with the inclusion of cryptophane molecules E in a transparent polysiloxane film,is inserted.The sensing principle is analyzed by optical waveguide theory.For different sensing film thicknesses and interaction lengths,the sensor signal is investigated within the methane concentration range of 0-14.5%(v/v).It is shown that the sensor signal with the thickness of 5μm and the interaction length of 3 mm strengthens linearly with the increasing concentration of methane,with a slope of 0.0186.The best detection limit of the sensor for methane is 2.2%(v/v) with a response time of 90 s.This sensor is suitable for the detection of methane concentration below the critical value of 5%.     

Z-扫描参量对薄膜材料三阶非线性光学特性的影响

采用数值计算方法对薄膜材料的Z-扫描参量进行研究.对不同激光脉宽下Z-扫描的三阶非线性折射系数和吸收系数进行分析,结果显示不同等级的脉宽激光器对计算结果的数量级影响很大.对不同小孔光阑半径的Z-扫描闭孔曲线进行仿真,结果显示光阑小孔越小,获得特征曲线的峰谷值越明显.对不同光阑离透镜焦点的距离值进行Z-扫描闭孔曲线仿真,结果显示距离为1/2透镜焦距值时闭孔Z-扫描曲线能得到相对较大的峰谷差值.数值分析结果与相关文献报道的实验结果基本一致.     

氢稀释对纳米晶硅薄膜晶化特性的影响及薄膜生长机理

以SiH₄与H₂作为前驱气体,采用射频等离子增强化学气相沉积技术制备了纳米晶硅薄膜.利用Raman散射和红外吸收光谱等技术,对不同氢稀释比条件下薄膜的微观结构和键合特性进行了研究.结果表明,随着氢稀释比增加,薄膜的晶化率明显提高,而氢稀释比过高时,薄膜晶化率呈现减少趋势.红外吸收光谱分析表明,纳米晶硅薄膜中氢的键合模式与薄膜的晶化特性密切相关.随着氢稀释比增加,薄膜中整体氢含量和SiH₂键合密度明显减少,而在高氢稀释比条件下,氢稀释比增加导致薄膜中SiH₂键合密度和整体氢含量增加.     

Z箍缩软X射线辐射能量薄膜量热计改进技术

薄膜量热计是进行Z箍缩辐射总能量测量的主要手段之一,准确可信的总能量参数对Z箍缩研究具有重要意义。对薄膜量热计装置进行技术改进,采用脉冲恒流源代替脉冲恒压源驱动镍薄膜量热计,撤除了回路中的串接电阻,可直接测量薄膜探测器的电阻变化,从而有效提高了辐射总能量测量的精度,拓宽了该设备的适用范围,使其可对目前强光一号加速器Z箍缩实验中所有典型负载进行测量。改进后平面型铝丝阵负载实验中总能量测量的相对不确定度由49.0%降低为19.6%。与闪烁探测系统功率测量结果积分值进行了对比,二者比值在0.87~1.04之间。     

电弧蒸馏光谱法测定地球化学样品中银及其他痕量元素的研究进展

发射光谱法因具有多元素同时测定,分析速度快,灵敏度高,检出限低,使用方便的特点,被用于地质样品中银及其他痕量元素的测定。随着我国地质勘查事业的发展和地球化学调查工作力度的加大,对覆盖区的多目标地球化学调查样品的测试及质量控制提出了更高的要求。同时分析方法和测试技术有了新的进展。基于蒸馏原理的电弧光谱测试技术也有了多方面的进展。本论文归纳总结了国内主要刊物上所发表的电弧蒸馏光谱法测定地球化学样品中银及其他痕量元素的研究和应用情况,重点就固体缓冲剂的组成成分进行简要概述,以期为今后样品测试提供参考。     

Surface Acoustic Wave Characterization of Equivalent Young's Moduli for Patterned Films北大核心CSCD

Based on the equivalent elasticity theory for layered materials, the micro-mechanics equivalent models for single and dual damascene structures were established. The equivalent elastic constant of the patterned structure was introduced, to establish the propagation model for the surface acoustic waves propagating in the layered structure of the patterned film/ substrate, and the theoretical dispersion curves of the surface acoustic waves were calculated with Green’s function and the matrix method. The finite element method was used to calculate 24 numerical examples of damascene structures with different volume ratios, and the results were compared with those of the strain energy method. The results show that, the average relative errors of the equivalent Young’s moduli of the 300 nm-thick dual damascene film and the 100 nm-thick single damascene film are 2.06% and 2.27%, respectively. The research verifies the correctness of the equivalent patterned structure model and the feasibility of the surface acoustic wave method to characterize the mechanical properties of patterned films, and provides a reference for the development of suitable chemico-mechanical polishing technologies for patterned films under low pressure. © 2023 Editorial Office of Applied Mathematics and Mechanics. All rights reserved.