Mehr-Detektor-Anordnung für die Koinzidenzmessung von Positronenstrahlern

Procedures are given for the title compounds, which allow their preparation in high chemical purity and without any depletion of the ¹⁵N-content. A nitrogen isotope exchange between NOBF₄ and ¹⁵N₂O₃ was found, but it is too slow for preparative purposes.     

局部方差在图像质量评价中的应用

将灰度图像的局部方差分布（QLS）作为表征图像结构信息的一个重要特征,对局部方差分布矩阵进行奇异值分解,计算得到相应的奇异值特征向量;通过计算降质图像与原参考图像局部方差矩阵奇异值特征向量的夹角大小度量两图像的结构相似度,实现了对降质图像的质量评价。实验结果表明：局部方差分布更能突出图像的结构特征,评价结果优于传统的均方误差（MSE）、峰值信噪比（PSNR）、结构相似度（SSIM）以及直接评价图像像素分布的奇异值分析（SVD）等方法,与人眼视觉感知效果的一致性较好。     

Preparation and Characterization of Poly Vinyl Alcohol/Poly Vinyl Pyrrolidone/Clay Based Nanocomposite by Gamma Irradiation

A series of PVA/PVP/clay nanocomposite were prepared by gamma irradiation with different clay contents of (0.15, 0.3, 1, 1.5, 3 and 5 wt%). The gelation content and swelling behavior were investigated. The morphology and structure of PVA/PVP/clay nanocomposite and dispersion of the clay nanoparticles in the polymeric matrix were examined by infrared spectroscopy (FT-IR) and scanning electron microscopy (SEM). The introduction of clay into polymeric matrix was investigated by X-ray diffraction pattern (XRD) and Transmission electron microscope (TEM). It is observed that, the increase of the clay content causes a decrease in the swelling percent. The thermal stability studies confirmed that the introduction of clay lead to an increase in the thermal stability. The TEM results showed that the clay nanoparticles are interchelated or exfoliated in the polymeric matrix. Some desirable characteristics such as relatively good swelling and excellent barrier capability against microbe penetration suggested that PVA/PVP/clay nanocomposite can be a good candidate as a wound dressing.     

Acyclovir-Loaded Chitosan Microspheres for Gastroretention: Development and Evaluation

Mucoadhesive chitosan microspheres of acyclovir were prepared to prolong the gastric residence time using simple emulsification phase separation technique. The particle morphology of drug-loaded formulations was measured by SEM and the particle size distribution was determined using an optical microscope. The release profile of acyclovir from microspheres was examined in simulated gastric fluid (SGF pH 1.2). The particles were found to be discreet and spherical with the maximum particles of an average size (31.62 ± 4.64). The entrapment efficiency was found to be in the range of 40.24 to 67.29%. The concentration of the glutaraldehyde (25%v/v) as a cross-linker 2 ml and drug polymer ratio of 1:2 caused an increase in the entrapment efficiency and the extent of drug release. The optimized chitosan microspheres were found to possess good bioadhesion (79.89 ± 1.01%). The gamma-scintigraphy study showed the gastric residence time of more than 6 hours which revealed that optimized formulation could be a good choice for gastroretentive systems.     

Mo_2C/γ-Al_2O_3催化剂上苯加氢反应的原位红外光谱研究

采用程序升温反应法制备了钝化态、还原钝化态和新鲜态Mo2C/γ-Al2O3催化剂,结合原位红外光谱表征技术和反应性能评价,考察、比较了三种催化剂苯加氢反应活性.原位红外光谱结果表明,新鲜态Mo2C/γ-Al2O3催化剂在室温就显示了较好的苯加氢反应活性,表现了类贵金属的催化活性.CO吸附在反应前后新鲜态Mo2C/γ-Al2O3催化剂上的对比结果表明,低价态的Mo位(Moδ+(0δ2))是苯加氢反应活性中心.三种催化剂的反应活性结果表明,新鲜态Mo2C/γ-Al2O3催化剂反应活性最好,催化剂寿命最长,失活之后在500°C下H2处理即可恢复原有活性.     

应用单波段亮度变化率获取无云干扰的卫星数据

在卫星遥感检测中,云对数据的反演带来了严重的干扰。精确地确定云区及减弱云的干扰是具有挑战性的问题。根据云的大气辐射特性给出了卫星图像亮度变化率计算公式、图像反射率的变化率计算公式和热红外波段图像亮度温度变化率的计算方法。利用单波段亮度变化率检测卫星数据中云干扰相对强度的新方法,快速、精确地获取云区位置,得到云区以外无云干扰的数据。根据各光谱波段具有不同的透射云层能力的特点,文章还给出了卫星各红外波段对云层透射能力的客观评价以及影响透射效果的因素。在此基础上利用红外波段对伪卷云透射图像数据完成了多波段数据融合。很好地恢复了可见光波段云区下面的真实数据。统计数据表明,融合后的云区图像数据与可见光波段相关性保持一致。     

基于灰度曲面匹配的虹膜识别方法

目前的虹膜识别都是采用在图像上提取特征点,并将特征点编码为固定长度的特征数据用于匹配的方式。这种方式使虹膜识别系统易受攻击。为了进一步提高虹膜识别系统的安全性和识别速度,提出了一种基于灰度曲面匹配的虹膜识别方法。该方法抛弃了特征提取和编码等传统操作,在特征分析的基础上直接利用了灰度曲面匹配的思想,首先对两幅图像中的像素灰度做差,得到灰度差曲面,然后求出该灰度差曲面的方差。将此方差作为衡量两个虹膜特征曲面之间距离的依据,并据此判定两个虹膜是否来自同一只眼睛。在给定阈值为40的前提下,正确识别率为96.89%,识别时间为53.2 ms。实验结果证明,该方法识别准确率高,识别速度快。