Dynamic mechanical thermal analysis transitions of partially and fully substituted cellulose fatty esters

The main transitions of cellulose fatty esters with different degrees of substitution (DSs) were investigated with dynamic mechanical thermal analysis. Two distinct main relaxations were observed in partially substituted cellulose esters (PSCEs). They were attributed to the glass‐transition temperature and to the chain local motion of the aliphatic substituents. The temperatures of both transitions decreased when DS or the number of carbon atoms (n) of the acyl substituent increased. Conversely, all the transitions of fully substituted cellulose esters occurred within a narrow temperature range, and they did not vary significantly with n. This phenomenon was explained by the formation of a crystalline phase of the fatty substituents. The presence of few residual OH groups in PSCEs was responsible for a large increase in the storage bending modulus, and it eliminated the effect of n on damping. © 2002 Wiley Periodicals, Inc. J Polym Sci Part B: Polym Phys 41: 281–288, 2003     

K-强凸空间的一些性质

结合Banach空间的Drop性，利用K维体积给出了K—强凸空间的一个新的定义，同时也给出了K—强光滑空间定义的K维体积表示，然后利用单位圆的切片证明了K—强凸空间是自反空间，进而证明了K—强凸空间与K—强光滑空间是一对对偶空间．最后利用Drop性的切片描述证明了K—强凸空间具有Drop性．     

关于非齐次m阶马氏信源的渐近均分割性

本文研究非齐次m阶马氏信源的渐近均分割性，首先我们得到关于此种信源m 1元函数的一类强极限定理，作为推论，得到关于任意非齐次m阶马氏信源状态和熵密度的几个极限定理，最后得到一类非齐次m阶马氏信源的渐近均分割性。     

四溴双酚A锑铝双金属化合物的合成及其阻燃性能

以四溴双酚Ａ（ＴＢＡ）合成了在水和空气中稳定的四溴双酚Ａ合锑铝双金属化合物（ＴＢＡＳＡ）．通过ＩＲ、１ＨＮＭＲ和元素分析予以表征，并研究了其对聚乙烯（ＰＥ）和聚环氧乙烷（ＰＥＯ）的阻燃性能．结果表明，这种分子中含有溴、锑和铝的化合物，对聚乙烯和聚环氧乙烷等高聚物材料有高的阻燃性能与消烟效果．     

Banach-Saks property in Marcinkiewicz spaces

We catalogue all Marcinkiewicz function and sequence spaces with the Banach-Saks property and present necessary and sufficient conditions for a wide subclass of spaces to possess the p-Banach-Saks property, 1<p<∞. We apply our results to several open problems.     

On the properties of solutions to the Goursat-Darboux problem with boundary and distributed controls

We consider a control system described by the Goursat-Darboux equation. The system is controlled by distributed and boundary controls. The controls are subject to the constraints given as multivalued mappings with closed, possibly nonconvex, values depending on the phase variable. Alongside the initial constraints, we consider the convexified constraints and the constraints whose values are the extreme points of the convexified constraints. We study the questions of existence of solutions and establish connections between the solutions under various constraints.     

Examples of non-Kähler Hamiltonian circle manifolds with the strong Lefschetz property

In this paper we construct six-dimensional compact non-Kähler Hamiltonian circle manifolds which satisfy the strong Lefschetz property themselves but nevertheless have a non-Lefschetz symplectic quotient. This provides the first known counterexamples to the question whether the strong Lefschetz property descends to the symplectic quotient. We also give examples of Hamiltonian strong Lefschetz circle manifolds which have a non-Lefschetz fixed point submanifold. In addition, we establish a sufficient and necessary condition for a finitely presentable group to be the fundamental group of a strong Lefschetz manifold. We then use it to show the existence of Lefschetz four-manifolds with non-Lefschetz finite covering spaces.     

Characterization and recognition of generalized clique-Helly graphs

Let p?1 and q?0 be integers. A family of sets F is (p,q)-intersecting when every subfamily F^′⊆F formed by p or less members has total intersection of cardinality at least q. A family of sets F is (p,q)-Helly when every (p,q)-intersecting subfamily F^′⊆F has total intersection of cardinality at least q. A graph G is a (p,q)-clique-Helly graph when its family of (maximal) cliques is (p,q)-Helly. According to this terminology, the usual Helly property and the clique-Helly graphs correspond to the case p=2,q=1. In this work we present a characterization for (p,q)-clique-Helly graphs. For fixed p,q, this characterization leads to a polynomial-time recognition algorithm. When p or q is not fixed, it is shown that the recognition of (p,q)-clique-Helly graphs is NP-hard.     

Generalized Physical and SRB Measures for Hyperbolic Diffeomorphisms

In this paper we introduce the notion of generalized physical and SRB measures. These measures naturally generalize classical physical and SRB measures to measures which are supported on invariant sets that are not necessarily attractors. We then perform a detailed case study of these measures for hyperbolic Hènon maps. For this class of systems we are able to develop a complete theory about the existence, uniqueness, finiteness, and properties of these natural measures. Moreover, we derive a classification for the existence of a measure of full dimension. We also consider general hyperbolic surface diffeomorphisms and discuss possible extensions of, as well as the differences to, the results for Hènon maps. Finally, we study the regular dependence of the dimension of the generalized physical/SRB measure on the diffeomorphism. For the proofs we apply various techniques from smooth ergodic theory including the thermodynamic formalism. 2000 Mathematics Subject Classification. Primary: 37C45, 37D20, 37D35, Secondary: 37A35, 37E30     

p型未掺杂富锌ZnO薄膜的形成和性能研究

以高纯ZnO为靶材,氩气为溅射气体,利用射频磁控溅射技术在石英衬底上生长出纤锌矿结构的富锌ZnO薄膜.薄膜沿(002)择优取向生长,厚约为1.2μm,呈现电绝缘特性.将溅射的ZnO薄膜在10-3Pa,510~1 000 K的温度范围等温退火1 h,室温Hall测量结果表明ZnO薄膜的导电性能经历了由绝缘—n型—p型—n型半导体的变化.XPS测试表明ZnO薄膜的Zn/O离子比随退火温度的升高而降低,但一直是富锌ZnO,说明未掺杂的富锌ZnO也可以形成p型导电.p型未掺杂富锌ZnO薄膜的形成可归因于VZn受主浓度可以克服VO和Zni本征施主的补偿效应.