胆固醇(Cholesterol)嵌入卵磷脂(PC)有序体后对其中CaCO3晶型结构的影响

在PC和Chol/PC有序体中进行CaCO₃沉淀反应,用X射线衍射和扫描电镜方法表征了反应物结构,研究了作为有机模板剂的不同分子有序体对CaCO₃的晶型和形态的指导作用.在反胶束合成中出纳米级CaCO₃颗粒.胆固醇对有序体有显著影响,进而影响此体系中形成的CaCO₃晶型,可诱导生成3种CaCO₃异构体:胶体CaCO₃、球霰石和方解石.方解石含量随胆固醇含量增加减少.     

ICA方法与NIR技术用于药片中活性成分含量的测定

用独立分量分析(ICA)方法提取药片近红外光谱数据矩阵的独立成分和相应的混合矩阵, 再用BP神经网络对混合矩阵和药片中活性成分的浓度矩阵进行建模, 提出了新的药片活性成分含量测定的基于独立分量分析-神经网络回归(ICA-NNR)的近红外光谱分析方法. 通过分析独立分量数和网络中间隐层的神经元数对模型性能的影响, 分别建立三类药片定量分析的最优模型. 该方法用于实测的三类药片中活性成分含量的测定, 测试样品集的化学检测值与近红外预测值的相关系数分别达到0.962, 0.980及0.979. 结果表明, 基于ICA-NNR的近红外光谱分析方法对制药业的药片进行定量分析是可行的.     

卵磷脂中PE及不同种类PC的高效液相色谱分析

卵磷脂具有重要的生理功能,是人体正常新陈代谢和健康生存不可少的物质,能改善治疗神经系统疾病,增强记忆力,防止心血管疾病等。在临床上卵磷脂的主要的用途是用于治疗动脉粥样硬化、脂肪肝、神经衰弱、营养不良及静脉注射脂肪乳的乳化剂、胆固醇结石的防治药物,引。美国、欧洲、日本等已将磷脂在临床上用于防治脑、心、肝、肿瘤等疾病。     

Electrical–thermal aging characteristic research of polymer materials by infrared spectroscopy,

Traditional insulation paper (pressboard) used in power transformers has weaknesses such as poor thermostability, low breakdown voltage, and high permittivity, which leads to its degradation or even breakdown over time. For this paper, in order to judge if they could be used as new insulation materials for transformers, polycarbonate and polyester films were selected for electrical–thermal aging tests in temperatures of 110°C and 130°C in comparison with the insulation paper. Several infrared spectral tests were carried out on the three materials under a scanning electron microscope to analyze their electrical–thermal aging characteristics, mechanical behaviors, and degrees of polymerization. The functional group whose absorption peak intensity decreased drastically with aging was referred to as the characteristic functional group, and its peak absorption intensity was used to reflect its aging level. This paper found that the polycarbonate had a better aging resistance than both the insulation paper and PET. Copyright © 2014 John Wiley & Sons, Ltd.     

Effect of triaxial stress constraint on the deformation and fracture of polymers

One purpose of this paper is to give a brief overview on the research status of deformation, fracture and toughening mechanisms of polymers, including experimental, theoretical and numerical studies. Emphasis is on the more recent progresses of micromechanics of rubber particle cavitation and crazing, and the development of fracture criteria for ductile polymers. The other purpose is to study the effect of triaxial stress constraint on the deformation and fracture behavior of polymers. Polycarbonate (PC), acrylonitrile-butadienestyrene (ABS) and PC/ABS alloy are considered in this investigation. A series of circumferentially blunt-notched bars are used to experimentally generate different triaxial stress fields. The fracture surfaces of specimens with different notch radius are examined by scanning electron microscope (SEM) to study the fracture and toughening mechanisms of polymer alloy. It is shown that the triaxial stress constraint has a significant effect on the deformation, fracture and toughening of PC, ABS and PC/ABS alloy. We will also discuss the extent to which a micromechanics criterion proposed by the first author can serve as a fracture criterion for ductile polymers. A new ductile fracture parameter is emphasized, which can be employed to evaluate the fracture ductility of polymers. Stress state independence of the parameter for the PC, ABS and PC/ABS alloy has been experimentally verified. The project supported by the National Natural Science Foundation of China (10125212), the Trans-Century Training Program Foundation and the Key Research Fund of the Education Ministry of China (01159)     

陀螺数字PID温度控制系统设计与实现

介绍了陀螺温控系统的传统控制方法,并在此基础上提出了基于PC/104的数字PID控制的陀螺温度控制方法。实验结果表明这种控制方法能够满足陀螺快速启动、并保持其内部工作温度恒定的精度要求。     

大型边界元方程组的并行直接分块求解算法

针对大型边界元方程组和网络微机机群环境提出了一种并行直接分块求解算法，算法基于分块高斯-若当消去法的原理，采用内外存交互技术，并行分块消去方法，节点超行的卷帘存储方案和并行环状循环逐次修正策略，增大了解题规模，提高了计算速度。算例计算结果表明该算法具有较高的并行加速比和并行效率，适用于大型问题的边界元法求解。     

有限元子结构并行算法的性能分析

 对有限元子结构并行算法的主要步骤进行了归纳，比较准确地 计算了算法的计算量和通信量. 并在此基础上分析了算法的性能和可 扩展性，最后指出了影响算法并行效率的关键因素，并给出了算法优 化方向和改进建议.     

选择性发射极晶体硅太阳电池的二维器件模拟及性能优化

利用PC2D二维模拟软件对选择性发射极晶体硅太阳电池(SE电池)进行了器件模拟和参数优化的研究.在对丝网印刷磷浆法制备的SE电池的实测典型电流-电压曲线实现完美拟合的基础上,全面系统地研究了栅线、基区、选择性发射区和背表面场层等的参数对电池性能的影响.模拟表明:基区少子寿命、前表面复合速度和背表面复合速度是对电池效率影响幅度最大的三个参数.在所研究的参数范围内,当基区少子寿命从50μs上升到600μs时,电池效率从18.53%上升到19.27%.低的前表面复合速度是使发射区方块电阻配比优化有意义的前提.要取得理想的电池效率,背表面复合速度需控制在500 cm/s以下.此外,对于不同的前表面复合速度,电池效率的最大值总是在50—90Ω/□的重掺区方阻、110—180Ω/□的轻掺区方阻的范围内取得.对不同的栅线数目,重掺区宽度与栅线间距之比为32%时,电池的效率最高.另外,在主栅结构保持较低面积比率的前提下,主栅数目的增加也可提高效率.最后,通过优化p型SE电池的效率可达到20.45%.