Comprehensive evaluation of solvent in dispersive liquid-liquid microextraction for determination of itraconazole and hydroxy itraconazole by high performance liquid chromatography with fluorescence detection

This paper aims to propose a multicriteria decision analysis (MCDA) method to evaluate and select solvent in a dispersive liquid-liquid microextraction (DLLME) approach. The DLLME is applied to the determination of itraconazole and hydroxy itraconazole in plasma by high performance liquid chromatography with fluorescence detection (HPLC-FLD). To achieve this goal, extraction efficiency, chromatographic resolution, and greenness of solvent were identified as the three indicators in MCDA. Then, Technique for Order of Preference by Similarity to Ideal Solution (TOPSIS) was employed to evaluate and select the solvent. Weight assignment was set up by integrating the subjective scoring from experienced analysts and the objective approach using Shannon’s entropy weight method. Under chosen parameters (extraction solvent: 1-decanol 40 μL, dispersing solvent: methanol 400 μL), the method was validated satisfactorily and applied successfully to the analysis of itraconazole and hydroxy itraconazole in real human plasma samples. The results show that the comprehensive weighted TOPSIS analysis is a promising tool to choose experimental conditions toward an integrative goal. It can provide analysts with a decision making reference to maintain a balance between the analytical performance and eco-friendliness.     

饱和土体自重固结问题的相似解

采用了比以往更为普遍的土体物理力学性质假设,利用Hopf-Cole变换方法求得了厚层土体在自重应力作用下的非线性固结问题的完整解析解答．通过试验数据,将该解答与传统的大应变线性固结理论解答和基于实验数据的有限元数值解答相比较,结果表明,该解答能够更好地描述土体的实际固结过程,而由线性化固结理论所得的解答对固结过程中的沉降量和固结度的估计偏小．     

地下强爆炸诱发地表塌陷的试验模拟与应用

地下核爆炸后会在地表产生下陷弹坑、塌陷带等不可逆变形爆炸后效应,利用地表形变信息对地下核试验进行有效监控和评估具有十分重要的意义。基于考虑重力影响的地下强爆炸塌陷成坑相似理论,利用陆军工程大学自主研制的地下爆炸效应真空室模拟试验装置,对2017年9月3日朝鲜地下核试验诱发的地表不可逆变形进行了模型试验。试验结果表明,地表塌陷带半径为257 m,下陷弹坑的半径为154 m,与美国、前苏联等国家已有的地下核试验经验公式的数据结果基本相当,并且符合天基雷达TS-InSar卫星监测数据的估算结果,验证了地下爆炸真空室模型试验在地下强爆炸诱发地表不可逆变形区域模拟和评估的可行性,成为有效补充地震波和卫星监测地下强爆炸的一种研究手段。     

Segmentation of synthetic aperture radar image using multiscale information measure-based spectral clustering

A multiscale information measure （MIM）, calculable from per-pixel wavelet coefficients, but relying on global statistics of synthetic aperture radar （SAR） image, is proposed. It fully exploits the variations in speckle pattern when the image resolution varies from course to fine, thus it can capture the intrinsic texture of the scene backscatter and the texture due to speckle simultaneously. Graph spectral segmen- tation methods based on MIM and the usual similarity measure are carried out on two real SAR images. Experimental results show that MIM can characterize texture information of SAR image more effectively than the commonly used similarity measure.     

海上浮式风力机支撑结构的流固耦合动力学研究

海上漂浮式风力机支撑结构动力载荷的确定不仅对于结构设计、施工过程非常重要,对于设施的运维保障同样重要。水动力载荷的计算可归为基于势流理论的理论模型和基于计算流体动力学的数值模型两类方法。本文简述了两类模型各自的基本原理,明确其优劣,为实际工程应用的合理建模提供参考。对于海洋工程,水池物理模型实验发挥着重要作用。本文以某结构型式的浮式支撑结构的物理模型实验为例,阐述了物理模型实验技术的局限性及改进措施,为工程建设提供必要的技术支撑。

     

On the Similarity of Perturbed Multiplication Operators

Let S be the multiplication operator by an independent variable x in L ₂(0,1), and let V be an integral operator of Volterra type. In this note, we find sufficient conditions for the similarity of the operators T := S + V and S and discuss some generalizations to an abstract setting of the results obtained.     

关于幂等阵的相似与线性组合

证明了数域上两个同阶幂等阵相似的充要条件是它们有相同的秩;给出了幂等阵的相似标准型;讨论了两个幂等阵的线性组合仍是幂等阵的充要条件.     

加权Bergman空间上解析Toeplitz算子的换位及相似

本文在加权Bergman 空间A_α²(D)(α>-1) 上证明了由n-Blaschke 因子诱导的解析Toeplitz算子相似于n个Bergman 移位的直接和, 刻画了一类解析Toeplitz 算子的换位并研究了两个解析Toeplitz 算子的相似性.     

Isomorphic edge disjoint subgraphs of hypergraphs

We show that any k‐uniform hypergraph with n edges contains two isomorphic edge disjoint subgraphs of size for k = 4, 5 and 6. This is best possible up to a logarithmic factor due to an upper bound construction of Erd?s, Pach, and Pyber who show there exist k‐uniform hypergraphs with n edges and with no two edge disjoint isomorphic subgraphs with size larger than . Furthermore, our result extends results Erd?s, Pach and Pyber who also established the lower bound for k = 2 (eg. for graphs), and of Gould and Rödl who established the result for k = 3. © 2016 Wiley Periodicals, Inc. Random Struct. Alg., 48, 767–793, 2016     

基于主元分析与动态时间弯曲的故障诊断方法及应用研究

轴承是工程实际中常用而又极易损坏的部件,特别是对其早期微弱响应的辨识,具有重要的社会价值和意义。为提高运转轴承的安全可靠性和可维护性,提出了基于主元分析与动态时间弯曲距离的故障诊断方法,它可以准确对早期微弱动态响应辨识、诊断。该方法首先将典型故障样本信号与待测信号小波去噪并EMD分解,并对若干固有模态分量主元分析求取主元,然后对主元分量进行分析,获得相关特征值组成特征向量,计算待测信号与已知故障样本信号特征向量的弯曲距离,弯曲距离越小表明两信号越相似,从而辨识故障。此外,还可将其应用于转子、碰磨、齿轮故障诊断中,工程应用实例表明该方法可以准确故障分类,高效故障诊断。