位置刻度分布族中参数的两步置信区间

寻找一些分布中的参数的具有预先给定宽度和预先给定覆盖概率的置信区间是令人感兴趣的，对于位置刻度分布族中位置参数和刻度参数，这种类型的置信区间的存在性问题已在文献中被解决，本文利用两步抽样，具体地构造出这样的固定宽度置信区间，此外，对于Cauchy分布，第一阶段的最优抽样量和一些统计量的分位点也被计算出，所得到的结果具有应用价值。     

ICP-AES氢化物发生法测定生物样品中的痕量硒

本文研究了ICP-AES氢化物发生法测定生物样品中痕量硒的方法。对氢化物发生条件和样品消化过程进行了选择,并使之达最佳化。方法检出限达0.09ng/ml。     

A new increasing delocalization of M=3d-elements (Ti, Fe, Co) in the channels network of the ternary MyMo6Se8 Chevrel phases

A structural investigation on single crystals of M_yMo₆Se₈ Chevrel phases (M=3d: Ti, Fe, and Co) has been carried out. These latter compounds as well as others with Cr, Mn, and Ni atoms make part of a new original family of Chevrel phases. The M ions occupy new interstices in the tridimensional channels network never observed in the other classical Chevrel phases as Li_y, Cu_y Mo₆X₈. They occupy only cavity 2 centered on and with a progressive delocalization of the M cation versus the nature of the cation from the center of the cavity to the outside . The position in cavity 2 is different from the position of the Cu (2) atoms, the second position of the copper atoms in the channels of the Cu_yMo₆X₈ compounds. This new position reinforces the interaction with the Mo₆ cluster, and may be able to involve new remarkable physical properties as thermoelectric properties.     

Mixing in the sample loop of the loop-type interface in coupled LC-GC

During introduction of an LC fraction into the sample loop of the loop-type interface mixing occurs between the fraction of interest and the material previously eluted from the LC. Such mixing may not only result in losses of the solute material of interest, but also in contamination of the fraction of interest with material from which it was supposed to have been isolated. Experimental determination of the extent of mixing has led to the conclusion that whereas the effects are negligible under some conditions, in some circumstances the mixing can cause severe problems.     

一类马氏样本下假设检验问题错误概率的估计

本文考虑样本不独立情形的统计推断问题,研究基于马氏样本的最优势检验,给出了此情形的Neyman-Pearson基本引理.当样本容易足够大时,利用大偏差原理,得到了Neyman-Pearson型检验所犯两类错误概率的精确估计,它推广了经典Neyman-Pearson基本引理的相关结果.     

A test for independence of two multivariate samples

The paper presents a new nonparametric test for independence of two vectors. The idea is based on zonotope approach by G. Koshevoy, H. Oja and others, see [4, 5]. Under the independence hypothesis the test statistic converges in distribution to the supremum of a certain Gaussian field, and its asymptotic distribution is found using the theory of extrema of random Gaussian fields developed by V. Piterbarg and Yu. Tyurin, see [6, 8]. In contrast to traditional correlation coefficients the formula is not symmetric.      

在线螯合树脂柱预富集分离ICP－AES测定生物试样中镉

本文报道了采用国产Ｄ４１２螯合树脂的在线微型螫合树脂柱预富集分离ＩＣＰ－ＡＥＳ法测定痕量镉的技术，选择了最佳的在线预富集条件，对生物标准参考物质中的痕量镉进行了测定，结果与标准值吻合。     

《1992年中央人民广播电台全国听众抽样调查》综合报告

本报告描述了１９９２年中央人民广播电台全国听众抽样调查的设计、主要结果和特色．     

Sample Duplication Method for Monte Carlo Simulation of Large Reaction-Diffusion System

The sample duplication method for the Monte Carlo simulation of large reaction-diffusion system is proposed in this paper. It is proved that the sample duplication method will effectively raise the efficiency and statistical precision of the simulation without changing the kinetic behaviour of the reaction-diffusion system and the critical condition for the bifurcation of the steady-states. The method has been applied to the simulation of spatial and time dissipative structure of Brusselator under the Dirichlet boundary condition. The results presented in this paper definitely show that the sample duplication method provides a very efficient way to sol-'e the master equation of large reaction-diffusion system. For the case of two-dimensional system, it is found that the computation time is reduced at least by a factor of two orders of magnitude compared to the algorithm reported in literature.     

竖直圆管中超临界压力CO2对流换热实验研究

本文对超临界压力CO2在竖直加热圆管内的对流换热进行了实验研究,比较了不同流向、不同热流密度等对流动和换热的影响。实验结果表明,管内径为2mm时,在低进口Re条件下,由于浮升力影响导致层流向湍流提前转变, 对流换热增强;与向上流动相比,向下流动更易由层流转变为湍流;向下流动的换热要强于向上流动,表明浮升力对换热有很大影响。对于管内径为0．27 mm的微细圆管,当进口Re高于104时,浮升力的影响可以忽略,对流换热系数的变化完全由物性的变化尤其是cp的变化导致。