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11.
Tereza C. R. dos Santos Ricardo Q. Aucélio Reinaldo C. Campos 《Mikrochimica acta》2003,142(1-2):63-66
A simple and direct spectrofluorimetric method has been developed for the determination of aluminum using alizarin red PS
(1,2,4-trihydroxy 9,10-anthraquinone-3-sulfonic acid). The method is based on the strong fluorescence (480/564 nm) of Al3+ and alizarin red. Experimental parameters such as pH, concentration of the ligand, ionic strength of the solution, reaction
time and temperature were optimized in order to maximize the analytical signal. Interferences of several ions (anions and
cations) were studied and evaluated. The linear range of the method extends from 3 to 100 μg L−1. Limit of detection (3sb) was 0.9 μg L−1. The method was tested with a silicate certified reference material. Interferences were eliminated by a liquid extraction
with cupferron.
Author for correspondence. E-mail: aucelior@rdc.puc-rio.br
Received September 10, 2002; accepted January 15, 2003
Published online May 5, 2003 相似文献
12.
对于超细长弹性杆静力学的Kirchhoff方程,用动力学的概念和方法研究其常值特解 和稳定性问题.计算了Kirchhoff方程相对固定坐标系、截面主轴坐标系以及中心线Frenet 坐标系的常值特解,进行了Kirchhoff动力学比拟,用一次近似理论分别讨论了它们的Lyapu nov稳定性,导出了若干稳定性判据,并在参数平面上绘出了稳定域.
关键词:
超细长弹性杆
Kirchhoff方程
常值特解
Lyapunov稳定性 相似文献
13.
从生物样品中检测未知物,一直以来是毒物分析中的一个难点。如何有效地提取目标化合物,并选择适合的检测手段将未知物筛选出来,GC-MS方法是快速筛选多种毒物和药物的一个简便、可靠的手段。随着MS技术的不断发展,更灵敏、更准确的特性将使其成为药物和毒物分析中必不可少的一门技术。 相似文献
14.
A model of two interacting (chemically different) linear polymer chains is solved exactly using the real-space renormalization
group transformation on a family of Sierpinski gasket type fractals and on a truncated 4-simplex lattice. The members of the
family of the Sierpinski gasket-type fractals are characterized by an integer scale factorb which runs from 2 to ∞. The Hausdorff dimensiond
F of these fractals tends to 2 from below asb → ∞. We calculate the contact exponenty for the transition from the State of segregation to a State in which the two chains are entangled forb = 2-5. Using arguments based on the finite-size scaling theory, we show that forb→∞, y = 2 - v(b) d
F, wherev is the end-toend distance exponent of a chain. For a truncated 4-simplex lattice it is shown that the system of two chains
either remains in a State in which these chains are intermingled in such a way that they cannot be told apart, in the sense
that the chemical difference between the polymer chains completely drop out of the thermodynamics of the system, or in a State
in which they are either zipped or entangled. We show the region of existence of these different phases separated by tricritical
lines. The value of the contact exponenty is calculated at the tricritical points. 相似文献
15.
A. Debussche 《Journal de Mathématiques Pures et Appliquées》1998,77(10):967-988
The notion of random attractor for a dissipative stochastic dynamical system has recently been introduced. It generalizes the concept of global attractor in the deterministic theory. It has been shown that many stochastic dynamical systems associated to a dissipative partial differential equation perturbed by noise do possess a random attractor. In this paper, we prove that, as in the case of the deterministic attractor, the Hausdorff dimension of the random attractor can be estimated by using global Lyapunov exponents. The result is obtained under very natural assumptions. As an application, we consider a stochastic reaction-diffusion equation and show that its random attractor has finite Hausdorff dimension. 相似文献
16.
具有避难所的非自治竞争系统的持续生存和全局稳定性 总被引:2,自引:0,他引:2
考虑一个四缀块模型,其中一缀块里有三个竞争种群,另外三个分别是它们的避难所,并且种群能在竞争缀块和各自的避难所间相互扩散.在一定的条件下,我们给出了此模型的持续生存,周期性和全局稳定性. 相似文献
17.
Understanding of the basic nature of arc root fluctuation is still one of the unsolved problems in thermal arc plasma physics.
It has direct impact on myriads of thermal plasma applications being implemented at present. Recently, chaotic nature of arc
root behavior has been reported through the analysis of voltages, acoustic and optical signals which are generated from a
hollow copper electrode arc plasma torch. In this paper we present details of computations involved in the estimation process
of various dynamic properties and show how they reflect chaotic behavior of arc root in the system. 相似文献
18.
本文介绍事后分层技术,说明了它不仅可用于简单随机抽样,而且可以用于放回PPS抽样。给出了事后分层估计量的形式,证明了它的无编性,并给出了它在交通运输抽样调查中的应用。 相似文献
19.
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