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排序方式: 共有1716条查询结果,搜索用时 17 毫秒
21.
Carolina A. Pinto P. M. Büchler J. Dweck 《Journal of Thermal Analysis and Calorimetry》2007,87(3):715-720
The catalyst
used in fluidized catalytic cracking (FCC) units of refineries after several
recovery cycles in regeneration units, reduces its activity and it is partially
substituted by new catalyst in the process. As it has a high silicon and aluminum
oxides content, the pozzolanic properties of a Brazilian FCC spent residual
catalyst, used in different substitution degrees to cement, were evaluated
by three thermal analysis techniques during the early stages of hydration
of a type II Portland cement. NCDTA curves show in real time that the residual
catalyst, accelerates the stages of cement hydration. TG and DSC curves of
respective pastes after 24 h of hydration evidence the pozzolanic activity
of the waste, respectively, by the lower water mass loss during the dehydroxylation
of the residual calcium hydroxide and by the lower dehydroxylation endothermal
effect. Within the analyzed period, the higher is the cement substitution
degree, the higher is the pozzolanic activity of the residual catalyst. 相似文献
22.
Residual stresses are found in the majority of multilayer thin film structures used in modem technology. The measurement and modeling of such stress fields and the elucidation of their effects on structural reliability and device operation have been a “growth area” in the literature, with contributions from authors in various scientific and engineering disciplines.
In this article the measurement of the residual stresses in thin film structures with X-ray diffraction techniques is reviewed and the interpretation of such data and their relationship to mechanical reliability concerns are discussed. 相似文献
23.
The expression of the continuous distribution function F(x) is obtained whenever % MathType!MTEF!2!1!+-% feaafeart1ev1aaatCvAUfeBSjuyZL2yd9gzLbvyNv2CaerbuLwBLn% hiov2DGi1BTfMBaeXafv3ySLgzGmvETj2BSbqefm0B1jxALjhiov2D% aebbfv3ySLgzGueE0jxyaibaiGc9yrFr0xXdbba91rFfpec8Eeeu0x% Xdbba9frFj0-OqFfea0dXdd9vqaq-JfrVkFHe9pgea0dXdar-Jb9hs% 0dXdbPYxe9vr0-vr0-vqpWqaaeaabiGaciaacaqabeaadaqaaqGaaO% qaaerbhv2BYDwAHbacfiGaa8xBaiaabIcacaWG4bGaaiilaiaadMha% caqGPaGaa8hiaiaab2dacaWFGaGaa8xraiaa-HcacaWFybGaa8hiai% aa-XhacaWFGaGaa8hEaiaa-bcacqGHKjYOcaWFGaGaa8hwaiaa-bca% cqGHKjYOcaWFGaGaa8xEaiaa-Lcaaaa!53EE!\[m{\rm{(}}x,y{\rm{)}} {\rm{ = }} E(X | x \le X \le y)\]is known. Moreover, we obtain the necessary and sufficient conditions so that any function m: 2 is the conditional expectation % MathType!MTEF!2!1!+-% feaafeart1ev1aaatCvAUfeBSjuyZL2yd9gzLbvyNv2CaerbuLwBLn% hiov2DGi1BTfMBaeXafv3ySLgzGmvETj2BSbqefm0B1jxALjhiov2D% aebbfv3ySLgzGueE0jxyaibaiGc9yrFr0xXdbba91rFfpec8Eeeu0x% Xdbba9frFj0-OqFfea0dXdd9vqaq-JfrVkFHe9pgea0dXdar-Jb9hs% 0dXdbPYxe9vr0-vr0-vqpWqaaeaabiGaciaacaqabeaadaqaaqGaaO% qaaiaadweacaGGOaGaamiwaerbhv2BYDwAHbacfiGaa8hiaiaacYha% caWFGaGaa8hEaiaa-bcacqGHKjYOcaWFGaGaa8hwaiaa-bcacqGHKj% YOcaWFGaGaa8xEaiaacMcaaaa!4D0D!\[E(X | x \le X \le y)\]of a random variable X with continuous distribution function. Furthermore, we relate m(x,y) to order statistics. 相似文献
24.
氯化聚乙烯弹性体的固相法合成 总被引:2,自引:0,他引:2
讨论了以固相法合成氯化聚乙烯(CPE)弹性体的过程.实验结果表明,以固相氯化反应所得的CPE,其大分子链上Cl取代基的分布比水相悬浮法更均匀.氯化过程的温度直接影响氯化速度及分子结构,如残留结晶、氯分布等.而聚乙烯颗粒表面与内部的氯化程度取决于氯化速度.大分子链上Cl取代基对邻近基团的氯化起阻碍作用 相似文献
25.
Yan J Kline AD Mo H Shapiro MJ Zartler ER 《Magnetic resonance in chemistry : MRC》2004,42(11):962-967
A novel methodology using the order matrix calculation to determine the absolute sign of spin-spin couplings based on the structure of organic compounds is presented. The sign of the residual dipolar coupling (RDC) depends on the sign of corresponding scalar spin-spin coupling constant and the sign of the RDC has a dramatic influence on the order matrix calculation. Therefore, the sign of the spin-spin coupling constant can be obtained by an order matrix calculation through the corresponding RDC. Six types of spin-spin coupling constants, including 2J(H,H), 1J(C,F), 2J(C,F), 3J(C,F), 2J(F,H) and 3J(F,H), were obtained simultaneously. Except for 3J(C,F) where the measured RDCs have very small magnitudes, the signs were determined unambiguously. 相似文献
26.
27.
JIA HongSheng JIA XiaoPeng XU Yue WAN LianRu JIE KaiKai & MA HongAn State Key Laboratory of Superhard Materials Jilin University Changchun China Test Science Experiment Center Changchun 《中国科学:物理学 力学 天文学(英文版)》2011,(1)
Polycrystalline diamond compacts (PDC) were synthesized using diamond powder of average crystal size 3-20 μm by the Ni 70 Mn 25 Co 5 alloy infiltration technique at high temperature and high pressure (HPHT).The surface residual stress of polycrystalline diamond (PCD) layer was measured using micro-Raman spectroscopy with hydrostatic stress model and X-ray diffraction (XRD).Measurements of the stress levels of PCDs show that the residual compressive stresses range from 0.12 to 0.22 GPa,which increase with th... 相似文献
28.
Anna Doppler Leo D.M. Nicholls Christopher Golz Manuel Alcarazo Michael John 《Magnetic resonance in chemistry : MRC》2019,57(11):961-967
Two functionalized [6]carbohelicenes, one of which was also available in its two enantiomeric pure forms, were oriented in stretched polystyrene in CDCl3, and in a recently introduced chiral thermoresponsive lyotropic polyaspartate (poly(benzyl)0.5(phenethyl)0.5-L-aspartate) in C2D2Cl4. From the resulting 1H,13C residual dipolar couplings, the helical pitch of a methylated [6]carbohelicene was determined and found to be in agreement with theoretical predictions and existing crystal structures (d(C2,C2′) ≈ 4.3 Å). For a second [6]carbohelicene with para-methoxyphenyl substituents, a clear conformational preference of the substituents was observed. The orientational properties of the two helicene enantiomers in the chiral polyaspartate are very similar, but both drastically change around 306 K. We suggest this behavior is due to an unusual phase transition in the liquid crystal. 相似文献
29.
Fernanda D. de Melo Hernández César A. Hernández Melo Horacio Tapia-Recillas 《代数通讯》2020,48(9):4013-4026
AbstractIn the present work, a procedure for determining idempotents of a commutative ring having a sequence of ideals with certain properties is presented. As an application of this procedure, idempotent elements of various commutative rings are determined. Several examples are included illustrating the main results. 相似文献
30.
Both residual Cesàro alpha-integrability (RCI( α)) and strongly residual Cesàro alpha-integrability (SRCI(α)) are two special kinds of extensions to uniform integrability, and both asymp-totically almost negative association (AANA) and asymptotically quadrant sub-independence (AQSI) are two special kinds of dependence structures. By relating the RCI(α) property as well as the SRCI(α) property with dependence condition AANA or AQSI, we formulate some tail-integrability conditions under which for appropriate α the RCI(α) property yields L1-convergence results and the SRCI(α) property yields strong laws of large numbers, which is the continuation of the corresponding literature. 相似文献