气基磁化焙烧回收包头稀土尾矿中铁的研究

试验采用磁化焙烧-磁选的方法来回收包头稀土尾矿中的Fe。考察了还原球团的粒径、焙烧温度、还原气体的成分、还原气气体流量、焙烧时间对于磁化焙烧回收Fe的影响。在焙烧温度为580℃,CO与CO2的浓度比为40∶60,还原气体气流量为1.2 L·min-1,焙烧时间为60 min的条件下对球团进行磁化焙烧,并将焙烧后的球团进行磨矿,使得-200目的物料占物料总重量的95%。将磨矿后的物料置于磁场强度为233 k A·m-1的磁选管中进行磁选,可以得到品位为60%左右的铁精矿,其铁回收率达到70%左右。     

On the relation between formal grade and depth with a view toward vanishing of Lyubeznik numbers

Let (R,𝔪) be a local ring and I an ideal. The aim of the present paper is twofold. At first we continue the investigation to compare fgrade(I,R) with depth R∕I and further we derive some results on the vanishing of Lyubeznik numbers.     

A note on flow and heat transfer of a viscoelastic fluid over a stretching sheet

This paper presents a study of the flow and heat transfer of an incompressible homogeneous second grade fluid past a stretching sheet. The governing partial differential equations are converted into ordinary differential equations by a similarity transformation. The effects of viscous dissipation and work due to deformation are considered in the energy equation and the variations of dimensionless surface temperature and dimensionless surface temperature gradient with various parameters are graphed and tabulated. Two cases are studied, namely, (i) the sheet with constant surface temperature (CST case) and (ii) the sheet with prescribed surface temperature (PST case).     

Stationary problem of third-grade fluids in two and three dimensions: existence and uniqueness

This paper is devoted to the stationary problem of third-grade fluids in two and three dimensions. In two dimensions, we show existence of solutions and uniqueness, for a boundary of class C^2,1 and small data, by generalizing the method used by J.M. Bernard for the stationary problem of second-grade fluids (we deal with a polynomial of four degrees instead of two degrees). Contrary to the case of two dimensions, the resolution of the problem of third-grade fluids in three dimensions requires the physical condition |α₁+α₂|<(24νβ)^1/2. From this condition, we derive two “pseudo ellipticities” for the operator ν|A(u)|²+(α₁+α₂)tr(A(u)³)+β|A(u)|⁴, where A(u) is a 3-order symmetric matrix such that tr(A(u))=0. Thus, with, in addition, a sharp estimate of the scalar product (|A(u)|²A(u)-|A(v)|²A(v),A(u)-A(v)), we are able to prove existence of solutions and uniqueness, for a boundary of class C^2,1 and small data, in three dimensions.

Résumé

Cet article est consacré au problème stationnaire des fluides de grade trois en dimension deux et trois. En dimension deux, nous montrons l’existence de solutions et l’unicité, pour une frontière de classe C^2,1 et une donnée petite, en généralisant la méthode utilisée par J.M. Bernard pour le problème stationnaire des fluides de grade deux (nous avons affaire à un polynôme de degré quatre au lieu de deux). Contrairement au cas de la dimension deux, la résolution du problème des fluides de grade trois en dimension trois requière la condition physique |α₁+α₂|<(24νβ)^1/2. De cette condition, nous déduisons deux “pseudo matrice” pour l’opérateur ν|A(u)|²+(α₁+α₂)tr(A(u)³)+β|A(u)|⁴, où A(u) est une matice symétrique d’ordre 3 à trace nulle. De là, avec, en plus, une fine estimation du produit scalaire (|A(u)|²A(u)-|A(v)|²A(v),A(u)-A(v)), nous sommes capables de prouver l’existence de solutions et l’unicité, pour une frontière de classe C^2,1 et une donnée petite, en dimension trois.     

Domino Pd-catalyzed Heck cyclization and bismuth-catalyzed hydroamination: formal synthesis of elacomine and isoelacomine

The formal synthesis of hemiterpene spirooxindole alkaloids elacomine (1) and isoelacomine (2) is described. Heck reaction of protected iodoanilines with 5,6-dihydro-2H-pyran-2-one or six-membered unsaturated lactams was investigated. The coupling product was readily converted to a carbamoyl chloride with an incorporated diene unit. The spiro(pyrrolidine-3,3'-oxindole) skeleton, which corresponds to the carbon skeleton of 1 and 2, was efficiently constructed from this intermediate by using a domino palladium-catalyzed Heck reaction and bismuth-catalyzed hydroamination. An isolated byproduct of the reaction could also be converted to the spirooxindole skeleton.     

Application of lag-k autocorrelation coefficient and the TGA signals approach to detecting and quantifying adulterations of extra virgin olive oil with inferior edible oils

The combination of lag-k autocorrelation coefficients (LCCs) and thermogravimetric analyzer (TGA) equipment is defined here as a tool to detect and quantify adulterations of extra virgin olive oil (EVOO) with refined olive (ROO), refined olive pomace (ROPO), sunflower (SO) or corn (CO) oils, when the adulterating agents concentration are less than 14%. The LCC is calculated from TGA scans of adulterated EVOO samples. Then, the standardized skewness of this coefficient has been applied to classify pure and adulterated samples of EVOO. In addition, this chaotic parameter has also been used to quantify the concentration of adulterant agents, by using successful linear correlation of LCCs and ROO, ROPO, SO or CO in 462 EVOO adulterated samples. In the case of detection, more than 82% of adulterated samples have been correctly classified. In the case of quantification of adulterant concentration, by an external validation process, the LCC/TGA approach estimates the adulterant agents concentration with a mean correlation coefficient (estimated versus real adulterant agent concentration) greater than 0.90 and a mean square error less than 4.9%.     

Flow due to non-coaxial rotation of a porous disk and a second grade fluid rotating at infinity

An exact solution for the three-dimensional flow due to non-coaxial rotation of a porous disk and a second grade fluid at infinity is obtained. It is shown that for uniform suction or uniform blowing at the disk, an asymptotic profile exists for the velocity distribution. The velocity depends on two parameters: one of them is the suction parameter or blowing parameter and the other is the visco-elastic parameter. Furthermore, it is found that when the value of the visco-elastic parameter is fixed, the velocity decreases with an increase in the value of the suction parameter and when the value of the suction parameter is fixed, the velocity increases with an increase in the value of the visco-elastic parameter.     

Exact analytical solutions for axial flow of a fractional second grade fluid between two coaxial cylinders

The velocity field and the adequate shear stress corresponding to the longitudinal flow of a fractional second grade fluid, between two infinite coaxial circular cylinders, are determined by applying the Laplace and finite Hankel transforms. Initially the fluid is at rest, and at time t = 0⁺, the inner cylinder suddenly begins to translate along the common axis with constant acceleration. The solutions that have been obtained are presented in terms of generalized G functions. Moreover, these solutions satisfy both the governing differential equations and all imposed initial and boundary conditions. The corresponding solutions for ordinary second grade and Newtonian fluids are obtained as limiting cases of the general solutions. Finally, some characteristics of the motion, as well as the influences of the material and fractional parameters on the fluid motion and a comparison between models, are underlined by graphical illustrations.     

Nonsingular systems of generalized Sylvester equations: An algorithmic approach

We consider the uniqueness of solution (i.e., nonsingularity) of systems of r generalized Sylvester and ?‐Sylvester equations with n×n coefficients. After several reductions, we show that it is sufficient to analyze periodic systems having, at most, one generalized ?‐Sylvester equation. We provide characterizations for the nonsingularity in terms of spectral properties of either matrix pencils or formal matrix products, both constructed from the coefficients of the system. The proposed approach uses the periodic Schur decomposition and leads to a backward stable O(n³r) algorithm for computing the (unique) solution.