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991.
合并带流动注射分光光度法研究硫羟乳酸掩蔽性能 总被引:1,自引:1,他引:1
本文运用合并带流动注射分析技术,建立了以Yb^3+XO显色体系为参考体系研究硫羟乳酸掩蔽性能的方法,在pH5.6硫羟乳酸能掩蔽Sn^4+,Bi^3+,Tl^3+,Hg^2+,Cu^2+,Cr^3+和Cd^2+测定Yb^3+的线性范围为1.36×10^-6~2.72×10^-5mol/L,采样频率可达120次/h。 相似文献
992.
反向流动注射化学发光法测定痕量铁 总被引:10,自引:1,他引:10
基于邻菲别名林对高碘酸钾-碱性鲁米诺-铁体系发光强度的增敏作用建立了水体中总铁的反向流动性化学发光检测方法。该法线性范围在1×10^-4-10mg/L,检测限为3×10^-6mg/L,对于5×10^-3mg/L Fe测定9次的相对标准偏差为0.9%。此方法已用在水处理中总铁的监测。 相似文献
993.
流动注射化学发光传感器测定抗坏血酸 总被引:9,自引:0,他引:9
基于抗坏血酸抑制KMnO4-鲁米诺体系化光反应这一效应,设计出一种简便,快速,灵敏度高的消耗型化学发光抗坏血酸传感器。该传感器线性响应范围为1.0*10^-5-4.0*10^-3g/L;相对标准偏差为2.3%(1.0*10^-4g/L,n=11); 相似文献
994.
995.
Ganesh P. Sanganwar Ram B. Gupta Alexandre Ermoline James V. Scicolone Rajesh N. Dave 《Journal of nanoparticle research》2009,11(2):405-419
Due to the increased use of nanocomposites, mixing at nanoscale has become important. Current mixing techniques can be classified
into: (a) dry mixing (mechanical mixing), (b) wet mixing, and (c) simultaneous production of mixed nanoparticles (when possible).
Dry mixing is in general not effective in achieving desired mixing at nanoscale, whereas wet mixing suffers from different
disadvantages like nanomaterial of interest should be insoluble, has to wet the liquid, and involves additional steps of filtration
and drying. This paper examines the use of pressurized carbon dioxide having high density and low viscosity to replace the
liquids (e.g., n-hexane, toluene). Ultrasound is applied to the suspension of nanopowders in gaseous and supercritical carbon dioxide where
high impact collisions during sonication help mixing and the final mixture is obtained by simple depressurization. The method
is tested for binary mixture of alumina/silica, silica/titania, MWNT (multiwalled carbon nanotubes)/silica, and MWNT/titania.
The effects of sonication intensity and pressure on the degree of mixing are studied. Comparative study is also done with
liquid n-hexane as a mixing media. Quantitative characterization (e.g., mean composition standard deviation, intensity of segregation)
of mixing of alumina/silica and silica/titania is done with energy-dispersive X-ray spectroscopy, and that of MWNT/silica
and MWNT/titania is done using field-emission scanning electron microscopy and day-light illumination spectrophotometry. Results
show that mixing in carbon dioxide at higher ultrasound amplitudes is as good as in liquid n-hexane, and the final mixed product does not contain any residual media as in the case of liquid n-hexane. 相似文献
996.
Guillaume Jouvet Matthias Huss Heinz Blatter Marco Picasso Jacques Rappaz 《Journal of computational physics》2009,228(17):6426-6439
Due to climatic change, many Alpine glaciers have significantly retreated during the last century. In this study we perform the numerical simulation of the temporal and spatial change of Rhonegletscher, Swiss Alps, from 1874 to 2007, and from 2007 to 2100. 相似文献
997.
Denys Dutykh 《Physics letters. A》2009,373(36):3212-3216
Water wave propagation can be attenuated by various physical mechanisms. One of the main sources of wave energy dissipation lies in boundary layers. The present work is entirely devoted to thorough analysis of the dispersion relation of the novel visco-potential formulation. Namely, in this study we relax all assumptions of the weak dependence of the wave frequency on time. As a result, we have to deal with complex integro-differential equations that describe transient behaviour of the phase and group velocities. Using numerical computations, we show several snapshots of these important quantities at different times as functions of the wave number. Good qualitative agreement with previous study [D. Dutykh, Eur. J. Mech. B/Fluids 28 (2009) 430] is obtained. Thus, we validate in some sense approximations made anteriorly. There is an unexpected conclusion of this study. According to our computations, the bottom boundary layer creates disintegrating modes in the group velocity. In the same time, the imaginary part of the phase velocity remains negative for all times. This result can be interpreted as a new kind of instability which is induced by the bottom boundary layer effect. 相似文献
998.
Ramadan M. Ali 《International Journal of Theoretical Physics》2009,48(5):1454-1458
A regular static interior solution of Einstein’s field equations representing a perfect fluid cylinder of finite radius is
presented. The solution is matched to the Levi-Civita vacuum solution at a boundary where the pressure vanishes. The density
and pressure are finite and positive inside the cylinder for a specific range of the mass parameter. The solution could thus
represent a reasonable source for the Levi-Civita metric. 相似文献
999.
V. Lepiller A. Goharzadeh A. Prigent I. Mutabazi 《The European Physical Journal B - Condensed Matter and Complex Systems》2008,61(4):445-455
We have investigated the influence of a weak radial
temperature gradient in a wide gap and large aspect ratio
Couette-Taylor system. The inner cylinder is rotating and can be
heated or cooled, the outer cylinder is at rest and immersed in a
large thermal bath. We found that a radial temperature gradient
destabilizes the Couette flow leading to a pattern of traveling
helicoidal vortices occurring only near the bottom of the system.
The size of the pattern increases as the rotation frequency of the cylinder is increased. We
have characterized the spatiotemporal properties of the pattern and we have shown that it
behaves as a wall mode found in the simulation of the
complex Ginzburg-Landau equation with homogeneous boundary
conditions. 相似文献
1000.
Yu. Ya. Trifonov 《Journal of Engineering Thermophysics》2008,17(1):30-52
This paper is devoted to a theoretical analysis of nonlinear two-dimensional waves using the Navier-Stokes equations in their
full statement. Steady-state travelling wave regimes have been found and an analysis of their linear stability has been carried
out. It is shown that the flow regimes obtained using the Navier-Stokes equations are qualitatively different from the solutions
of Shkadov’s integral approach starting from some values of the Kapitza number. It is also found that the wave regimes of
the Navier-Stokes equations have an internal vortex at moderate Reynolds numbers. The results obtained using “the regularized
integral model” are in excellent agreement with the Navier-Stokes calculations for Re/Ka ≤2. Unlike the solutions found using an integral approach, it is shown that only a few types of nonlinear waves exist when
the full Navier-Stokes equations are considered.
The text was submitted by the author in English. 相似文献