Influence of Mn ions concentration on optical and magnetic properties of Mn-doped ZnS nanowires

The optical and magnetic properties of ZnS:Mn²⁺ nanowires are tuned by Mn²⁺ concentration. The magnetic variation is ascribed to the competition between antiferromagnetic and ferromagnetic exchange interactions.

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溶胶-凝胶VO2薄膜转换特性研究

利用溶胶凝胶法在SiO2Si衬底上沉积高取向的V2O5薄膜,在压强低于2Pa,温度高于400℃的条件下,对V2O5薄膜进行真空烘烤,获得了电阻率变化3个数量级以上、弛豫宽度为62℃的VO2多晶薄膜.以X射线衍射(XRD)、扫描电子显微镜(SEM)图和电阻率转换特性等实验结果为依据,详细分析了溶胶凝胶薄膜在真空烘烤时从V2O5向VO2的转化,它经历了从VnO2n+1(n=2,3,4,6)到VO2的过程.实验证明,根据选择合适的成膜热处理条件和真空烘烤条件是实现溶胶凝胶V2O5结构向VO2结构成功转换的关键 关键词： 溶胶-凝胶法 氧化钒薄膜 VO2膜转换特性     

The studies of high-temperature and short-time annealing,phase transition process,and magnetic property for LaFe11.7Si1.3 compound

The high-temperature phase transition is analyzed according to the DSC of as-cast LaFe_11.7 Si_1.3 compound and the X-ray patterns of LaFe_11.7Si_1.3 compounds prepared by high-temperature and short-time annealing. Large amount of 1:13 phase begins to appear in LaFe_11.7Si_1.3 compound annealed near the melting point of LaFeSi phase (about 1422?K). When the annealing temperature is close to the temperature of peritectic reaction (about 1497?K), the speed of 1:13 phase formation is the fastest. The phase relation and microstructure of the LaFe_11.7Si_1.3 compounds annealed at 1523?K (5?h), 1373?K (2?h)?+?1523?K (5?h), and 1523?K (7?h) +1373?K (2?h) show that longer time annealing near peritectic reaction is helpful to decrease the impurity phases. For studying the influence of different high-temperature and short-time annealing on magnetic property, the Curie temperature, thermal, and magnetic hystereses, and the magnetocaloric effect of LaFe_11.7Si_1.3 compound annealed at three different temperatures are also investigated. Three compounds all keep the first order of magnetic transition behavior. The maximal magnetic entropy change ΔS_M (T, H) of the samples is 12.9, 16.04, and 23.8?J?kg^?1?K^?1 under a magnetic field of 0–2?T, respectively.     

简单有效的运动汽车投影阴影分割算法

在实时的车型识别系统中,由于光照的影响,需要一种简单快速有效的方法将汽车车体与其阴影分割开。利用阴影的光谱属性,同时根据阴影的几何特征及阴影区域内的点和汽车的空间位置、形状等相关特点,提出一种基于小波变换多分辨率特性的阴影分割算法,该算法能有效地分割出阴影与目标之间的分界线。先利用阴影的光谱属性对阴影进行粗分割,然后利用小波变换的多尺度性对候选阴影点进行特征提取,从而获取最后的阴影分界线。该方法不需要事先确定光源的方向、车体的彩色信息和背景纹理信息,能有效地分割任何颜色、任何背景纹理下、任何光源方向下的运动汽车投影阴影。实验表明,该方法定位准确,处理速度快,抗噪能力强,为进一步的车型识别提供基础。     

Correlation of soft magnetic properties with free volume and medium range ordering in metallic glasses probed by fluctuation microscopy and positron annihilation technique

Amorphous ribbons of different thicknesses of Co_64.5Fe_3.5Si₁₆B₁₄Ni₂ alloy were synthesized using the melt spinning technique by varying wheel speed. The effect of cooling rate on the ribbon thickness and their soft magnetic properties have been studied. The amorphous structure has been characterized in terms of structural free volume and medium range order (MRO) by positron annihilation spectroscopy and fluctuation electron microscopy techniques. Positron lifetime spectra of amorphous samples showed two lifetime components. The first component was found to be correlated with MRO whereas, the second lifetime component was found to be associated with nanovoid type of defects, and the second component was strongly dependent on processing conditions. It could be established that the coercivity of the amorphous samples produced by the rapid solidification technique mainly depends on the defects formed during processing rather than change induced in MRO.     

短波长相变光盘记录介质Ge2Sb2Te5薄膜的制备及静态性能研究

研究了６３２．８ｎｍ波长下适用的相变光盘介质Ｇｅ２Ｓｂ２Ｔｅ５薄膜的制备方法和静态光存诸记录特性，发现该薄膜可在１００ｎｓ条件下实现直接重写，在优化膜层结构后，写擦循环次数高达１０＾６，反射率对比度在１５％以上。     

双带频率选择表面设计

为了实现频率选择表面(FSS)的双带特性,设计了由矩形栅格和三圆环组合单元FSS。对FSS的谱域求解方法进行了详细的描述。采用谱域法分析了不同角度和极化入射波下FSS的频率响应性能。结果表明,所设计的FSS对于不同入射角度和极化电磁波具有稳定的双带、平顶传输及陡峭下降边缘特性。双带特性大致表现为1.8～5.4GHz的阻带和5.4～20.0GHz的通带。阻带谐振频率稳定在3.1GHz左右,而通带在-4dB的平顶传输带宽达14.3GHz以上。其陡峭下降边缘特性表现为S波段信号强烈反射,而其他波段信号通过,从而实现多波段通讯。该结构FSS可应用于卫星通信、雷达罩及其他相关领域。     

CYCIAE型回旋加速器负离子剥离引出的光学行为研究

为了CYCIAE型回旋加速器的剥离靶轴线及旋转角的概念设计,必须对负离子剥离后的光学特性进行研究,基于根据CYCIAE型回旋加速器剥离引出特点编制的程序CYCRS,计算了CYCIAE30加速器不同能量束流引出剥离点的位置,并与实际位置进行比较,证明计算所用的理论及方法是正确的,同时,考察了剥离后的束流空间运动的光学特性.在此基础上,确定了CYCIAE70回旋加速器能量为35—70MeV的束流引出剥离点位置.     

双参数变形玻色湮没算符高次幂的本征态及其量子统计性质

本文构造了双参数变形玻色湮没算符高次幂a^'k(k≥3)的k个正交归一木征态的数学结构,发现它们能构成一个完备的Hilbert空间,并且讨论了它们的量子统计性质.     

磁场辅助激光熔覆制备Ni60CuMoW复合涂层

采用磁场辅助激光熔覆技术,在Q235钢表面制备了Ni60CuMoW复合涂层,借助SEM,EDS 和XRD 等表征手段对涂层进行了微观组织和物相分析,利用维氏硬度计测试了复合涂层截面的显微硬度分布,通过摩擦磨损实验和电化学测试系统研究了复合涂层的磨损性能和耐腐蚀性能。研究结果表明：涂层主要由-Ni,Cu）固溶体、硅化物和硼化物组成,Cr3Si晶粒细化且均匀致密;磁场辅助作用下,激光熔覆涂层平均显微硬度达到913HV0.5,为无磁场辅助涂层的1.5 倍,磨损失重仅为无磁场涂层的36%,自腐蚀电位上升了100 mV,腐蚀电流密度降低了70%,耐磨耐蚀性能得到了显著改善。