BEPC Ⅱ注入器相控系统的设计

以2.856GHz频率上相位控制达到±2°为目标,阐述北京正负电子对撞机重大改造工程注入器相控系统设计思路,提出相应的系统实现结构。在分析相控过程的基础上,分解系统指标,把它作为相控系统详细设计和关键部件测试的依据。最后,针对相位测量这一关键问题,给出了具体的实现方法。     

HIRFL注入器高频腔体与高频机的匹配

叙述了兰州重离子加速器注入器(SFC)高频系统的200 kW高频机与高频腔体的功率匹配,匹配测量系统的工作原理,以及对匹配系统的改进和完善,并对高频腔体的输入阻抗和耦合电容进行了计算。为提高高频系统的稳定性和可靠性,对影响高频功率传输和D电压提高的问题进行了深入的研究和改进。采用矢量阻抗仪冷态测量腔体匹配阻抗的方法和一些相应的技术和措施,用矢量电压表动态测量功率输出级的相位差,判断D电路是否工作在匹配状态,从而使SFC的D电压由原来的50~65 kV（不稳定）提高到稳定工作的105 kV,改善了SFC的工作状态和保证了SFC的高效运行。     

GC-14A气相色谱仪分流装置的故障排除

 介绍了日本岛津公司产GC-14A气相色谱仪中SPL- 14分流/不分流进样器的连接管引起的故障现象及排除方法。指出该公司产同类型带有分流/ 不分流装置的气相色谱仪,若长期分析高沸点油状化合物,则应定期清洗连接管,及时清除 堵塞物,以保证测试数据有较好的重现性。     

Application of a thermal desorption cold trap injector to multidimensional GC and GC-MS

The Thermal desorption Cold Trap injector (TCT) was used as a part of modified multidimensional GC (MDGC) or MDGC mass spectroscopy (MS) systems. These systems were based on a preparative GC (GC1), an analytical GC (GC2), or GC-MS and the TCT. The TCT was mounted on the GC2 or GC-MS. Analysis was carried out as follows: first, the volatile compounds heart-cut after separation on the GC1 column were adsorbed onto the Porapak Q column out of the GC1 oven. This Porapak Q column was then coupled to the TCT, and the volatile compounds adsorbed on the Porapak Q were thermally desorbed, cold trapped, and injected onto an analytical column in the GC2 or GC-MS. Repeatability of the retention time (RT) and area % of model samples consisting of citronellol, decanol, and geranyl acetate was examined. Also, the volatile compounds present at very low concentrations in ethanol solution were concentrated on the Porapak Q column. These were injected onto the analytical column by the same method as described above, and the repeatability of the RT and area % on the chromatogram was examined. In the two experiments, the standard deviation of the RT and area % for each compound was about 0.02 and less than 2.85, respectively. A commercial geranium oil was successfully analyzed by this technique. The results indicate that this modified MDGC and MDGC-MS system are very useful for detection and determination of compounds in complex mixtures.     

The main injector particle production experiment at Fermilab

We describe the physics capabilities and status of the MIPP experiment which concluded its physics data taking run in March 2006. We show some preliminary results from this run and describe plans to upgrade the spectrometer.     

毛细管气相色谱分流进样技术研究

研究出一种改进的毛细管分流进样器，设计了一种新型螺旋进样内衬管。使分流进样的重复精度有显著提高，沸点歧视效应减小，色谱峰尾尖锐，使毛细管色谱柱的高分离效能得以充分发挥。对４种常用的进样内衬进行了考察，得到了有重要实用意义的结果，并从理论上解释了与传统观点相悖的实验现象，深化了对分流进样动态过程的理解。     

Swirl number based transposition of flow-induced mechanical stresses from reduced scale to full-size Francis turbine runners

At part load conditions, Francis turbines are subject to the emergence of a hydrodynamic instability in their draft tube, referred to as precessing vortex rope. It induces pressure pulsations in the water passages at the precession frequency of the vortex, leading to additional vibrations and dynamic loads on the runner blades. The prediction of both the dynamic behaviour of the vortex rope and the resulting dynamic loads over a wide operating range is of importance to improve the runner design and robustness on the one hand and to assess additional fatigue and related maintenance costs on the other hand. Such a prediction, either with numerical simulation or reduced scale physical model tests, remains however challenging. The present paper aims at introducing a methodology to assess the vortex behaviour, the related pressure fluctuations and the resulting dynamic strains on the runner over the complete part load operating range. It is based on reduced scale physical model tests of a Francis turbine, including the measurement of the pressure and the load on the runner with instrumented blades. It is shown that the influence of both the discharge factor and speed factor on the vortex dynamics behaviour and related pressure fluctuations can be represented by a single parameter; the swirl number. The correlation with the swirl number is further extended to the dynamic strains induced by the vortex rope on the runner blades. Similar mechanical load and pressure measurements are finally performed on the full-scale machine during a power ramp-up and the results are compared to the empirical correlations established on the reduced scale physical model.     

Development of a curie-point headspace sampler for capillary gas chromatography

A Curie-point headspace sampler (CPHS) equipped with a purge and trap sampler has been developed for use with capillary gas chromatography. The new system can handle a variety of samples, including gases, liquids, and solids, and can also be used as a pyrolyzer.     

Splitless injection of up to hundreds of microliters of liquid samples in capillary GC: Part 1, concept

If a sample evaporates by flash vaporization in an empty injector insert, the solute material is well mixed with the expanding solvent vapors and the maximum injection volume is determined by the requirement that no vapors must leave the vaporizing chamber. If evaporation occurs from a surface (e.g., of Tenax packing), however, the solvent evaporates first. The site of evaporation is cooled to the solvent's boiling point, and the cool island formed in the hot injector retains solutes of at least intermediate boiling point (visually observed for perylene). Solvent vapors, free from such solutes, may now expand backwards from the injector insert and leave through the septum purge exit. When solvent evaporation is complete, the site of evaporation warms up, causing the high boiling solutes to evaporate and to be carried into the column by the carrier gas. The technique somewhat resembles PTV injection, but is performed using a classical vaporizing injector.