Characterization of bacterial lipid profiles by using rapid sample preparation and fast comprehensive two‐dimensional gas chromatography in combination with mass spectrometry

The bacteria fatty acid profile has been extensively studied for taxonomic classification purposes, since bacteria, in general, contain particular and rare fatty acids, compared with animal and plant tissues. As for any real‐world sample type, the development of rapid and reliable methods for (i) sample identification (in this case, bacterium type), and (ii) constituent identification (in this instance, the fatty acid profile) is desirable. In this research, a half‐an‐hour procedure, to analyze bacteria, was developed: a 2‐min one‐step sample preparation step was followed by a relatively fast comprehensive 2D GC‐MS separation (25 min). Furthermore, dedicated MS libraries were constructed for the identification of bacteria and fatty acids. Finally, data processing, only qualitative at this stage, was carried out with the support of a novel comprehensive 2D GC software.     

A viscosity method with no spectral radius requirements for the split common fixed point problem

This paper is concerned with an algorithmic solution to the split common fixed point problem in Hilbert spaces. Our method can be regarded as a variant of the “viscosity approximation method”. Under very classical assumptions, we establish a strong convergence theorem with regard to involved operators belonging to the wide class of quasi-nonexpansive operators. In contrast with other related processes, our algorithm does not require any estimate of some spectral radius. The technique of analysis developed in this work is new and can be applied to many other fixed point iterations. Numerical experiments are also performed with regard to an inverse heat problem.     

Split Weight Enumerators for the Preparata Codes with Applications to Designs

For quaternary Preparata and Kerdock codes of length N=2 ^m ,m odd, we prove that the split complete weight enumerator for a coordinate partition into 3 and N-3 coordinates is independent of the chosen partition. The result implies that the words of a given complete weight in either a Preparata code or Kerdock code define a 3-design.     

Disjunctive cuts for continuous linear bilevel programming

This work shows how disjunctive cuts can be generated for a bilevel linear programming problem (BLP) with continuous variables. First, a brief summary on disjunctive programming and bilevel programming is presented. Then duality theory is used to reformulate BLP as a disjunctive program and, from there, disjunctive programming results are applied to derive valid cuts. These cuts tighten the domain of the linear relaxation of BLP. An example is given to illustrate this idea, and a discussion follows on how these cuts may be incorporated in an algorithm for solving BLP.     

Automated optimization of split ratio in capillary gas chromatography

An electronic gas-flow controller system called Advanced Flow Control (AFC), which controls not only carrier gas pressure at the column inlet but also the total gas flow including the split flow, was designed and evaluated. BASIC programming of repetitive analyses of standard mixtures under varied split ratios and pressure programs allowed automated optimization of those conditions for the desired column loading and resolution between adjacent peaks.     

Cutting and Surrogate Constraint Analysis for Improved Multidimensional Knapsack Solutions

We use surrogate analysis and constraint pairing in multidimensional knapsack problems to fix some variables to zero and to separate the rest into two groups – those that tend to be zero and those that tend to be one, in an optimal integer solution. Using an initial feasible integer solution, we generate logic cuts based on our analysis before solving the problem with branch and bound. Computational testing, including the set of problems in the OR-library and our own set of difficult problems, shows our approach helps to solve difficult problems in a reasonable amount of time and, in most cases, with a fewer number of nodes in the search tree than leading commercial software.     

Dynamic and Quasi-Static Propagation of Compaction Waves in a Low-Density Epoxy Foam

We conducted dynamic and quasi-static compression experiments with low-density (ρ = 120 kg/m³) epoxy foam specimens. The specimens had a 10.0-mm-square cross-section and a length of 19.3 mm. Dynamic experiments were conducted with a modified split Hopkinson pressure bar (SHPB), and the quasi-static experiments were conducted with a hydraulic load frame device (MTS-810). In both cases, the specimens were loaded from one end at a constant velocity. Equally spaced grid lines were marked on the specimens to monitor the deformation history. Digital images taken at equally spaced time intervals gave the positions of each grid line. These images showed that a constant end-face velocity V produced a compaction wave front that traveled at a constant velocity C in both dynamic and quasi-static experiments. We described these results with a shockwave analysis that used a locking solid material model.     

Testing Aluminum Alloy from Quasi-static to Dynamic Strain-rates with a Modified Split Hopkinson Bar Method

An aluminum alloy¹ was tested at quasi-static to dynamic strain-rates (from 10⁻¹ to 5 10³ s⁻¹), using a single measuring device, a modified Split Hopkinson Bar. A wave separation technique [Bussac et al., J Mech Phys Solids 50:321–350, 2002] based on the maximum likelihood method was applied to process the strain and velocity measurements recorded at various points on each bar. With this method, it is possible to compute the stress, strain, displacement and velocity at any point on the bar. Since the measurement time is unlimited, the maximum strain measured in a given specimen no longer decreases with the strain-rate, as occurs with the classical Split Hopkinson Bar method. ¹The authors wish to thank the automobile manufacturer who provided samples of the alloy used in this study. For reasons of commercial and industrial confidentiality, we were not informed about the composition of this alloy.     

A complete characterization of disjunctive conic cuts for mixed integer second order cone optimization

We study the convex hull of the intersection of a disjunctive set defined by parallel hyperplanes and the feasible set of a mixed integer second order cone optimization (MISOCO) problem. We extend our prior work on disjunctive conic cuts (DCCs), which has thus far been restricted to the case in which the intersection of the hyperplanes and the feasible set is bounded. Using a similar technique, we show that one can extend our previous results to the case in which that intersection is unbounded. We provide a complete characterization in closed form of the conic inequalities required to describe the convex hull when the hyperplanes defining the disjunction are parallel.     

A remark on split least-squares mixed element procedures for pseudo-parabolic equations

In this paper, we introduce two novel split least-squares mixed element procedures for pseudo-parabolic equations. By selecting the least-squares functional properly, each procedure can be split into two independent symmetric positive definite sub-procedures. One of sub-procedures is for the primitive unknown variable u, which is the same as the standard Galerkin finite element procedure and the other is for the introduced flux variable σ. Optimal order error estimates are developed. A numerical example is given to show the efficiency of the introduced schemes.