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151.
The paper shows a computer-assisted procedure for the optimization of selectivity of two columns coupled in series by tuning the working temperature (using the isothermal mode) and columns coupling-point pressure at constant inlet and outlet carrier gas pressures. The optimization procedure validation was tested by the separation of 32 hydrocarbons in a column series with the aim to resolve the maximum number of components in the shortest possible analysis time.Dedicated to Professor J. F. K. Huber on the occasion of his 65th birthday 相似文献
152.
iPP/sPP, iPP/rPP, iPP/PVDF and iPP/PA-6 blends, and their β-nucleated forms were prepared in the present study. The components of iPP/sPP and iPP/rPP blends are compatible in the molten state. The phase structure of the melt of iPP/PVDF and iPP/PA-6 blends is heterogeneous. The melting and crystallisation characteristics as well as the structure and polymorphic composition of these blends were studied by polarised light microscopy (PLM) and differential scanning calorimetry (DSC). When semicrystalline polymers are added to iPP, the most important factor of the formation a blend with β-crystalline phase is the α-nucleation effect of the second polymer. In the case of polymers with an α-nucleating effect, the temperature range of their crystallisation should be lower than that of β-iPP. β-nucleated iPP/PVDF and iPP/PA-6 blends are extreme examples showing that completely β-iPP matrix can not form even in the presence of a highly effective β-nucleant, because of the strong α-nucleating ability and higher crystallisation temperature range of PVDF and PA-6. We found that the β-crystallisation tendency of random propylene copolymers can be enhanced by adding an iPP homopolymer. 相似文献
153.
In spite of Sinai's result that the decay of the velocity autocorrelation function for a random walk on
d
(d=2) can drastically change if local impurities are present, it is shown that local impurities can not abolish weak convergence to the Brownian motion if d2. 相似文献
154.
155.
This paper investigates the rotating flow and heat transfer of a viscous fluid induced by a stretching surface. The nonlinear problem subject to a given skin friction at the boundary is solved. Analytic solution is obtained using homotopy analysis method. The velocity, temperature, and stretching velocity is calculated for different values of the rotation parameter (λ). The obtained results are compared with the well known results of rotating flow induced by a stretching surface by using four sets of boundary conditions. Copyright © 2011 John Wiley & Sons, Ltd. 相似文献
156.
Matthew Thompson Carolyn Carkner Adrian Bailey Nicholas J. Mosey Nadia Kapernaum 《Liquid crystals》2013,40(9):1246-1260
Two sterically equivalent series of phenoxy-terminated 5-alkoxy-2-(4-alkoxyphenyl)pyrimidine liquid crystals were synthesised, and their mesogenic properties were characterised by polarised optical microscopy and differential scanning calorimetry (DSC). The phenoxy end-group causes a significant increase in melting point and inhibits – at least partially – the mesomorphism of these materials relative to the parent isomers; in most cases, the broad enantiotropic SmC phase formed by the parent isomers is suppressed by the addition of the phenoxy end-group. However, detailed analyses by small-angle X-ray scattering and monodomain 2D X-ray scattering suggest that these compounds form a SmA phase with a partially intercalated bilayer structure in which the phenoxy end-groups are nanosegregated. Such an intercalated bilayer structure might enable the tuning of smectogenic properties by appropriate substitution of the phenoxy end-groups. 相似文献
157.
《Stochastics An International Journal of Probability and Stochastic Processes》2013,85(3-4):207-226
In the present paper, a framework for parametric estimation in nonlinear time series is developed. Strong consistency and asymptotic normality of minimum Hellinger distance estimates for a determined class of nonlinear models are investigated. The main Interest for these estimates is motivated by their robustness under perturbations as it has been emphazized in Beran [2]. The first part of the paper is devoted to the study of some probabilistic properties which ensure the existence and the optimal properties of the estimates 相似文献
158.
We consider β-expansions of formal Laurent series over finite fields. If the base β is a Pisot or Salem series, we prove that the β-expansion of a Laurent series α is automatic if and only if α is algebraic. 相似文献
159.
虫害检测算法研究是开展虫害快速、准确监测,制定精准森防检疫措施的重要基础。以毛竹叶片为研究尺度,基于刚竹毒蛾危害下的寄主外部形态与内部生理现象总结,选择并实测叶损量LL、相对叶绿素含量RCC、相对含水量RWC、原始光谱的733.66~898.56 nm值(ρ733.66~898.56)、一阶微分光谱的562.95~585.25 nm值(ρ′562.95~585.25)与706.18~725.41 nm值(ρ′706.18~725.41)等理化参数,随机划分实验组(63组)和验证组(37组)并设计5次重复实验;分别运用Fisher判别分析、BP神经网络、随机森林等三种方法建立刚竹毒蛾危害等级的检测模型,从检测精度、Kappa系数及R2等指标对模型的检测效果予以分析和比较。结果显示,Fisher判别分析、BP神经网络、随机森林的检测精度分别为69.19%,65.41%,83.78%,Kappa系数分别为0.576 9,0.532 4和0.778 8,R2分别为0.722 2,0.582 6和0.870 9,总体而言,三种方法均具备刚竹毒蛾危害的检测能力,随机森林的检测效果最优,Fisher判别分析次之,再次为BP神经网络;从分等级来看,随机森林的检测精度亦优于Fisher判别分析与BP神经网络,但3种方法对中度危害等级的检测精度均有所不足。该成果可为刚竹毒蛾危害及其他病虫害检测算法的选择提供参考,并为进一步建立冠层、遥感影像像元等尺度的虫害检测模型奠定基础。 相似文献
160.
J. V. Leyendekkers A. G. Shannon 《International Journal of Mathematical Education in Science & Technology》2013,44(2):303-306
The modular ring ?6 defines integers via (6r i + (i ? 3)) where i is the class and r i the row when tabulated in an array. Since only Classes 26 and 46 contain odd primes, this modular ring is ideally suited to the analysis of twin primes. The calculations are facilitated by the use of the right-end digit (RED) technique. 相似文献