High-precision SMI microscopy size measurements by simultaneous frequency domain reconstruction of the axial point spread function

An improved size measurement method using spatially modulated illumination (SMI) microscopy enhances subwavelength size determination of fluorescent objects. In this new approach the point spread function of the SMI microscope is reconstructed in each measurement. For this, reference objects with known dye distribution have to be put additionally to the unknown objects on the object slide or on the cover slip. We present data from measurements on fluorescent microspheres with diameters of 140 and 200 nm using an excitation wavelength of 488 nm.     

基于深度变化成像模型的调整EM算法

在实际成像中,通常样本中的物质是变化的,故样本中不同位置的折射率不一样。由于三维样本的折射率与物镜所浸物质的折射率的不匹配,导致不同深度的点扩展函数可能不同。在此深度变化成像模型基础上应用最大期望(EM)复原算法能够提高图像清晰度,尤其是深度方向,但会丢失图像的一些微弱细节且出现一些孤立亮点,因此将调整EM算法运用到基于三维显微光学切片中成像随深度变化的图像模型上,此二者结合后的新算法可以避免上述缺点,较好地恢复图像微弱细节。     

铂-氧化铈/聚苯胺/聚砜复合膜电极的制备及对甲醇的电催化氧化

采用电化学聚合法制备了掺杂CeO2纳米粒子的聚苯胺(PAN)/聚砜(PSF)复合膜电极,在其上电沉积铂粒子,制得了铂-氧化铈/聚苯胺/聚砜的复合膜修饰电极。 复合膜的形貌和化学组分通过冷场发射扫描电子显微镜（Cold FE-SEM）和能量散射X射线谱（EDS）进行了表征,用循环伏安法和电化学交流阻抗法考察了复合膜电极对甲醇的电催化氧化性能。 结果表明,复合膜的双层多孔结构使铂粒子与CeO2粒子在复合膜内层的多孔聚苯胺上均匀沉积,粒子平均尺寸约为80 nm;CeO2为铂质量的7%时,铂-氧化铈/聚苯胺/聚砜复合膜修饰电极对甲醇有很好的电催化氧化性能和高的稳定性。     

特殊Thue系统表现的幺半群的两个性质

本文给出了有限特殊Ｃｈｕｒｃｈ－ＲｏｓｓｅｒＴｈｕｅ系统表现的上半群是群或正则半群的两个充要条件．并由此获得了判定该种幺半群是否群、正则半群的十分简单的算法．     

液晶共聚物与PSF原位复合的界面研究

合成了两种热致性液晶共聚酯ＢＰ—ＬＣＰ和ＳＤＰ—ＬＣＰ，对其熔融指数、取向性作了考察。选用基体聚砜（ＰＳＦ）与液晶共聚酯进行熔融共混，得原位复合材料。ＳＥＭ断口形态显示了两种液晶在基体中不同的成纤性，并显示出两相的不相容性。采用ＦＴ—ＩＲ方法分析了液晶共聚酯与ＰＳＦ界面间的分子相互作用。进一步研究发现在ＰＳＦ／ＢＰ－ＬＣＰ原位复合体系中加入含ＰＳＦ和ＢＰ－ＬＣＰ的嵌段共聚物，其相容性得以改善     

Formation and thermal stability of BMI-based interpenetrating polymers for gas separation membranes

Semi-interpenetrating polymer networks (semi-IPNs) were prepared by sol–gel technique through in situ polymerization of bismaleimide (BMI) in thermoplastic polyetherimide (PEI) as well as in polysulfone (PSF). This synthesis route allows arresting thermoset/thermoplastic phase separation at an early stage by solidifying the semi-IPNs through membrane phase inversion. The phase separation could be observed visually in the casting solution or by optical microscope on the surface of the produced membranes. These semi-IPNs with a density lower than their thermoplastic base polymer allowed easier water penetration during membrane phase inversion. This led to improved membrane morphology that was confirmed by scanning electron microscopy. Membranes fabricated from these semi-IPN materials had thinner skin layers and longer straight fingers perpendicular to membrane surface. Differential scanning calorimetry (DSC) and thermogravimetric analysis (TGA) showed that these semi-IPNs membranes have improved glass transition temperatures but a lower thermal stability. However, at ambient conditions, these membranes with their improved structure and morphology showed superior gas separation characteristics compared to base polymers. For example, the permeance was increased by 12–15 times without a significant decrease in the selectivity of oxygen over nitrogen in air separation experiments.     

Totally Ordered Monoids Based on Triangular Norms

A totally ordered monoid, or tomonoid for short, is a monoid together with a translation-invariant (i.e., compatible) total order. We consider in this paper tomonoids fulfilling the following conditions: the multiplication is commutative; the monoidal identity is the top element; all nonempty suprema exist; and the multiplication distributes over arbitrary suprema. The real unit interval endowed with its natural order and a left-continuous t-norm is our motivating example. A t-norm is a binary operation used in fuzzy logic for the interpretation of the conjunction.

Given a tomonoid of the indicated type, we consider the chain of its quotients induced by filters. The intention is to understand the tomonoid as the result of a linear construction process, leading from the coarsest quotient, which is the one-element tomonoid, up to the finest quotient, which is the tomonoid itself. Consecutive elements of this chain correspond to extensions by Archimedean tomonoids. If in this case the congruence classes are order-isomorphic to real intervals, a systematic specification turns out to be possible.

In order to deal with tomonoids and their quotients in an effective and transparent way, we follow an approach with a geometrical flavor: we work with transformation monoids, using the Cayley representation theorem. Our main results are formulated in this framework. Finally, a number of examples from the area of t-norms are included for illustration.     

基于高斯分布的星点图像亚像元定位算法研究

应用高斯点分布函数为数学模型,提出了一种新的获取高精度恒星质心位置的方法.由于入射到星像点邻域内像元中的光子能量呈近高斯分布,因此利用成像邻域内像元强度的比值,将高斯点分布函数展开成为关于质心位置的多项式,可将质心位置在x、y轴方向分别计算出来,并利用从星图中提取出的多星对角距误差的统计值来间接验证提出的算法.试验结果...     

甚高精度星敏感器的点扩散函数检测技术

为了研制精确的星点定位误差补偿算法,得到星像轮廓面的形貌信息,研究了检测星敏感器点扩散函数(PSF)的方法。在高精度测量平台上进行光电采样,获取星像像素灰度值分布,根据扩展Nijboer-Zernike理论进行PSF拟合重建。噪声仿真实验证明,该算法能够在星像信噪比较低的情况下准确地得到Zernike系数,从而快速地重建甚高精度星敏感器的空域PSF。基本满足自动检测甚高精度星敏感器星像轮廓面的要求。