Fabrication and Optimization of Poly(vinyl alcohol)/Zirconium Acetate Electrospun Nanofibers Using Taguchi Experimental Design

This paper presents an investigation regarding poly(vinyl alcohol)/zirconium acetate (organic–inorganic) (PVA/Zrace) nanofibers prepared by electrospinning which could be used as a precursor for fabricating ceramic metal oxide nanofibers. The effect of some processing variables, including polymer solution concentration, tip to collector distance and applied voltage of electrospinning, and the amount of Zrace and their interactions, on the diameter of the nanofibers were studied. Taguchi experimental design and a statistical analysis (ANOVA) were employed and the relationship between experimental conditions and yield levels determined. It was concluded that to obtain a narrow diameter distribution as well as maximum fiber fineness, a polymer concentration of 10 wt%, tip to collector distance of 18 cm and applied voltage of 20 kV variables were the optimum. Furthermore, it was also concluded that the ratio of Zrace (6 g) to PVA solution (10% wt) played an important role for achieving the minimum fiber diameter. Under these optimum conditions, the diameters of the electrospun composite fibers ranged from 86 nm to 381 nm with a diameter average of 193 nm. The experiments were done with Qualitek-4 software with “smaller is better” as the quality characteristics. The optimized conditions showed an improvement in the fibers diameter distribution and the average fibers diameter showed good resemblance with the result predicted using the Taguchi method and the Qualitek-4 software. The ANOVA results showed that all factors had significant effects on the fibers diameter and distribution, but the effect of PVA concentration and zirconium acetate were more significant than the other factors.     

准方波脉冲形成网络的理论分析与设计

针对微波驱动源、固态调制器等对宽平顶脉冲源的应用需求,开展了基于脉冲形成网络输出准方波的理论研究与分析设计。首先采用Prony算法获得准方波波形的解析表达式,然后基于最佳一致逼近的优化控制思路,列出极点控制方程,采用数值方法求解非线性方程组,获得优化波形参数。在此基础上采用阻抗函数匹配的算法求解出脉冲形成网络的元件参数初始值,根据工程设计的实际情况舍弃部分参数并对个别参数进行优化后,获得最终的元器件参数。通过理论分析与数值模拟相结合的方法,系统地给出了获取长脉宽、低纹波准方波脉冲形成网络的设计方法以及设计准则。该方法可用于设计任意阶低纹波系数的准方波脉冲源,也可用于设计其他输出波形要求的脉冲源。     

超高强块体非晶合金的研究进展

研制具有极限力学性能的金属材料一直是材料研究人员的梦想.超高强块体非晶合金是一类具有极高断裂强度(4 GPa)、高热稳定性(玻璃化转变温度通常高于800 K)和高硬度(通常高于12 GPa)的新型先进金属材料,其代表合金材料Co-Ta-B的断裂强度可达6 GPa,为目前公开报道的块体金属材料的强度记录值.本文系统地综述了该类超高强度块体非晶合金的组分、热学性能、弹性模量及力学性能,阐述了该类材料的研发历程;以弹性模量为联系桥梁,阐明了该类超高强块体非晶合金材料各物理性能的关联性,并揭示了其高强度、高硬度的价键本质.相关内容对于材料工作者了解该类超高强度金属材料的性能和特点,并推进该类材料在航空航天先进制造、超持久部件、机械加工等领域的实际应用有着重要意义.     

Numerical investigation on broadband mid-infrared supercontinuum generation in chalcogenide suspended-core fibers

As_2S_3 and As_2Se_3 chalcogenide 3-bridges suspended-core fibers(SCFs) are designed with shifted zero-dispersion wavelengths(ZDWs) at around 1.5 μm, 2 μm, and 2.8 μm, respectively. A generalized nonlinear Schr ¨odinger equation is used to numerically compare supercontinuum(SC) generation in these SCFs pumped at an anomalous dispersion region nearby their ZDWs. Evolutions of the long-wavelength edge(LWE), the power proportion in the long-wavelength region(PPL), and spectral flatness(SF) are calculated and analyzed. Meanwhile, the optimal pump parameters and fiber length are given with LWE, PPL, and SF taken into account. For As_2S_3 SCFs, SC from a 14 mm-long fiber with a ZDW of 2825 nm pumped at 2870 nm can achieve the longest LWE of ～ 13 μm and PPL up to ～72%. For As_2Se_3 SCFs, the LWE of 15.5 μm and the highest PPL of ～ 87% can be achieved in a 10 mm-long fiber with ZDW of 1982 nm pumped at 2000 nm. Although the As_2Se_3 SCFs can achieve much longer LWE than the As_2S_3 SCFs, the core diameter of As_2Se_3 SCFs will be much smaller to obtain a similar ZDW, leading to lower damage threshold and output power. Finally, the optimal parameters for generating SC spanning over different mid-IR windows are given.     

300MeV质子同步加速器概念设计优化（英文）

目前处于设计阶段的哈尔滨工业大学空间辐照效应装置,其核心部件是由1台10 MeV的注入器、1台300MeV的同步加速器以及输运线构成的加速器装置。同步加速器中引出的质子束流被用于辐照研究。基于装置的概念设计,优化了其同步加速器部分的设计。设计了新的磁聚焦结构,优化了基于新的磁聚焦结构的多圈注入系统的凸轨变化模式,提高了注入效率。为了更好地优化引出束流的时间结构,慢引出系统采用了RF knock-out的方法。为了满足精准辐照的要求,研究了RF Kicker的频率调制,发现RF Kicker的双频调制能使得引出束流更均匀。A research complex for aerospace radiation effects research is in the designing stage in Harbin Institute of Technology. Its core part is a proton accelerator complex, which consists of a 10 MeV injector, a 300 MeV synchrotron and beam transport lines. The proton beam extracted from the synchrotron is utilized for the radiation effects research. Based on the conceptual design, the design study for optimizing the synchrotron has been done. A new lattice design was worked out, and the decreasing pattern of the bump of the multi-turn injection system was optimized to increase the injection efficiency. In order to improve the time structure of the extracted beam, a RF knock-out method is employed in the slow extraction system. To meet the requirement of accurate control of dose, the frequency modulation of the RF kicker is well investigated, and the dual frequency modulation has been found to have a better performance for a uniform spill.     

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介绍了EAST托卡马克逆磁线圈加补偿线圈的逆磁测量。该方法的优点是补偿线圈有效地消除了纵场线圈产生的磁通变化,而调节机构能降低来自极向场的误差信号。详细地叙述了逆磁线圈工程设计中考虑的材料选择和结构设计对逆磁线圈的影响。最后给出了次测量系统的误差分析。     

大口径照相物镜制造与设计的综合考虑

给出了透射式 f′ =60 0mm ,D =40 0mm ,2ω =2 5° ,工作波段在 0 5～ 0 8μm之间的照相物镜的两个设计方案。考虑到在制造过程中可能存在的问题 ,作者对设计方案进行了分析和比较后选择了其中之一。     

低温低噪声放大器的发展概况及其结构设计综述

介绍了低温低噪声放大器的研制历史、现状及应用情况 ,举例分析了在该类放大器的结构设计中需要解决的关键技术 ,对军事和民用装备的有关领域有参考作用。     

叶轮机械设计与影响性能及内流的若干重要问题

本文按照假想等价速度三角形的概念及应用平面叶栅资料,给出了叶轮机械准三元设计时Ｓ１流面叶片造型的几种不同方法,通过设计例作了比较。同时用数值计算和实验结果,对影响叶轮机机械性能及内流的若干重要问题如叶顶间隙、来流条件（前置进气箱、进口速度畸变、预旋等）进行了讨论。     

激光光源粒子计数器响应曲线对粒子折射率敏感度及多值性的分析

采用激光作光源的光学粒子计数器(L_OPC)克服了白炽灯作光源时使用寿命短、发光强度不稳定、需要经常标定的缺点,但激光波长的单一也带来了一些问题,如响应曲线对折射率敏感度的变化和多值性等问题。利用Mie散射理论,通过数值模拟实验,对L_OPC的这些问题进行了分析,提出了L_OPC实验样机的设计参数。