首页 | 本学科首页   官方微博 | 高级检索  
文章检索
  按 检索   检索词:      
出版年份:   被引次数:   他引次数: 提示:输入*表示无穷大
  收费全文   187篇
  免费   28篇
  国内免费   24篇
化学   34篇
晶体学   1篇
力学   7篇
综合类   14篇
数学   110篇
物理学   73篇
  2023年   3篇
  2022年   10篇
  2021年   14篇
  2020年   10篇
  2019年   4篇
  2018年   2篇
  2017年   5篇
  2016年   16篇
  2015年   5篇
  2014年   8篇
  2013年   13篇
  2012年   29篇
  2011年   14篇
  2010年   10篇
  2009年   9篇
  2008年   20篇
  2007年   9篇
  2006年   11篇
  2005年   12篇
  2004年   2篇
  2003年   7篇
  2002年   5篇
  2001年   6篇
  2000年   6篇
  1999年   2篇
  1998年   3篇
  1997年   1篇
  1994年   1篇
  1992年   1篇
  1989年   1篇
排序方式: 共有239条查询结果,搜索用时 15 毫秒
31.
In this paper,we study a general Lévy risk process with positive and negative jumps.A renewal equation and an infinite series expression are obtained for the expected discounted penalty function of this risk model.We also examine some asymptotic behaviors for the ruin probability as the initial capital tends to infinity.  相似文献   
32.
给出了一种基于均方误差估计的非本征光纤法布里-珀罗(EFPI)传感器的腔长解调算法。在参量估计方面, 均方误差将估计子的方差和偏差结合在一起, 具有更高的估计精度和准确度。如果给出某一个真值的一系列估计子, 则具有最小均方误差的估计子比其他估计子更为有效。在非本征光纤法-珀传感器的腔长解调方面, 则实际腔长对应于腔长均方误差估计取最小值时的腔长估计子。对一个非本征光纤法-珀压力传感器的测试结果表明, 腔长解调分辨率为0.18 nm, 对应的压力分辨率可达2.99 kPa。与传统的解调算法相比, 通过该算法可在较宽的动态范围内获得高的解调分辨率, 并实现绝对腔长的解调。  相似文献   
33.
用157 nm激光制作的光子晶体光纤法布里-珀罗传感器   总被引:6,自引:2,他引:4  
157nm准分子激光用于微加工具有单光子能量高,峰值功率高,材料吸收系数高,分辨率高等优点。利用157nm激光微加工的方法,在光子晶体光纤上融切出微小矩形孔,从而构成腔长为45.6μm的微光纤法布里-珀罗干涉腔,得到的干涉条纹平滑,衬比度约为26dB,并从激光与石英材料的相互作用上分析了形成较好干涉条纹的原因。把这种微腔应用于应变测量,在550μm范围内,腔长增量相对于应变的灵敏度为0.32nm/μm,线形度达0.9994。实验证明该微腔对温度不敏感,800℃范围内腔长变化仅20nm。157nm准分子激光加工光纤法布里-珀罗腔方法简单,一次成型,具有较高的加工效率和精度,有望实现光纤法布里-珀罗腔的规模化批量制造,具有较好的应用前景。  相似文献   
34.
宽截止窄带高反射滤光膜设计   总被引:2,自引:1,他引:1  
窄带高反射滤光膜在光通讯、光学探测仪器等领域有着重要应用.探讨了"基片|H(LH)m1aL(HL)m2βCr,M|空气"膜系结构的窄带高反射滤光膜系,讨论了金属Cr层厚度,以及两种不同的匹配膜系对滤光膜特性的影响,计算了Cr层内部的电场分布.结果表明,较厚的金属层可实现更宽的截止带宽,匹配层的加入有效地实现了宽截止带的深截止,使中心波长处导纳为较大值的匹配膜系可以更好地实现滤光膜宽截止、窄带高反射特性;匹配膜层使中心波长处Cr层内部的电场强度趋于零,有效地降低了整个膜系的吸收,提高了反射率.  相似文献   
35.
戴霞娟  王鸣  贲玉红 《光学学报》2008,28(7):1241-1246
将快速傅里叶变换(FFT)与线性调频Z变换(CZT)联合变换的方法应用到法布里-珀罗(F-P)腔传感器的解调中,从理论上分析了该方法的解调原理及误差.模拟计算得出,该联合算法解调出的腔长的相对误差达到0.01%,腔长的最大绝对误差小于0.05 μm.在对测量范围为O~3 MPa的F-P腔微机电系统(MEMS)压力传感器进行的解调试验中,该算法可以辨别0.01 MPa的压力,腔长与压力数据的拟合度为0.99316,测量压力与实际压力的标准偏差小于0.005 MPa.实验结果表明,FFT与CZT联合解调的方法可以在较少计算量的基础上达到较高的精度,满足实际需求.  相似文献   
36.
The chemical functionalization of carbon nanotubes is often a prerequisite prior to their use in various applications. The covalent grafting of 4,4,5,5-tetramethyl-1,3,2-dioxaborolane (BPin) functional groups directly on the surface of multi- and single-walled carbon nanotubes, activated by nucleophilic addition of nBuLi, was carried out. Thermogravimetric analysis (TGA) coupled with mass spectrometry, Raman spectroscopy, X-ray photoelectron spectroscopy (XPS) and time-of-flight secondary ions mass spectrometry (ToF-SIMS) confirmed the efficiency of this methodology and proved the integrity and covalent grafting of the BPin functional groups. These groups were further reacted with various nucleophiles in the presence of a copper(II) source in the conditions of the aerobic Chan–Lam–Evans coupling. The resulting materials were characterized by TGA, XPS and ToF-SIMS. This route is efficient, reliable and among the scarce reactions that enable the direct grafting of heteroatoms at carbonaceous material surfaces.  相似文献   
37.
An in‐capillary 2, 2‐diphenyl‐1‐picrylhydrazyl (DPPH)‐CE‐the DAD (in‐capillary DPPH‐CE‐DAD) combined with reversed‐electrode polarity stacking mode has been developed to screen and quantify the active antioxidant components of Cuscuta chinensis Lam. The operation parameters were optimized with regard to the pH and concentration of buffer solution, SDS, β‐CDs, organic modifier, as well as separation voltage and temperature. Six antioxidants including chlorogenic acid, p‐coumaric acid, rutin, hyperin, isoquercitrin, and astragalin were screened and the total antioxidant activity of the complex matrix was successfully evaluated based on the decreased peak area of DPPH by the established DPPH‐CE‐DAD method. Sensitivity was enhanced under reversed‐electrode polarity stacking mode and 10‐ to 31‐fold of magnitude improvement in detection sensitivity for each analyte was attained. The results demonstrated that the newly established in‐capillary DPPH‐CE‐DAD method combined with reversed‐electrode polarity stacking mode could integrate sample concentration, the oxidizing reaction, separation, and detection into one capillary to fully automate the system. It was considered a suitable technique for the separation, screening, and determination of trace antioxidants in natural products.  相似文献   
38.
We obtain an explicit formula for the number of Lamé equations (modulo linear changes of variable) with index and projective monodromy group of order , for given and . This is done by performing the combinatorics of the `dessins d'enfants' associated to the Belyi covers which transform hypergeometric equations into Lamé equations by pull-back.

  相似文献   

39.
Toddalia asiatica (L.) Lam. (Rutaceae) has shown a broad spectrum of biological properties, such as anti-inflammatory, antioxidant, antimicrobial, anti-HIV, and anticancer properties. The present study is concerned with the separation of the main components with broad partition coefficients (KD values) from T. asiatica, using linear gradient high-speed counter-current chromatography (LGCCC) combined with an off-line two-dimensional (2D) mode. Similar to the binary gradient HPLC, the LGCCC mode is operated by the adjustment of the proportion between the mobile phase of 5:5:1:9 (v/v) (pump A) and 5:5:4.5:5.5 (v/v) (pump B) in an n-hexane/ethyl acetate/methanol/water solvent system. The off-line 2D-CCC mode was used in this study for the secondary separation of two similar KD value compounds with n-hexane/ethyl acetate/methanol/water (5:5:4:6, v/v). Notably, six coumarins, namely, tomentin (1), toddalolactone (2), 5,7,8-trimethoxycoumarin (3), mexoticin (4), isopimpinellin (5), and toddanone (6), were efficiently separated. The structures of the pure compounds were elucidated by spectral techniques and compared with the literature.  相似文献   
40.
选取纯弯曲梁进行裂缝扩展研究,在理论上符合Ⅰ型断裂模式.因此,本文利用扩展有限元法(XFEM)模拟了混凝土纯弯曲梁裂缝发展的全过程,结合线性叠加渐进假定,得到了不同初始缝高比的P-δ曲线、P-CMOD曲线以及临界有效裂缝扩展长度(ac-a0)/h与裂缝发展路经.对比试验数据和模拟结果表明:随着初始缝高比的增大,起裂荷载Pini、最大荷载Pmax、离散弗雷歇距离δdF与δd F,以及临界有效裂缝长度(ac-a0)/h均逐渐减小;试验与模拟的裂纹发展路径存在一定偏差,可知试验数据与模拟结果存在规律性差异.  相似文献   
设为首页 | 免责声明 | 关于勤云 | 加入收藏

Copyright©北京勤云科技发展有限公司  京ICP备09084417号