Spectroscopic investigation of arsenate and selenate incorporation into hydroxylapatite

The mechanism(s) of arsenate and selenate incorporation into hydroxylapatite (HAP) using extended X-ray absorption fine structure (EXAFS) spectroscopy was investigated for As- and Se-doped HAP samples with concentrations between 200 and 2500 ppm. EXAFS data on As and Se K-edges have shown similar local coordination environments and are similar to that of P in HAP, suggesting the substitution of arsenate or selenate tetrahedra on the phosphate sites. EXAFS best-fitting for As-doped samples shows that the first shell is fitted with approximately 4 O atoms at 1.68 Å, showing As(V) in tetrahedral coordination, and Se K-edge EXAFS data are characterized by the backscattering contributions an oxygen shell at 1.2 Å in the Fourier transform, which can be fit with 4 O atoms at 1.65 ± 0.01 Å. This is characteristic of Se–O distances in SeO₄ tetrahedron. These findings suggest that arsenate and selenate substitute for phosphate groups with local distortions during the incorporation of these metals into the structure of HAP.     

自然闪电条件下敷地线缆耦合试验

研制了一套能够同时测量线缆皮线和芯线感应电流的试验系统,研究自然闪电条件下敷地线缆的耦合问题。结果表明：不同位置处的线缆皮线感应电流波形基本一致,但幅值存在一定差异,说明感应电流空间分布不均匀; 所测线缆芯线和皮线感应电流的时域波形和频谱比较相似,能量集中在1 kHz~1 MHz之间; 正负地闪芯线感应电压波形均为单一脉冲型,波形持续时间10~49 μs; 正地闪线缆感应电压的幅值范围及幅值平均值都大于负地闪相应结果,说明正地闪产生的线缆耦合作用大于负地闪; 不同雷电过程的线缆感应电压幅值与磁感应强度有较小的相关性,而同一雷电过程则基本成线性关系; 正地闪线缆感应电压波形持续时间、半峰值宽度、10%~90%上升时间的范围及均值都比负地闪的要大。     

飞机外露物隐身改进设计研究

外露物在一定程度上影响飞机隐身性能,而外露物的共形设计会增加成本。针对低成本准隐身飞机,本文探讨了一种外露物的隐身改进设计,主要采取优化外形,涂敷吸波材料、提升加工工艺等措施实现低成本飞机RCS值的缩减。经过隐身仿真、隐身测试等手段,获取了外露物在不同频点、不同极化下的RCS值,并通过仿真、测试数据对比验证采取隐身改进措施的有效性,并为其它外露物隐身设计提供了设计依据和手段。     

基于Al_2O_3封装薄膜的OLED水汽透过率测试方法及系统研究

水汽透过率(WVTR)是衡量有机电致发光器件(OLED)封装薄膜性能的重要参数之一。本文研究了基于钙电学法的WVTR测试方法,设计并研制了可满足OLED水汽透过率测试精度和功能要求的测试系统,测试精度达1×10-6g·m-2·d-1,量程为10 g·m-2·d-1,可同时完成20个样品的快速、精确测量。利用本系统对采用原子层沉积技术制备的不同厚度Al2O3封装薄膜的WVTR进行了测试研究,结果表明,Al2O3薄膜具有良好的水汽阻挡性能。     

KB scanning of X‐ray beam for Laue microdiffraction on accelero‐phobic samples: application to in situ mechanically loaded nanowires

A mapping technique has been developed where a sub‐micrometer focused polychromatic X‐ray beam is scanned across a stationary sample instead of scanning the sample in front of the X‐ray microbeam. This method is applied to a gold nanowire during its mechanical loading using the tip of an atomic force microscope. During the loading process, such a sample is `accelero‐phobic', i.e. the sample scanning stages must not to be moved to avoid parasitic additional load. Without beam scanning, only one single position within the sample can be probed during the test. The probed material point may even change because of drifts or movements induced by the test itself. The new scanning approach facilitates the in situ mapping of the entire wire giving access to the evolution of the wire shape as well as to the boundary conditions. This novel scanning technique opens promising perspectives for studies where sample motion is forbidden because of the sample environment.     

基于验前试验信息熵的测试性验证试验方案

产品在研制阶段存在大量的试验数据,为有效利用验前数据,降低测试性验证试验样本量,提出一种基于验前试验信息熵的测试性验证试验方案。该方案利用信息熵来度量研制阶段多次验前试验数据对测试性验证试验所起的作用,依据平均互信息熵和信息总量相等的原则,将多次验前试验数据等效成一次成败型数据。在此基础上,通过相容性检验方法确定验前数据与试验数据的相容性水平,并以Beta分布为验前分布,利用加权混合贝叶斯理论建立混合验后分布,之后,基于贝叶斯平均风险理论求解满足双方风险要求的试验方案。最后,以某型雷达发射分机为例,对其进行测试性验证试验研究,研究结果验证了该方案的有效性。     

一种多功能信号源系统设计

针对单一信号源无法满足测试需求的现状,提出了一种新型多功能信号源系统设计方案;详细阐述了信号源系统的硬件及软件设计,方案基于标准化、高速、可靠性三方面的考虑,硬件环境基于Compact PCI工控计算机,设计了3U CPCI结构的信号源板卡,配套软件采取模块化设计;该方案可实现多类型、多通道的高精度、高可靠性信号的独立输出和同时输出;实验结果表明,该多功能信号源系统稳定性好、可靠性高、使用便捷,满足设计需求。     

声诱饵仿真试验系统

文章介绍了声诱饵仿真试验系统中的有关问题，包括：系统的组成、工作原理、对接装置结构等。建立了对接装置声耦合状态下的数学模型，对近场声压分布进行了仿真计算，得出了匹配材料厚度、发射和接收换能器的选取原则。     

大数值孔径、高次非球面透镜的加工与检验

通过一空间相机光学系统中某透镜的高次非球面表面加工过程,提出了一种基于小磨头数控光学表面成型技术(CCOS,Computercontrolopticalsurfacing)和非球面轮廓检验、零位补偿检验技术的中等口径高次非球面光学表面的加工、检测方法,并且给出了补偿器实际光学设计结果。文中采用这种方法加工的高次非球面表面,最终精度优于1λP V(λ=632.8nm),满足了设计要求。对这种技术的适用范围进行了简明的讨论。     

多气隙电阻板室的宇宙线测量结果

介绍了20多个多气隙电阻板室的宇宙线测量结果.测量所用的宇宙线平台可以同时测量同一个电阻板室的多个cell,其参考时间的时间分辨为70ps.在宇宙线的测量条件下,用国产材料制作的多气隙电阻板室的时间分辨可达到90ps.利用这套宇宙线测量系统,还对多气隙电阻板室的探测效率和cell间的相互串扰进行了研究.