红外光谱法快速测定润滑油添加剂

利用ＰＥ－ＦＴＩＲ红外光谱仪及ＰＥ公司“Ｑｕａｎｔ”计算机软件,测定润滑油添加剂单剂与复合剂含量,实际测定了１５Ｗ／４０ＳＥ、１５／３０ ＳＥ／ＣＤ、１５／Ｗ４０ＣＤ、１５Ｗ／３０ＣＣ油品试样。测量范围为０．２％￣９０％,测定相对误差小于１０％。     

Schrödinger Operators with Empty Singularly Continuous Spectra

Let H be a semibounded perturbation of the Laplacian H ₀ in L ²( ^d ). For an admissible function sufficient conditions are given for the completeness of the scattering system (H), (H ₀). If is the exponential function and if e^{– H} is an integral operator we denote the kernel of the difference D = e^{– H} – e^{– H} ₀ by D (x, y), > 0. The singularly continuous spectrum of H is empty if^d dx ^d dy |D(x,y)| (1 + |y|²)< for some > 1. This result is applied to potential perturbations and to perturbations by imposing Dirichlet boundary conditions.     

Elastoplastic stress analysis for cylindrical shell with flat strip imperfection

Based on unequidistant B-spline function, generalized spline subdomain displacement mode of rotational shell is obtained by taking double-direction interpolation of spline. The elastoplastic constitutive equation of shells is established by using the endochronic theory.According to the initial deflection theory of shells, the elastoplastic stress analysis of cylindrical shells with flat strip geometrical imperfection is studied. Numerical results show that the geometrical imperfection has a great effect on the stress distribution of shells.     

四元数矩阵方程AX-YB=C的最佳逼近解

本利用四元数矩阵的广义Frobenius范数建立一个关于四元数矩阵的实函数，并讨论了它的极值问题．然后在四元数矩阵方程AX-YB=C的解集合中导出了与给定矩阵的最佳逼近解的表达式．     

计量调整型抽样检验系统GB/T6378-1986与ISO3951 :1989的比较分析

GB/T6378-1986作为计量抽样检验方面的基础性国家标准,是参照国际标准ISO3951:1989而制定的。1989年国际标准化组织ISO/TC69发布了ISO3951的修订版本ISO3951:1989,ISO3951的这一修订版反映了计量抽样检验的最新研究成果,为开展国家标准GB/T6378的修订工作,本文系统地对GB/T6378-86和ISO3951:89进行了比较分析研究。     

Isotope-dependent crystalline phases at ambient temperature: Spectroscopic and calorimetric evidence for a deuteration-induced phase transition at 320 K in α-DCrO2

The heat capacities of HCrO₂ and DCrO₂ have been measured at temperatures between 5 and 360 K. A lambda anomaly occurred at 320 K for DCrO₂ but not for HCrO₂. Infrared spectra were recorded at temperatures between 5 and 405 K. The spectrum of DCrO₂ changed at 320 K with respect to the peak wave-number and splitting of some of the vibrations, while those of HCrO₂ depended smoothly on temperature. These experimental results are discussed in terms of a deuteration-induced phase transition.     

InGaAsSb/AlGaAsSb长波长多量子阱激光器有源区的优化设计

系统地研究了波长为2.7μm的InGaAsSb/AlGaAsSb多量子阱激光器中有源区的优化设计.分别用含应变势的6带KP模型和抛物带模型计算价带和导带的能带结构，并得到薛定谔方程和泊松方程的自洽解，由此计算量子阱在载流子注入时的增益谱.研究表明制约量子阱增益的主要因素不是跃迁矩阵元，而是粒子数反转程度，尤其是空穴填充HH1子带的概率.增加压应变或减小阱宽都会提高量子阱增益.前者降低了价带HH1子带空穴的平面内有效质量；后者拉大了价带子带间距，尽管它同时略微增加了空穴有效质量.这两种因素都导致价带顶空穴态     

Waiting time problems for a sequence of discrete random variables

Let X ₁, X ₂,... be a sequence of nonnegative integer valued random variables.For each nonnegative integer i, we are given a positive integer k _i . For every i = 0, 1, 2,..., E _i denotes the event that a run of i of length k _i occurs in the sequence X ₁, X ₂,.... For the sequence X ₁, X ₂,..., the generalized pgf's of the distributions of the waiting times until the r-th occurrence among the events % MathType!MTEF!2!1!+-% feaafeart1ev1aaatCvAUfeBSjuyZL2yd9gzLbvyNv2CaerbuLwBLn% hiov2DGi1BTfMBaeXafv3ySLgzGmvETj2BSbqefm0B1jxALjhiov2D% aebbfv3ySLgzGueE0jxyaibaiiYdd9qrFfea0dXdf9vqai-hEir8Ve% ea0de9qq-hbrpepeea0db9q8as0-LqLs-Jirpepeea0-as0Fb9pgea% 0lrP0xe9Fve9Fve9qapdbaqaaeGacaGaaiaabeqaamaabaabcaGcba% WaaiWabeaacaWGfbWaaSbaaSqaaiaadMgaaeqaaaGccaGL7bGaayzF% aaWaa0baaSqaaiaadMgacqGH9aqpcaaIWaaabaGaeyOhIukaaaaa!43D8!\[\left\{ {E_i } \right\}_{i = 0}^\infty\]are obtained. Though our situations are general, the results are very simple. For the special cases that X's are i.i.d. and {0, 1}-valued, the corresponding results are consistent with previously published results.This research was partially supported by the ISM Cooperative Research Program (90-ISM-CRP-11) of the Institute of Statistical Mathematics.     

Studies on the thermal decomposition of N,N'-ethylenebis(salicylideneiminato) diaquochromium(III) nitrate

A complex of N,N'-ethylenebis(salicylideneiminato)diaquochromium(III) nitrate, [Cr(salen)(H₂O)₂]NO₃ was characterized and its decomposition mechanism was studied by TG. The IR spectrum and X-ray analysis were examined for the complex. The non-isothermal kinetic data were analyzed by means of the Achar method and the Coats—Redfern method. The most probable kinetic model function was suggested by comparison of the kinetic parameters.This revised version was published online in November 2005 with corrections to the Cover Date.     

污染气体红外光谱鉴别器的优化设计

针对污染气体红外光谱特征分布的复杂性，结合几种线性分类器的特点，通过对每个环节的深入分析，设计出一种混合多叉树状光谱鉴别器。实验结果表明：此光谱鉴别器不仅结构简洁，设计合理，具有很高的分类能力和判别准确率，而且具有较好的灵活性和稳定性，完全满足快速识别的需要，是一种高效的光谱鉴别器。