Fe-Al-N films were fabricated by reactive sputtering using a radio-frequency magnetron sputtering system. The effects of Al and N content and annealing temperature on microstructure and magnetic properties were investigated. The Fe-Al-N films, which have good soft magnetic properties, consist of nanocrystalline α-Fe grains and a small amount of other phases in the boundaries of α-Fe grains. The average α-Fe grain size is about 10-15nm. A slight amount of Fe-N and Al-N compounds precipitate in the boundaries of α-Fe grains and suppress their growth. Annealing improves the soft magnetic properties slightly by releasing the residual stress and reducing defects. 相似文献
Summary: The sol‐gel transition of one thermoreversible gelling mixture made of xanthan gum and locust bean gum has been studied by using in situ time‐resolved dynamic light scattering (DLS) and measuring the spin‐lattice relaxation time T1 of several protons. A critical dynamical behavior was observed near the sol‐gel transition, which is characterized by the presence of power‐law spectra over four decades of the delay time in the time‐intensity correlation function g2(t)−1 ∼ t−μ at 48 °C. The increase in T1 with increasing temperature becomes steeper at 50 °C indicating a significant change in the local mobility of one anomeric proton of the xanthan side chain and the anomeric protons of the locust bean gum mannose backbone.
Temperature dependence of the spin‐lattice relaxation time T1 for the equatorial anomeric proton of the mannopyranosic unit located next to the main chain of the xanthan. 相似文献
The distributive, codistributive, standard, costandard, and neutral elements of the lattice of overcommutative varieties of semigroups are completely described. 相似文献