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In-situ energy dispersive x-ray diffraction on ZnS nanocrystalline was carried out under high pressure by using a diamond anvil cell. Phase transition of wurtzite of 10nm ZnS to rocksalt occurred at 16.0GPa, which was higher than that of the bulk materials. The structures of ZnS nanocrystalline at different pressures were built by using materials studio and the bulk modulus, and the pressure derivative of ZnS nanocrystalline were derived by fitting the equation of Birch-Murnaghan. The resulting modulus was higher than that of the corresponding bulk material, which indicates that the nanomaterial has higher hardness than its bulk materials. 相似文献
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FENGYi-Si YAORi-Sheng ZHANGLi-De 《中国物理快报》2004,21(7):1374-1376
SnO2/SiO2 nanocomposites have been prepared by the soaking-thermal-decomposing method, tin oxide nanoparticles are uniformly dispersed in the mesopores of silica. The optical absorption edge of the obtained nanocomposite presents a redshift compared with bulk tin oxide, With the increasing annealing temperature during the procedure of the sample preparation, the optical absorption edge of the sample moves to shorter wavelength (blueshift). These optical properties can be ascribed to the amorphous structure and band defects of surface layers of the tin oxide nanoparticles. 相似文献
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Field Emission from Silicon Nanocrystallite Films with Compact Alignment and Uniform Orientation
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Patterned silicon nanocrystallite (SINC) films were fabricated on (100) orientation p-type boron-doped sificon wafer by the hydrogen ion implantation technique and the anodic etching method. The efficient field emission with low turn-on field of about 3.5V/μm at current density of 0.1μA/cm^2 was obtained. The emission current density from the SiNC films reached 1mA/cm^2 under a bias field of about 9.1V/μm. The experimental results demonstrate that there are great potential applications of the SiNC films for fiat panel displays. A surface treatment with hydrogen plasma was performed on the SiNC films and a significant improvement of emission properties was achieved. 相似文献
77.
所谓超固体(supersolid)是这样一类物质,它们自身具有互斥的性质:一方面是刚性晶体,长程空间有序;另一方面,又象是自由流动的超流体.对于超固体的研究历史,可以追溯到1969年,Andreev and Lifshitz研究了晶体中格点空位的作用.他们提出:在极低温下,空位有可能在整个晶体范围内退局域化,形成玻色-爱因斯坦凝聚;尽管原子排列规则有序,超流行为仍可能在其中发生.在实验室中观察超固体行为的研究努力,持续了35年.2004年,美国宾州大学的Kim E等报告了关于超固体的第一个实验证据.加压4^He被置于一个扭摆容器中,当样品被冷却到175mK以下,实验者观察到扭摆转动惯量的突然下降.定量的估计表明,样品中大约有1%的组分停止了随固态氦的震荡,或者说有1%成为超流.不过,其中的机制,迄今尚无共识. 相似文献
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合成了Co@SiO2核壳式纳米粒子,并采用透射电镜(TEM)、X射线衍射(XRD)、扫描电镜(SEM)和振动样品磁强计(VSM)对其形状、尺寸、荧光及磁特性进行了表征,探讨了其在细胞分离和细胞芯片上的应用和原理. 相似文献
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Large quantities of CaN nanorods are successfully synthesized on Si(111) substrates by ammoniating the films of Ga2O3/ZnO at 950℃ in a quartz tube. The structure, morphology and optical properties of the as-prepared CaN nanorods are studied by x-ray diffraction, scanning electron microscopy, high-resolution transmission electron microscopy, Fourier transform infrared spectroscopy, and photoluminescence. The results show that the CaN nanorods have a hexagonal wurtzite structure with lengths of several micrometres and diameters from 80 nm to 300hm, which could supply an attractive potential to harmonically incorporate future GaN optoelectronic devices into Si-based large-scale integrated circuits. The growth mechanism is also briefly discussed. 相似文献
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