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41.
通过水热法合成由临床用药蒙脱石(Montmorillonite, MMT)负载的高效纳米酶氧化铈(Cerium dioxide, CeO2), 通过开展体内外实验, 拓展其在炎症性肠病治疗中的普适性. 结果显示, CeO2@MMT具有良好的类超氧化物歧化酶活性及类过氧化氢酶活性, 并且在小鼠克罗恩病的治疗中体现了明显的疗效及优异的生物安全性, 为CeO2@MMT的应用拓宽了方向. 相似文献
42.
Fan Yi Lin-Zhen Liu Mei-Jiang Zhang Ting-Ting Wang Jian-Nong Ye 《Analytical letters》2018,51(9):1358-1372
The primary clinical diagnosis of Alzheimer’s disease is mainly based on medical history and neuropsychiatric inventory. It is urgent to seek biological indicators with better sensitivity and higher specificity to clinically diagnose and evaluate Alzheimer’s disease. In this work, an electrophoretic method based on 2-thiobarbituric acid derivatization and amperometric detection was developed to determine formaldehyde as a urinary biomarker of Alzheimer’s disease. Under the optimum conditions, the formaldehyde derivative was well separated from the coexisting interferences in urine sample. The limit of detection for formaldehyde was 80.0?nM (2.4?ng/?mL) based on an electrophoretic stacking technology. The average recovery values were in the range of 91.7–110%, and the relative standard deviation values were less than 4.1%. This method has been applied to analyze human urine samples from healthy volunteers and patients with different degrees of Alzheimer’s disease. The assay results showed that the content of urinary formaldehyde in patients suffering Alzheimer’s disease was significantly higher than that in healthy subjects (P?0.01), suggesting that urinary formaldehyde may be speculated to be an auxiliary noninvasive biomarker for the preliminary diagnosis of Alzheimer’s disease. High separation efficiency, simple sample preparation, environmental friendliness, and low cost are the main advantages of this proposed method. 相似文献
43.
Four commercially available formulations containing iron, zinc, and manganese were subjected to dissolution profile testing during 60 min and the dissolution was analyzed by ion chromatography. The obtained curves were analyzed directly by principal component analysis (PCA). The main trend (87.1% of variance) was connected with average dissolution percentage over the investigated time. The second component (11.2% of variance) is connected with shape of dissolution profile. All metals behave in the similar way and the differences were connected with excipients. An additional fit was completed on 12 kinetic models: first order kinetics (4 variants), Higuchi (2 variants), Hixson-Crowell (2 variants), Korsemeyer-Peppas, Logistic (2 variants), Peppas-Sahlin, Quadratic (2 variants), Weibull (3 variants), and Zero order kinetics (2 variants). The ranking of the fitting was performed by Akaike information criteria (AIC) values with additional PCA analysis on them, an approach presented in literature for the first time. The main trend (67.4% of variance) was connected with average fit. The second (14.8% of variance) is connected with differences of fitting ability to investigated dissolution curves. This methodology brought an overall look to trends and variances inside obtained data, both the profile shape and fitting ability to particular models. 相似文献
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采用湿法对沾化冬枣叶茶样进行消化处理,利用火焰原子吸收光谱法测定了茶中K、Na、Ca、Mg、Fe、Mn、Cu、Zn的含量.结果表明,该法的加标回收率为95.2%~104.2%,RSD≤3.35%.该法操作简单,结果准确,为开发和利用冬枣叶茶提供了一定的科学依据. 相似文献
46.
Let p(z) be a polynomial of degree at most n. In this paper we obtain some new results about the dependence of p(Rz)-βp(rz) + α (R+1/r+1)n-|β | p(rz) s on p(z) s for every α, β∈ C with |α|≤ 1, |β | ≤ 1, R > r 1, and s > 0. Our results not only generalize some well known inequalities, but also are variety of interesting results deduced from them by a fairly uniform procedure. 相似文献
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文献《On elementary bounds for∞∑k=n 1/ks》(American Mathematical Monthly,2015,122(2):155-158)给出了p-级数余项的一个估计,本文利用Taylor展开公式进一步改进了这个估计. 相似文献
49.
基于氧气A吸收带的baseline拟合距离反演算法 总被引:1,自引:0,他引:1
目标红外被动测距的实现同气体及其波段的选取密切相关。氧气A吸收带具有独特的谱线结构,对于火箭羽流或者高温辐射体的距离探测,氧气A吸收带是最佳的距离反演通道。利用该特点,详细研究了逐线积分算法(LBLRTM),并设计了氧气A带吸收系数及标准光谱计算软件;利用A吸收带吸收光谱带外数据,采用多项式拟合方法,实现基线(baseline)拟合,进而得到带平均透过率;在不同的距离条件下,将两种带平均透过率进行对比,误差在1.9%左右,拟合精度较高,该方法为后续距离的精确反演提供了理论依据。 相似文献
50.
大学物理教学的一个基本点是培养学生的空间想象力.麦克斯韦速率分布律是气体分子运动论的中心内容,是大学物理气体运动理论中讲授的一个难点,其公式抽象、繁难,学生不易理解.本文根据速度空间概念,给出速度球的表面积相当于气体分子微观状态数的观点,利用拉郎格日函数,推导理想气体平衡态下气体分子的速率分布函数.这种推导方法相对比较... 相似文献