邻硝基苯基荧光酮-氯代十六烷基吡啶双波长增敏法测定微量铁(Ⅲ)

在ＨＡＣ－ＮａＡＣ缓冲体系中,邻硝基苯基荧光酮、氯代十六烷基吡啶与铁形成三元络合物。试剂的最大吸收为５３０ｎｍ,络合物的最大吸收为６４４ｎｍ,用双波长增敏法测得表观摩尔吸光系数为５５×１０４络合物的组成比为１∶１∶１,铁量在０～６μｇ／２５ｍＬ符合比     

因子分析在企业增长方式评价中的应用

根据因子分析的基本原理 ,将企业生产要素划分为规模因子和效率因子 ,进而实现了企业增长方式的评价。     

无须极限新微分法

本文摆脱传统的除法 ,以括代除 ,无须极限也能求出切线 ,作出定理 A.由此微积分完全改观 .这是依靠实数有序“无漏”,建立强无穷小ω(Δx) ,取代ε-δ,实质又相互等价 ,作出定理 B.由ω(Δx)定义无穷小与连续 ,由连续再作极限更为自然 .聚点是极限的初步 ,大可发挥 .     

新型喷射制冷循环的研究

本文提出了利用双元工质在降低压缩比的同时降低蒸发温度的新型喷射制冷循环,由于双元工质低温域蒸发产生的双相流压缩过程也得到了圆满的解决;并且对R11取代物进行了研究．文中介绍了R123,R141b,R123／R141b,R123／R141b和R141b／R142b的实验及数据分析结果．实验结果显示了新型喷射制冷循环的优越性．     

序Banach空间中集值混合单调映象的耦合不动点定理

在序Banach空间中,研究了一类集值混合单调映象,用不同方法证明了两个新的耦合不动点存在性定理,所做工作扩充了文[5]的研究成果.     

PHOTOCONDUCTIVITY STUDY OF NEW POLYACETYLENE DERIVATIVES WITH DIFFERENT SUBSTITUENTS

The photoconductivities of a series of novel polyacetylene derivatives （PAs） serving as charge generation materials in the single-layered photoreceptors were investigated using photoinduced xerographic discharge technique. It was found that the substitution can improve the photosensitivity of PAs by increasing the conjugation of π electrons. When the substituent is itself photoconductive, the photoconductivity becomes even higher. It can be concluded from cyclic voltammetry that when the HOMO level of the polymer is closer to that of the charge transport material, the photoconduction performance will be better.     

TRANSAMIDATION IN THE in situ BLENDING OF POLYAMIDE 1212 WITH POLYAMIDE 6 THROUGH ANIONIC POLYMERIZATION OF CAPROLACTAM

20 wt% polyamide 12(PA1212)pellets were dissolved in molten caprolactam.The caprolactam was then catalyzed at 180℃and polymerized by means of anionic ring-opening polymerization to produce in situ blends of the resultant polyamide 6(PA6)and PA1212.Mechanical blends with same ingredient were prepared through melt blending on a twin-screw extruder.Scanning electron microscopy(SEM)observation revealed that contrary to the mechanical blends with small spherulites embedded in the matrix,no phase-separation existed in the in situ blends.The results of thermal analysis by differential scanning calorimetry(DSC)showed that single melting peak and crystallization peak existed for the in situ blends,while two melting and crystallization peaks appeared for the mechanical blends.The in situ blend film and the mixed blend film,both cast from a dilute formic acid solution with a concentration of 0.5 g/L,remained similar crystallization and melting behavior as above.It is proved by solution ~(13)C-NMR analysis that transamidation took place during the in situ blending,and it is suggested that the combination of temperature increasing and the basic surrounding derived from NaOH during polymerization resulted in the occurrence of transamidation.Furthermore,it is proposed that the interchange reaction between PA1212 and PA6 also resulted from the degradative reaction during the anionic polymerization.     

两指标局部鞅的停止变换及Wiener过程的鞅刻划

本文主要讨论两指标局部平方可积鞅的停止变换问题及Ｗｉｅｎｅｒ过程的鞅刻划和停止问题。     

Relationships between pure tail orderings of lifetime distributions and some concepts of residual life

The concepts of pure-tail orderings as defined by sq- and D-orderings are shown to order the family of reliability life distributions which age smoothly in a natural way. This ordering extends to comparisons regarding the limiting behavior of the residual life, mean residual life, sojourn time between perfect repairs in repairable systems, failure rate and, through the preservation of sq- and D-orderings by various reliability operations, to certain coherent systems of components that age smoothly. Possible applications of the results to the industrial practice of cannibalization are also noted.     

随机利率下的增额寿险模型研究

在实际的保险精算中,保单保险金现值函数的期望就是该种保单的纯保费,而方差常用来度量该种保单的风险.对随机利率采用W iener过程建模,得到了增额寿险保险金现值函数的期望和方差.