Synthesis and Photocytotoxicity of Mono-functionalised Porphyrin with Valine Moiety

A mono-funtionalised tetraphenylporphyrin (TPP) bearing valine moiety at the phenyl ring was synthesized for photocytotoxicity examination in four steps, starting from regiospecific mono-nitration of TPP at the phenyl ring. The in vitro photocytotoxicitic effect against SPC-Al adenocarcinona cell line was tested.     

2003年普通高等学校招生全国统一考试数学（理工农医类）（北京卷）

参考公式与文科相同一 选择题 :本大题共 1 0小题 ,每小题 5分 ,共 5 0分 .在每小题给出的四个选项中 ,只有一项是符合题目要求的 .( 1 ) ,( 2 )与文科 ( 1 ) ,( 2 )相同( 3)“cos2α=- 32 ”是“α=kπ+ 5π1 2 ,k∈Z”的(A)必要非充分条件(B)充分非必要条件(C)充分必要条件(D)既非充分又非必要条件( 4 )与文科 ( 4 )相同( 5 )极坐标方程 ρ2 cos2θ- 2 ρcosθ =1表示的曲线是(A)圆 (B)椭圆(C)抛物线 (D)双曲线( 6) ,( 7) ,( 8)分别与文科 ( 6) ,( 7) ,( 9)相同( 9)若数列 {an}的通项公式是an =3-n+ 2 -n+ ( - 1 ) n( 3-n- 2 -n)2 ,n…     

两个回归函数相等的Bootstrap检验

两个回归参数相等性检验一直是统计界感兴趣的问题之一．在这篇文章中，四个检验统计量被用于度量两曲线的差异，在原假设下统计量的分布采用向量数据的重复抽样来逼近，并给出了—些模拟结果．     

如何在大学数学课堂教学中培养学生创新思维

论述了在大学数学课堂教学中传授数学思想与数学方法的必要性与重要性 ,重点介绍了作者从大学数学教学中总结出来的一些数学思想与教学方法 .     

Multiple Scattering Effects of Ag Particles in Random Ag-SiN Film

A layer of 40nm-thick Ag-SiN film with Ag nano-particles embedded and distributed randomly in the SiN thin film were deposited by the method of radiant-frequency magnetron sputtering. Specimens orderly comprising a random Ag-SiN film and an optical phase change recording layer were exposed to a focused laser beam with wavelength of 69Ohm. It is shown that, with a random Ag-SiN layer deposited above the recording layer. Calculation by the finite difference time domain method of a 4Ohm-thick SiN film under a Gaussian beam irradiation has been carried out to simulate the near-field distribution in the film, which showed a huge local near-field intensity enhancement of about 200 times if small Ag particles with diameter of 6 nm were modelled inthe SiN film in the central region of the in cident laser spot.     

A Continuation Method of Parameter Inversion for Non-Equilibrium Convection-Dispersion Equation

Based on the homotopy mapping, a globally convergent method of parameter inversion for non-equilibrium convection-dispersion equations （CDEs） is developed. Moreover, in order to further improve the computational efficiency of the algorithm, a properly smooth function, which is derived from the sigmoid function, is employed to update the homotopy parameter during iteration. Numerical results show the feature of global convergence and high performance of this method. In addition, even the measurement quantities are heavily contaminated by noises, and a good solution can be found.     

NECESSARY CONDITIONS FOR OPTIMAL CONTROLS OF SEMILINEAR ELLIPTIC VARIATIONAL INEQUALITIES INVOLVING STATE CONSTRAINT

This paper deals with maximum principle for some optimal control problem governed by some elliptic variational inequalities. Some state constraints are discussed. The basic techniques used here are based on those in [1] and a new penalty functional defined in this paper.     

Bounds for the Least Laplacian Eigenvalue of a Signed Graph

A signed graph is a graph with a sign attached to each edge. This paper extends some fundamental concepts of the Laplacian matrices from graphs to signed graphs. In particular, the relationships between the least Laplacian eigenvalue and the unbalancedness of a signed graph are investigated.     

守恒方程的差分型格子气方法

给出了守恒型模型方程的差分型格子气方法，通过定义广义的分布函数，将原方程的求解问题化成关于分布函数的差分算法。该方法的意义在于建立格子气方法和差分法之间的联系，是而可以构造真正用于空气动力的格子气模型，使格子敢方法在可压缩领域成为一种实用方法。     

空间有源消声的微机控制

本文讨论用通用微机控制空间有源消声．以修正的PID（比例、积分、微分）算法加上逻辑判断构成的控制软件，使得系统收敛迅速，跟踪速度快，消声效果令人满意，而且系统工作稳定可靠，