分数填补下两非参数总体一般差异的经验似然置信区间

在一定的条件下证明了缺失数据情形基于分数填补方法得到的两非参数总体一般差异指标的经验似然比统计量的渐近分布为加权χ21,由此可构造差异指标的经验似然置信区间.     

Bernstein算子的点态同时逼近

借助光滑模ω_φ~2(f,t)(φ是一般步权函数),研究了Bernstein算子的点态同时逼近问题,给出了Bernstein算子同时逼近的等价定理,建立了其导数与光滑函数间的关系,对以前已有的结果予以补充和完善.     

随机插补下两线性模型中响应变量分位数差异的经验似然置信区间

设两个样本数据不完全的线性模型,其中协变量的观测值不缺失,响应变量的观测值随机缺失。采用随机回归插补法对响应变量的缺失值进行补足,得到两个线性回归模型的"完全"样本数据,在一定条件下得到两响应变量分位数差异的对数经验似然比统计量的极限分布为加权x_1~2,并利用此结果构造分位数差异的经验似然置信区间。模拟结果表明在随机插补下得到的置信区间具有较高的覆盖精度。     

Bootstrap approximation of wavelet estimates in a semiparametric regression model

The inference for the parameters in a semiparametric regression model is studied by using the wavelet and the bootstrap methods. The bootstrap statistics are constructed by using Efron＇s resampling technique, and the strong uniform convergence of the bootstrap approximation is proved. Our results can be used to construct the large sample confidence intervals for the parameters of interest. A simulation study is conducted to evaluate the finite-sample performance of the bootstrap method and to compare it with the normal approximation-based method.     

Determinations of plasma density and decay time in the hollow cathode discharge by microwave transmission

The microwave （MW） transmission method is employed to measure both the plasma density and the plasma decay time in the hollow cathode discharge （HCD） in argon at low pressure. The plasma density in DC-driven or pulsed HCD is on the order of 1012 cm-3, which can block the X-band MW effectively. In the case of pulsed HCD, the MW transmittance shows the same waveform as the pulsed current during the rising edge if the driving frequency is low, but with a longer delay during the falling edge. The MW transmittance reaches a constant low level when the driving frequency is high enough. The plasma decay time in the HCD system is measured to be about 100 μs around a pressure of 120 Pa. The ambipolar diffusion is considered to be the major mechanism in the decay process.     

微波辐照活性炭床同时脱除SO2和NOx实验研究

论文进行了微波辐照活性炭同时脱硫脱硝实验,研究了烟气中不同组分对脱硫脱硝效率的影响。结果表明,高浓度SO₂对脱硝有轻微抑制。NO对脱硫有一定程度的促进;烟气中O₂的加入对脱硫脱硝均有促进作用;而含湿量的增加首先会使脱硫脱硝效果提高,当含湿量增至9.1%时,脱硫脱硝效率均有下降趋势;烟气中加入CO₂后,脱硫脱硝效率均下降,在氧含量为10%时,脱硫效率下降6%,脱硝效率下降7%。BET测试表明,微波辐照活性炭后其表面积与基炭相比有少量下降。     

LiNO3热物性参数及热稳定性试验研究

介绍了太阳能热发电系统中的熔融盐传热蓄热介质,验证了文中试验测量方法的正确性;在此基础上完成了工业级LiNO3盐的物性参数的测定;同时测量了经过100多个加热冷却循环后的工业级LiNO3的热物性参数,将其与工业级LiNO3新盐的物性参数进行比较,结果表明,在100多个加热冷却循环后工业级LiNO3的热物性参数变化很小,热稳定性好.     

BaAl2O4催化同时去除NOx和碳烟的性能研究

BaAl2O4催化同时去除碳烟和NOx具有较高的活性.与非催化燃烧比,在BaAl2O4催化作用下,碳烟的起燃温度(tig)降低了175℃以上,最大燃烧温度(tm)降低了240℃以上.碳烟与BaAl204紧密接触、反应气体中O2含量越高、反应气体的总流量越低越有利于催化反应进行.通过漫反射红外光谱(DRIFTS)分析,证实了以单齿硝酸盐、离子硝酸盐和桥位硝酸盐的形式存在于BaAl2O4表面的NO2(ad)物种与碳烟的反应在同时去除碳烟和NOx的过程中起主要作用.     

碱熔-氢化物发生原子荧光光谱法连续测定锑精矿中的砷、铋、硒、锡

建立了氢化物发生原子荧光光谱法测定锑精矿中砷、铋、硒、锡的方法.研究了基体及共存元素的干扰情况,实验表明,在酒石酸、硫脲-抗坏血酸存在下,适当的增加酸度可以有效地消除干扰.采用Na2O2熔解样品,用HCl酸化,无需分离基体,实现了锑精矿中砷、铋、硒、锡的连续测定,其回收率为90.6%～103.8%,检出限分别为0.35、0.20、0.65和0.35 μg/L.应用该方法分析了锑精矿样品,结果令人满意.