A Vibrational Spectroscopy Study of “Urinary Sand”

Laser Raman Spectroscopy and FT-IR spectroscopy are used for the study of “urinary sand”. The examination of Raman spectra indicates the presence of struvite and apatite in the sample. The FT-IR spectrum is used to evaluate the relative concentration of apatitebtruvite components in the sample. The form of band profile may be correlated to the history of particle growth.     

Approximate Quantitation of Ascorbic Acid in Citrus and Tomato Juices with “Sandwich”-Indicator Sticks

Abstract

A rapid field-test of ascorbic acid content in fruit juices is feasible by the application of indicator papers capable for approximate quantitation.     

Dual representations of hulls for functions satisfying f (0) = inf f (X\{0}) *

Let Xbe a setW set of extended-real valued functions on Xand 0 an element of Xsuch that w(0) = 0 for all win W. We give a general theory of dual representations, without any extra parameters, of various hulls for extended-real valued functions on X satisfying f(0)= inf f(X\{0})We use the unifying framework of quasi-convex functions with respect to families of subsets of Xand a condition generalizing the bipolar theorem. Our results contain, as particular cases, some recent results of Thach (1991, 1993) and Rubinov and Glover (1996) on W-pseudo-affine and W-quasi-coaffine hulls.We also give some

results in the converse direction. These yield, in particular, that the bipolar theorem is equivalent to a certain property of the lower semi-continuous quasi-convex hulls of functions on locally convex spaces     

“三径”闭锁窗口模型的实验研究

 在解释CMOS器件辐射感应的闭锁窗口现象时，提出了所谓的“三径”闭锁窗口模型。在分析CMOS器件闭锁电路模型的基础上，简要介绍了“三径”闭锁窗口模型的有关情况。为了实验验证该模型，设计了实验电路以模拟CMOS器件的寄生闭锁路径，给出了相应的参数。“强光I”瞬时伽马辐照实验显示，实验电路像预计的那样出现了闭锁窗口。这说明，用“三径”模型解释某些闭锁窗口现象是合理的。     

新型荧光增强法检测水样品中碘离子

Hg2+可以猝灭核黄素的荧光,碘离子(I-)可以与Hg2+形成HgI2,基于此,发展了一种新型的荧光增强法检测水中I-的方法。Hg2+加入后,核黄素在525 nm处的荧光被猝灭;继续在体系中加入不同浓度的I-,体系中Hg2+被不断消耗,导致核黄素在525 nm处的荧光逐渐增强。该方法检测I-的线性范围在1-100μmol·L-1,检测限是0.4μmol·L-1;同时,该方法具有较快的响应时间(2 min);对其他卤素离子具有较好的选择性;用于水中I-检测时得到了较好的回收率。     

“LIVING-LIKE” CATIONIC POLYMERIZATION OF ISOBUTYL VINYL ETHER INITIATED BY CARBOXYL GROUPS ON CARBON BLACK SURFACE/ETHYLALUMINUM DICHLORIDE SYSTEM IN THE PRESENCE OF 1,4-DIOXANE

The effect of 1,4-dioxane as an added base on the cationic polymerization of isobutyl vinyl ether (IBVE) initiated by carboxyl groups on carbon black surface/ethylaluminum dichloride (EtAlCl₂) system was investigated. Although the cationic polymerization of IBVE by carbon black/EtAlCl₂ system the absence of 1,4-dioxane instaneously proceeded and the monomer conversion achieved 100% within a minute. The molecular weight distribution (MWD) of polyIBVE obtained was very broad. On the contrary, the MWD of polyIBVE obtained was very narrow and narrower than that obtained from the carbon black/ZnCl₂ initiating system by the addition of 1,4-dioxane. The number-average molecular weight (Mn) of polyIBVE obtained was directly proportional to monomer conversion in the cationic polymerization. However, the Mn of polyIBVE obtained from the polymerization by the initiating system in the the presence of 1,4-dioxane was smaller than that of the calculated value, assuming that polyl(IBVE) chain forms per unit carboxyl group on carbon black surface. It was concluded that carbon black/EtAlCl₂ initiating systems in the presence of 1,4-dioxane has an ability to initiate “living-like” cationic polymerization of IBVE based on the above results. PolyIBVE was grafted onto a carbon black surface after quenching the above “living-like” cationic polymerization systems with methanol.     

基于“桶中能量法”的相位共轭保真度测量研究

 给出了基于“桶中能量法”的相位共轭保真度测量原理、方法与结果。通过对适当大小的空间滤波针孔能量透过率的直接测量可以得到相位共轭保真度并简单实现系数 标定, 给出了针孔大小的选择原则、系数标定方法和共轭保真度的计算公式以及单池受激 布里渊散射相位共轭镜在几种条件下的实验结果, 指明了这种方法的重要性与不足之处。     

基于自制暗箱测量光电效应中光强与光电流的关系

本文基于自制的“暗箱”实验装置,通过3种方法来验证光电流与光强的关系:一是通过控制光电管两端的电压研究不同光强下光电管两端的伏安特性曲线;二是通过在相同光强下改变光电管与光源的距离研究光电管的光电特性曲线;三是通过光强传感器直接测定光电流与光强的关系.以上3种方法的实验数据均通过PASCO平台进行实时采集和分析,获得了未达到饱和时光电流随光强增加而增大的实验结果.     

Properties of the Zeros of the Sum of two Polynomials

Some properties—including relations having a Diophantine character—of the zeros of the sum of two polynomials are reported.