几种光学图象相位加密方法的比较

本文分析比较了多种实现光学图象相位加密的方法,发现不同方法获得的加密图象有不同类型的噪音分布.无论加密相位是随机相位模板、浑沌序列的相位列阵,还是用相位重构迭代算法计算的结果,它们都能起到加密图象的功能.解密图象的质量或被相关识别的能力与解密过程中所使用正确解密相位的不同部分以及高低频分量多少有关,且其依赖程度是由不同的加密方法自身决定.     

Data Envelopment Analysis of multiple response experiments

Taguchi method is the usual strategy in robust design and involves conducting experiments using orthogonal arrays and estimating the combination of factor levels that optimizes a given performance measure, typically a signal-to-noise ratio. The problem is more complex in the case of multiple responses since the combinations of factor levels that optimize the different responses usually differ. In this paper, an Artificial Neural Network, trained with the experiments results, is used to estimate the responses for all factor level combinations. After that, Data Envelopment Analysis (DEA) is used first to select the efficient (i.e. non-dominated) factor level combinations and then for choosing among them the one which leads to a most robust quality loss penalization. Mean Square Deviations of the quality characteristics are used as DEA inputs. Among the advantages of the proposed approach over traditional Taguchi method are the non-parametric, non-linear way of estimating quality loss measures for unobserved factor combinations and the non-parametric character of the performance evaluation of all the factor combinations. The proposed approach is applied to a number of case studies from the literature and compared with existing approaches.     

近红外漫反射光谱法测定玉米秸秆NDF与ADF含量

应用主成分空间和傅里叶变换近红外光谱技术,采用偏最小二乘回归法(PLS),在国内首次建立了适合不同品种类型、不同生长发育时期和不同部位且适配范围广的近红外漫反射光谱(NIRS)测定玉米秸秆中性洗涤纤维(NeutralDetergentFiber,NDF)和酸性洗涤纤维(AcidDetergentFiber,ADF)含量的稳定校正模型。结果表明,采用一阶导数 矢量归一化预处理和一阶导数 多元散射校正预处理,谱区均为7502～5450cm-1和4601～4247cm-1,所建立的NDF与ADF校正模型,其校正和预测效果最佳。其校正决定系数(R2cal)均大于094,交叉验证和外部验证决定系数(R2cv,R2val)为092～096,各项误差(RMSEE,RMSECV和RMSEP)为149%～181%。该结果对青贮玉米秸秆材料快速鉴定和筛选具有重要的意义。     

高强度三次谐波转换对光束质量的影响

分别利用光强对比度和功率谱密度作为激光束的振幅调制和位相畸变的定量描述参量,研究了在高功率条件下,三次谐波转换过程对激光光束质量的影响,详细分析了基频光的光束质量与三倍频光光束质量的定量变化关系.     

多孔建材中VOC扩散系数的两尺度模型

基于对建材微观结构的分析和压汞实验,提出了预测建材中有机挥发物(VOC)扩散系数的宏观一介观两尺度模型.和传统的从压汞实验计算扩散系数方法不同的是,本模型不仅考虑了孔隙率,还对孔的尺度分布和孔的连接方式进行了研究和分析.三种不同中密度板中VOC的散发实验表明,采用新模型计算的扩散系数比文献中的传统模型更好地吻合实验数据.     

激光诱导荧光探测水体中溶解有机物浓度

用Nd∶YAG激光器的三倍频355 nm光作为激发光源,根据激光诱导荧光(LIF)方法激发并探测污染水体的荧光光谱.通过对荧光光谱的分析处理研究归一化荧光强度,即450 nm处水中溶解有机物(DOM)峰与405 nm处水的拉曼峰的比值,反演溶解有机物浓度.用商品腐殖酸和去离子水配置成已知浓度的溶液代替标准DOM溶液进行标定,得到回归方程.结果证明,DOM的归一化荧光强度与水体中DOM浓度有较好的线性关系,因此LIF方法是对大面积水域水质进行动态遥测的较理想方法.     

Normal modes and quality factors of spherical dielectric resonators: I — shielded dielectric sphere

Electromagnetic theoretic analysis of shielded homogeneous and isotropic dielectric spheres has been made. Characteristic equations for the TE and TM modes have been derived. Dielectric spheres of radii of the order of μm size are found suitable for the optical frequency region whereas for the microwave region radii of the order of mm size are found suitable. Parameters suitable for their application in the optical and microwave frequency ranges have been used to compute the frequencies corresponding to the normal modes for the TE and TM modes. Expressions for the quality factors for realistic resonators, i.e., for a dielectric sphere with a non-zero conductivity and a metal shield with a finite conductivity have also been derived for the TE and TM modes. Computations of the quality factors have been made for resonators with parameters suitable for the optical and the microwave regions.     

Melting thermodynamics of oligonucleic acids conjugated with relatively solvophobic linear polymers: A coarse‐grained molecular simulation study

Oligonucleic acids (ONAs), such as DNA and RNA, are used in various biotechnology and nanotechnology applications due to their ability to form a double helix that is stable at low temperature and melts at high temperatures. The melting temperature (T_m) of ONA duplexes can be tuned by the ONA composition, sequence, length and concentration, solvent quality, and salt concentration and by conjugation to other macromolecules. In this article, we use coarse‐grained (CG) molecular simulations to study ONAs conjugated with linear homopolymers that are relatively more solvophobic than the ONA. We study charged and stiff 8‐mer ONAs (e.g., DNA) and neutral and flexible 8‐mer ONAs (e.g., peptide nucleic acids or PNA), and vary the composition (or G‐C content) and sequence of ONA, conjugated homopolymer lengths and solvent quality for the polymer. For neutral and flexible ONAs, as the solvent quality worsens for the polymer, the ONA melting temperature increases from that of unconjugated ONA. The melting curves broaden with polymer length and worsening solvent quality, especially for ONAs with higher G‐C content. For charged and stiff ONAs, as the solvent quality worsens, the ONA melting temperature decreases compared to unconjugated ONA while the width of the melting curve remains the same. © 2019 Wiley Periodicals, Inc. J. Polym. Sci., Part B: Polym. Phys. 2019 , 57, 1196–1208     

Stability-indicating RP-HPLC method development and validation for determination of nine impurities in apixaban tablet dosage forms. Robustness study by quality by design approach

A quality by design (QbD) based high-resolution HPLC method is described for determination of impurities in apixaban (APX) in the tablet dosage form. Employing a simple and stability-indicating HPLC method, nine known impurities were quantified with good peak resolution. Mobile phase A (MP-A) was prepared with buffer and acetonitrile 90:10 v/v, while mobile phase B (MP-B) contained water and acetonitrile 10:90 v/v. The gradient program was 0 min, MP-A 75%, B 25%; 20 min, MP-A 65%, B 35%; 30 min, MP-A 40%, B 60%; 40min, MP-A 40%, B 60%; 42 min, MP-A 75%, B 25%; and 50 min, MP-A 75%, B 25%. The chromatographic separation was achieved using a Zorbax RX C₁₈ 250 × 4.6 mm column, 5 μm (1.0 ml min⁻¹, 280 nm, 50 μl) and a column temperature of 40°C. Several separation studies were carried out using design of experiments to optimize the method. Validation results confirm the applicability of the developed method for quality analysis and stability studies of the regular product on the manufacturing stream.