Immersion behaviour of calcium polyphosphate in simulated body fluid

This work documents an investigation into the immersion behaviour of calcium polyphosphate (CPP) in simulated body fluid (SBF) for various periods. The results showed that with the increase of soaking time in SBF, a number of tiny particles were observed on the surface of samples by scanning electron microscope (SEM). The results of X-ray diffraction (XRD) indicated that the particles were contributed to apatite. And the changes of PO₄³⁻ and Ca²⁺ concentrations in SBF were detected by phospho-vanado-molybdate method and inductively coupled plasma atomic emission spectroscopy (ICP) methods respectively. The results indicated that the concentrations of PO₄³⁻ and Ca²⁺ in SBF reached the maximum value after 25 days of immersion, and then decreased with further increase of the soaking time. It is suggested that the degradation and ion exchange of CPP samples are dominant during the early stage of soaking, and then the precipitates begin to form and increase gradually as the soaking time increases. This study has demonstrated that apatite could be formed on the surface of CPP samples, and CPP would be used as bone substitution material.     

嵌入式三维数字成像系统

提出一种基于数字信号处理器(DSP)的嵌入式三维数字成像系统设计方案。该方案的硬件平台由条纹投影模块、数据采集模块、条纹自动分析模块及储存器等其他辅助电路组成。条纹投影模块将DSP输出的正弦光栅条纹, 经视频编码后用DLP投射到物体表面; 数据采集模块通过CCD相机采集被物体表面三维信息调制后的变形条纹图, 并进行视频解码; 条纹自动分析模块中利用相移算法计算折叠相位, 再结合相位展开算法求绝对相位分布。系统软件采用多线程技术并行控制三个模块。在相位解调过程中以软件流水线为主综合运用了循环展开、数据预取和内联函数等多种方法优化解调程序。实验结果表明, 该系统可以高速、准确地实现三维轮廓测量,优化后相位展开程序速度是优化前的7倍。     

甘草酸二铵与牛血清白蛋白相互作用的光谱

在模拟人体生理条件下,用常规荧光光谱和紫外－可见吸收光谱研究甘草酸二铵和牛血清白蛋白的相互作用机制,并利用同步荧光光谱和三维荧光光谱研究了药物对牛血清白蛋白构象的影响。研究表明,甘草酸二铵对牛血清白蛋白具有荧光猝灭作用,且为单一的动态猝灭过程。根据Stern-Volmer方程求出了两者相互作用的动态猝灭常数,并根据Förster非辐射能量转移理论确定了药物与蛋白的结合距离。     

胶体晶体模板法制备三维有序大孔复合氧化物*

胶体晶体模板法是制备三维有序大孔（3DOM）复合氧化物材料的有效方法。制备过程一般包括3个步骤：首先,将单分散微球堆积成三维有序排列的胶体晶体;其次,将液态前驱体填充到胶体晶体的间隙,并在原位转化为固体骨架;最后,将微球去除,在原来微球间的空隙位置得到固体骨架,原来微球占据的位置则成为相互连接的孔穴。其中,胶体晶体模板的组装、前驱体的填充以及模板的去除都是制备3DOM复合氧化物的关键影响因素。本文针对这几个控制因素对胶体晶体模板法制备3DOM复合氧化物的影响进行了概述,并对孔结构的表征以及材料在催化和电极材料等方面的应用作了简单介绍。     

Linear stability of three-dimensional boundary layers

Stability of compressible three-dimensional boundary layers on a swept wing model is studied within the framework of the linear theory. The analysis based on the approximation of local self-similarity of the mean flow was performed within the Falkner-Skan-Cooke solution extended to compressible flows. The calculated characteristics of stability for a subsonic boundary layer are found to agree well with the measured results. In the case of a supersonic boundary layer, the results calculated for a Mach number M = 2 are also in good agreement with the measured spanwise scales of nonstationary vortices of the secondary flow. The calculated growth rates of disturbances, however, are substantially different from the measured values. This difference can be attributed to a high initial amplitude of disturbances generated in the experiment, which does not allow the linear stability theory to be applied. The evolution of natural disturbances with moderate amplitudes is fairly well predicted by the theory. The effect of compressibility on crossflow instability modes is demonstrated to be insignificant. __________ Translated from Prikladnaya Mekhanika i Tekhnicheskaya Fizika, Vol. 49, No. 2, pp. 3–14, March–April, 2008.     

Spurious velocities in the steady flow of an incompressible fluid subjected to external forces

We show that a non-physical velocity may appear in the numerical computation of the flow of an incompressible fluid subjected to external forces. A distorted mesh and the use of a numerical method which does not rigorously ensure the incompressibility condition turn out to be responsible for this phenomenon. We illustrate it with numerical examples and we propose a projection method which improves the results. © 1997 John Wiley & Sons, Ltd.     

Calculation of vertical velocity in three-dimensional,shallow water equation,finite element models

Computation of vertical velocity within the confines of a three-dimensional, finite element model is a difficult but important task. This paper examines four approaches to the solution of the overdetermined system of equations arising when the first-order continuity equation is solved in conjunction with two boundary conditions. The traditional (TRAD) method neglects one boundary condition, solving the continuity equation with the remaining boundary condition. The vertical derivative of continuity (VDC) method involves solution of the second-order equation obtained by differentiation of the continuity equation with respect to the vertical co-ordinate. The least squares (LS) method minimizes the residuals of the continuity equation (in discrete form) and the two boundary conditions. The adjoint (ADJ) method minimizes the residuals of the continuity equation (in continuous form) and the two boundary conditions. Two domains are considered: a quarter-annular harbour and the southwest coast of Vancouver Island. Results indicate that the highest-quality solution is obtained with both LS and ADJ. Furthermore, ADJ requires less CPU and memory than LS. Therefore the optimal method for computation of vertical velocity in a three-dimensional finite element model is the adjoint (ADJ) method. © 1997 John Wiley & Sons, Ltd.     

半导体外延层晶格失配度的计算

比较了晶格失配度的各种定义,建议统一使用同一定义。采用简化模型系统地探讨了各种情况下半导体外延生长层和衬底的二维晶格失配度的计算,最后讨论了结合XRD衍射图谱确定失配度的方法。结果表明,正三角形晶格和长方形晶格匹配,长方形晶格的宽列原子的匹配具有优先性,不受长列原子匹配的影响。长方形的长宽比接近匹配比时,整体匹配较好。     

Simulation of bluff body stabilized flows with hybrid RANS and PDF method

The motivation of this study is to investigate the turbulence–chemistry interactions by using probability density function (PDF) method. A consistent hybrid Reynolds Averaged Navier–Stokes (RANS)/PDF method is used to simulate the turbulent non-reacting and reacting flows. The joint fluctuating velocity–frequency–composition PDF equation coupled with the Reynolds averaged density, momentum and energy equations are solved on unstructured meshes by the Lagrangian Monte Carlo (MC) method combined with the finite volume (FV) method. The simulation of the axisymmetric bluff body stabilized non-reacting flow fields is presented in this paper. The calculated length of the recirculation zone is in good agreement with the experimental data. Moreover, the significant change of the flow pattern with the increase of the jet-to-coflow momentum flux ratio is well predicted. In addition, comparisons are made between the joint PDF model and two different Reynolds stress models. The project supported by the National Natural Science Foundation of China (50506028), and Action Scheme for Invigorating Education Towards the twenty-first century.     

Construction and Verification of a Simple Smooth Chaotic System

This article introduces a new chaotic system of three-dimensional quadratic autonomous ordinary differential equations, which can display different attractors with two unstable equilibrium points and four unstable equilibrium points respectively. Dynamical properties of this system are then studied. Furthermore, by applying the undetermined coefficient method, heteroclinic orbit of (S)hil'nikov's type in this system is found and the convergence of the series expansions of this heteroclinic orbit are proved in this article. The (S)hil'nikov's theorem guarantees that this system has Smale horseshoes and the horseshoe chaos.