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41.
Summary The retention and selectivity of flavonoids (baicalin, baicalein, wogonin, oroxylin A) inScutellariae radix have been studies by high-performance thin-layer chromatography on phenyldimethylethoxysilane-treated silica plates. The silica plates treated with phenyl groups were used for physical and chemical analysis. From elemental carbon analysis, the maximum number of bonded phenyl surface groups per gram was calculated to be 0.467×1021 (Oginal silica plate: Merck Art. 15109, Silica gel 100 F254). With methanol-1/15 M phosphate buffer (pH 6.2) mixtures as mobile phase, baicalin, baicalein, wogonin, and oroxylin A inScutellariae radix were separated. It has been shown that phenyl-treated plates are more suitable for selective separation of baicalin, baicalein, wogonin, and oroxylin A than octadecyl-treated plates. 相似文献
42.
Styrene (St)-acrylic acid (AA) copolymer plates were synthesized in the frames made of glass, aluminum (Al) and poly(difluoroethylene) (PDFE). Surface properties of the prepared copolymer plates were characterized with regard to critical surface tension (
C
), chemical components by IR analysis and surface energies (total energy,
S
; dispersion force components,
S
d
; polar component,
S
p
; hydrogen bonding component,
S
h
) and the following results were obtained.The
C
values of the copolymer plates increased with AA content and also depended on the sort of the used frame. The increasing order of the
C
values of the copolymer plates corresponded to those of the used frames, namely, PDFE frame < Al frame < Glass frame.The prepared copolymer plates with low AA contents (ca. 10 mol%) were enriched in the AA moiety in the surface layer regardless of the kind of the used frame.The total and the individual components of the surface free energies of the copolymer plates were largely affected by the property of the used frame. The glass frame gave the plate with higher
S
h
values suggesting preferential orientation of the polar site of AA component. 相似文献
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47.
微通道板选通X射线皮秒分幅相机曝光时间的均匀设计 总被引:3,自引:2,他引:1
将均匀设计法应用于微通道板选通X射线皮秒分幅相机(MCP-XPFC)曝光时间的研究工作中,目的是找到一个简单高效的试验预估方法来指导分幅相机的研制和试验工作.基于分幅相机皮秒动态选通理论模型,建立了采用0.5 mm厚、长径比40的MCP的皮秒分幅相机选通脉冲参量与曝光时间之间的快速预估模型.利用这一模型得出了相机的曝光时间随选通脉冲脉宽和幅值分别呈抛物线变化,且脉宽和幅值对曝光时间具有交互影响作用.在试验参量范围内,此预估模型能够精确地代替相机理论模型和高效地指导实验.通过实验验证了预估模型,并分析了影响结果的因素. 相似文献
48.
Oblique perforation of thick metallic plates by rigid projectiles with various nose shapes is studied in this paper. Two perforation mechanisms, i.e., the hole enlargement for a sharp projectile nose and the plugging formation for a blunt projectile nose, are considered in the proposed analytical model. It is shown that the perforation of a thick plate is dominated by several non-dimensional numbers, i.e., the impact function, the geometry function of projectile, the non-dimensional thickness of target and the impact obliquity. Explicit formulae are obtained to predict the ballistic limit, residual velocity and directional change for the oblique perforation of thick metallic plates. The proposed model is able to predict the critical condition for the occurrence of ricochet. The proposed model is validated by comparing the predictions with other existing models and independent experimental data.The English text was polished by Keren Wang 相似文献
49.
本文发展一种功能梯度构件分析的细观元法.细观元法在构件的常规有限元内部设置密集观细单元以反映材料特性变化,又通过协调条件将各细观元结点自由度转换为同一常规有限元自由度,再上机计算.这种细观元法既能充分反映材料功能梯度沿各方向任意变化特性;而其计算单元又和常规有限元一样,是一种针对功能梯度结构分析的有效数值方法.现有功能梯度板件分析中无论对不同形状还是不同边界的功能梯度构件,其材料特性均沿板厚度方向梯度变化,本文用细观元法进行计算与分析,给出了目前尚未得到的沿板平面方向功能梯度变化构件的力学量三维分布形态. 相似文献
50.