Contributions to numerical developments in shock waves attenuation in porous filters

The paper deals with the numerical method of the compressible gas flow through a porous filter emphasizing the treatment of the interface between a pure gaseous phase and a solid phase. An incident shock wave is initiated in the gaseous phase interacting with a porous filter inducing a transmitted and a reflected wave. To take into account the discontinuity jump in the porosity between the gaseous phase and the porous filter, an approximate Riemann solver is used to compute homogeneous non-conservative Euler equations in porous media using ideal gas state law. The discretization of this problem is based on a finite volume method where the fluxes are evaluated by a “volumes finis Roe” (VFRoe) scheme. A stationary solution is determined with a continuous variable porosity in order to test the numerical scheme. Numerical results are compared with the two-phase shock tube experiments and simulations of a shock wave attenuation and gas filtration in porous filters are presented.      

Elasticoplastic Model of Sludge Injection into a Weak Water-Pressurized Reservoir

Sludge injection, i. e., injection of a mixture of water and solid particles (rock waste or drilling cuttings), can be interpreted as the penetration of a plastic mass into an elastoplastic water-pressurized stratum under the action of high gradients of the pore pressure. A system of elastoplastic deformation of a saturated porous medium describing the injection processes in both the sand formation and the zone occupied by sludge is formulated. An axisymmetric self-similar problem implying the frontal stable displacement of sand by sludge is considered. The chosen interval of variables and the results obtained correspond to the field experimental data.     

Changes of the affinity between fungal proteins and vanillin bonded to thermally modified porous glass support

Summary The affinity of peroxidase and the fungal proteins to vanillin attached to controlled porous glasses depends on the porosity of the glass and additional thermal treatment of the support. The additional thermal treatment of controlled porous glasses leads to an enrichment in boron atoms of their surface.The results presented in this paper show a better resolution of the analyzed substances when glass with a surface enriched in boron was used as the support for vanillin.     

Microstorms in cellular polymers: a route to soft piezoelectric transducer materials with engineered macroscopic dipoles.

Cellular polymers can be internally charged by "microstorms" (silent or partial discharges) within the voids of the polymer foam. The resulting material, which carries positive and negative charges on the internal void surfaces, is called a ferroelectret. Ferroelectrets behave like typical ferroelectrics, hence they provide a novel class of ferroic materials. The soft foams are strongly piezoelectric and can be used, in a wide range of applications, as transducers for interconverting mechanical and electrical signals. Herein, an overview is provided on the preparation of cellular polymers by physical foaming (extrusion, biaxial stretching, and controlled inflation by pressure treatments), on their charging by "microstorms", on their piezo- and pyroelectricity, and on analogies to ferroelectrics. Finally, a survey of selected applications is presented.     

Microstructure and Porosity of Silica Xerogel Monoliths Prepared by the Fast Sol-Gel Method

An adaptation of the fast sol-gel method to the synthesis of xerogel monoliths using tetramethoxysilane (TMOS) as the alkoxide precursor is described in this paper. The procedure involves running the reaction at 70–80°C in an open vessel, which accelerates hydrolysis and condensation and reduces the amount of liquid by expelling excess methanol through outdistillation. This procedure yields crack-free monoliths. The porosity and microstructure of these xerogel monoliths were studied by using N₂ adsorption and desorption and scanning electron microscopy (SEM). The SEM data show that the solid skeletal phase has a globular morphology with particles, 20–40 nm in diameter, arranged into agglomerates a few hundred nm in diameter. The microstructure of the acid-catalyzed xerogel is a consolidation of these agglomerates. The isotherm data show these xerogels to be microporous. In contrast, the base-catalyzed xerogel has a hierarchical morphology with the clusters of agglomerates organized into larger clusters approaching 1 m in diameter. An analysis of the isotherm data shows these xerogels to be less microporous with a narrow distribution of mesopores having an average diameter of 50 Å.     

A simple approach to porous low-temperature-sintering BaTiO3

Porous tetragonal BaTiO 3 ceramic was successfully prepared by a combination of hydrothermal and low-temperature-sintering method.The hollow TiO2@BaCO 3 as the sintering precursor was synthesized via a simple hydrothermal method,and then porous BaTiO 3 was generated by calcining the hollow TiO2@BaCO 3 precursor at 900 ℃ without additive.The hollow TiO2@BaCO 3 structure plays two important roles in the preparing of the porous BaTiO 3 ceramic.First,the TiO2@BaCO 3 hollow structure provides high surface areas and increases the contact points between BaCO 3 and TiO2,which can reduce the sintering temperature of the BaTiO 3 ceramic.Second,the cavity of the ordered arranged TiO2@BaCO 3 hollow sphere shows important influence on the porous structure,and the pore size of the as-prepared porous BaTiO 3 ceramic can be tuned from several nanometers to hundreds nanomters by changing the sintering temperature.The formation mechanism of the porous BaTiO 3 ceramic was proposed.     

裂缝性低渗透油藏流固耦合渗流分析

在低渗透油田的开发过程中，油藏流体渗流和储层岩土之间存在明显的耦合作用。本文首先研究给出了低渗裂缝性储层孔渗参数的等效方法，然后将渗流力学和岩土力学相结合，给出了低渗透裂缝性储层流固耦合渗流的数学模型，该模型不仅可以反映基质孔渗参数在开发中的变化，而且更能反映裂缝开度变化所引起的渗透率变化，而这对于低渗透裂缝性油田而言十分重要。最后对一实际井网进行了流固耦合油藏数值模拟，给出了开发过程中孔渗参数的变化及其耦合效应对油田开发的影响．     

铁合金和青铜多孔材料屈服应力的实验研究

对铁合金和青铜多孔材料做静态实验和Taylor冲击实验,得到静态屈服应力和孔隙率以及动态屈服应力和应变率的变化规律,同时将静动态载荷作用下的多孔材料的本构方程与实验结果进行了对比,发现理论分析和实验研究有良好的一致性,表明本文采用的模型基本能满足实际工程应用。     

THE RATE-INDEPENDENT CONSTITUTIVE MODELING FOR POROUS AND MULTI-PHASE NANOCRYSTALLINE MATERIALS

To determine the time-independent constitutive modeling for porous and multiphase nanocrystalline materials and understand the effects of grain size and porosity on their mechanical behavior, each phase was treated as a mixture of grain interior and grain boundary, and pores were taken as a single phase, then Budiansky's self-consistent method was used to calculate the Young's modulus of porous, possible multi-phase, nanocrystalline materials, the prediction being in good agreement with the results in the literature. Further, the established method is extended to simulate the constitutive relations of porous and possible multi-phase nanocrystalline materials with small plastic deformation in conjunction with the secant-moduli approach and iso-strain assumption. Comparisons between the experimental grain size and porosity dependent mechanical data and the corresponding predictions using the established model show that it appears to be capable of describing the time-independent mechanical behaviors for porous and multi-phase nanocrystalline materials in a small plastic strain range. Further discussion on the modification factor, the advantages and limitations of the model developed were present.     

回归分析方法在大庆葡西地区地层压力预测上的应用

本根据数理统计分析,应用渗流力学理论,结合油田实际生产资料,得出大庆探区西部葡西地区各压力系统的地层压力预测公式,经实际资料验证,相对误差在0.27～4.89%之间,效果较好,有力地指导了油田钻井、固井、射孔和试油等项工作。