柱形装药水中爆炸近场径向压力测试初探

 针对端面起爆柱形装药水中爆炸近场冲击波阵面呈现非球形传播的特点,采用分幅相机记录了炸药起爆36 μs内近场冲击波的传播情况,分析了冲击波在不同时间和不同位置的形状;采用两台高速扫描相机测量了侧边任意一点的冲击波速度,结合Rankine-Hugoniot关系,得到了冲击波阵面的压力;同时用LS-DYNA方法对侧边任意一点的压力进行了数值模拟,两者得到的结果基本一致。     

电炮加载下靶板的高速摄影技术研究

叙述高速摄影在电炮加载多层铝板实验中的应用情况,用普通高速摄影技术和激光阴影摄影首次得到双层和三层铝板在Mylar膜飞片碰撞靶板后形成碎片云的变化图像和靶板表面的微物质喷射发展过程,观察改变起爆系统充电电压、靶板厚度及靶板之间距离等不同条件下的高速碰撞现象,初步得到碎片云和微物质的运动速度等实验结果。     

Analysis of Multiple Melting of High-Speed Melt Spun Polylactide Fibers Based on Kinetic Modeling

Multiple melting behavior of high-speed melt-spun polylactide (PLA) fibers was investigated by temperature modulated differential scanning calorimetry (TMDSC) in the heating process with various modulation periods in the calorimeter. In the case of the as-spun PLA fibers taken-up at 1 km/min, a melting endothermic peak and a recrystallization exothermic peak appeared at the same peak temperature of 151°C in the reversing and non-reversing heat flows (RHF and NRHF), respectively, whereas at 168°C, an endothermic peak was observed in both the RHF and NRHF. On the other hand, the as-spun PLA fibers taken-up at a high-speed of 6 km/min showed the melting in both the RHF and NRHF, but the recrystallization behavior was not obvious in the NRHF at the shorter modulation period conditions. The obtained data were analyzed based on the kinetic modeling of melting proposed by Toda et al. The real and imaginary parts of the complex apparent heat capacity in the melting region showed a strong modulation period dependence for both the low- and high-speed spun fibers. The endothermic heat flow of melting was separated by extrapolating the frequency to zero. For the PLA fibers spun at 1 km/min, a set of melting and recrystallization peaks in the RHF and NRHF appeared even for the melting at 168°C. In other words, the simultaneous occurrence of melting and recrystallization was confirmed through this extrapolation. For the 6 km/min PLA fibers, the presence of an exothermic heat of recrystallization was clearly confirmed at a peak temperature of 164°C.     

环境风对高速列车气动噪声特性的影响分析

气动噪声随着列车运行速度的提高急剧增加,是高速列车噪声的重要组成部分。本文使用缩比为1:20的三车编组模型,通过三维瞬态延迟分离涡模型求解高速列车的外流场,分析了环境风对流场结构与声源特性的影响;之后使用FW-H方程进行噪声传播计算,分析了不同速度的环境风对高速列车气动声学行为特性的影响。结果表明：高速列车主要的噪声源分布在转向架附近,在环境风的影响下,列车背风侧声源强度高于迎风侧,列车底部声源强度增幅较大。10 m/s以内的环境风会改变高速列车在尾流区域的声学指向性,并使气动噪声增加2.1~8.7 dB。相关结论可以为高速列车气动声学设计等研究提供参考。     

An integrated approach of homogenization-ultrasound-assisted extraction followed by high-speed countercurrent chromatography for rapidly preparative separation naphthoquinones and diarylheptanes from Juglands mandshurica Maxim. exocarp

This research investigated the effectiveness of an integrated method for the extraction and separation of naphthoquinones and diarylheptanes from exocarp of Juglands mandshurica Maxim. (namely, green walnut husks). The target compounds were obtained by ultra-turrax homogenization (UTH) coupled with ultrasound-assisted extraction (UAE) technology followed by high-speed countercurrent chromatography (HSCCC). The UTH-UAE extraction method achieved higher efficiency with 2.49- and 2.36-fold to those by UAE, and 1.39- and 1.34-fold to those by UTH in a short time. HSCCC was adopted for further separation and purification; six target compounds, namely, regiolone (RE), juglone (JU), myricatomento-genin (MG), galleon (GA), 2-oxatrycyclo[13.2.2.13,7]eicosa-3,5,7(20),15,17,18-hexaen-10-16-diol (OE), and juglanin A (JA), were separated with more than 95.37% purities and more than 84.71% final recovery rates, respectively. In this study, the integrated strategy of extraction and separation could get high purity compounds quickly, which would provide time and solvent saved method for the natural products separation from plants.     

Isolation and purification of high polar glycosides from aerial parts of Gynostemma pentaphyllum (Thunb.) Makino by linear gradient counter-current chromatography coupled with inner-recycling mode

Gynostemma pentaphyllum (Thunb.) Makino represents the popular health food and supplemental product with broad pharmacological activities. The highly polar glycosides, including flavonoids and saponins, are major effective active components that contain diverse sugar positions and quantities, which result in diverse chemical polarities, making it challenging to separate and isolate these components. The present work described the rapid and efficient linear gradient counter-current chromatography to preparatively separate glycosides from aboveground parts of G. pentaphyllum. Besides, the ethyl acetate and n-butanol binary mobile phases were achieved through adjusting associated proportions. Six glycosides, including quercetin-3-O-neohesperidoside ( 1 ), kaempferol-3-O-robinobioside ( 2 ), kaempferol-3-O-neohesperidoside ( 3 ), gypenoside LVI ( 4 ), ginsenoside Rb3 ( 5 ), and gypenoside XLVI ( 6 ), were isolated at the purities greater than 98%. Moreover, electrospray ionization mass spectrometry and nuclear magnetic resonance tandem mass spectrometry were conducted for structural identification. According to our findings, the established linear gradient counter-current chromatography was an efficient approach to separate the highly polar glycosides from aboveground parts of G. pentaphyllum. Our proposed strategy can be used to separate active compounds from other complex natural products.