高g值加速度计的设计与冲击特性分析

针对特殊场合的测试需求,设计了四端全固支的高过载梁岛结构加速度计;利用Hopkinson杆冲击校准装置对该加速度计的动态特性进行了测试。测试结果表明,传感器的灵敏度为1.2V/g,线性度5%左右;结构受到2105g冲击后完好且输出信号正常,能有效满足高冲击、强烈振动场合的特殊测试要求,可以应用于侵彻系统。 更多还原     

分子印迹固相萃取搅拌棒的制备及对复杂样品中双烯雌酚和己烷雌酚的萃取性能

以己烯雌酚为替代模板,利用整体材料的“原位”合成技术制备了分子印迹聚合物,并将其作为固相萃取搅拌棒的涂层(MIP-SBSE)制备了新的搅拌棒。详细考察了分子印迹聚合物制备条件中模板分子及功能单体用量对MIP-SBSE选择性萃取性能的影响,同时利用元素分析、扫描电镜和红外光谱对聚合物进行表征。以双烯雌酚(DS)和己烷雌酚(HS)为目标化合物,将MIP-SBSE与高效液相色谱-二极管阵列检测器联用,建立起复杂样品中DS和HS的分离分析方法。考察了吸附和解吸时间、解吸溶剂、离子强度和样品pH值等萃取条件对MIP-SBSE选择性萃取性能的影响。结果表明,在最佳萃取条件下,MIP-SBSE对DS和HS具有较高的选择性萃取性能,线性范围分别为1.0～400.0 μg/L和5.0～400.0 μg/L,利用氮吹再定容的方法,对DS和HS的检出限(S/N=3)分别可低至0.04和0.14 μg/L。在对实际污水、蜂蜜和牛尿样品的分析中取得了良好的加标回收率,其值为61.3%～120%。所建方法具有简便、高选择性和灵敏等特点,可用于复杂样品中双烯雌酚和己烷雌酚的分析监测。     

超薄柔性透射型超构材料吸收器

设计并加工了一种超薄柔性透射型吸收器,总体厚度为0.288 mm,可实现柔性弯曲,容易做到与曲面目标共形.该吸收器由三层结构组成,底层是金属光栅,中间为介质层,表面单元由两条平行放置的尺寸不同的金属线组成.仿真和实验结果表明,对横电波在5和7 GHz的吸收分别达到97.5%和96.0%,对横磁波在3.0—6.5 GHz都能保持90%以上的透射率.两个吸收频点可分别独立调节,增加了设计的灵活性.另外,当入射角增大到60°时,该吸收器的性能基本不受影响,表现出良好的广角特性.     

A Pulse-Heated Kolsky Bar Technique for Measuring the Flow Stress of Metals at High Loading and Heating Rates

The National Institute of Standards and Technology (NIST) has developed an electrical pulse-heated Kolsky Bar technique for measuring the constitutive response of metals at heating rates of up to 6,000 K/s and strain rates up to 10⁴ s⁻¹. Under these conditions, which are approaching those found in high speed machining, thermally activated microstructural processes such as grain growth, solid state phase transformation and dislocation annealing can be bypassed, leading to unique non-equilibrium superheated microstructural states. Flow stresses can thus differ significantly from equilibrium high temperature conditions. This paper describes the NIST pulse-heated Kolsky bar technique in detail, including a thorough assessment of uncertainties in temperature and flow stress measurement.

晶粒度对纯铝动态力学性能的影响

通过热处理方式制备了3种不同晶粒度的纯铝样品。利用分离式霍普金森压杆加载装置测量了3种纯铝在应变率102～104 s-1范围内的应力应变曲线。实验曲线表明,纯铝的屈服应力和流动应力随晶粒度的增大而减小;根据实验数据拟合了纯铝在动态下的Hall-Petch公式。同时采用一级轻气炮对3种纯铝进行了层裂实验,结果表明晶粒度对纯铝的层裂特性几乎没有影响。     

RRR-PRP平面六杆Ⅱ级机构的运动学仿真

以机构的组成原理为出发点,以应用最为广泛的RRR-PRP平面六杆机构为分析对象,采用复数向量推导出曲柄、RRRⅡ级杆组、PRPⅡ级杆组三个基本模组的运动学数学模型,利用其组成机构杆组并搭建平面连杆机构的运动学仿真模型,充分利用MATLAB的S imu link仿真模型数据可视化的特点观察     

单烯烃分子结构有限元方法及定量结构-沸点相关性研究

按照有限元方法, 将烯烃分子中的“C—C”单键和“C＝C”双键当作两种不同的线性杆元处理, 构建单烯烃分子的刚度矩阵, 连同质量矩阵求解相应的特征方程, 得到单烯烃分子的结构特征参量——固有频率, 将其用于定量结构-沸点预测模型, 对150个单烯烃分子的沸点实验测定值进行多元回归分析, 结果表明, 单烯烃分子结构与沸点性质间存在高相关性, 说明该方法是合理可行的.     

High Power 940 nm Al-free Active Region Laser Diodes and Bars with a Broad Waveguide

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TGSA-Flex: Extending the capabilities of the Topo-Geometrical Superposition Algorithm to handle flexible molecules

In this work, an extension of the already studied Topo-Geometrical Superposition Approach (TGSA) is presented. TGSA, a general-purpose, fast, automatic, and user-intuitive three-dimensional molecular alignment procedure, was originally designed to superpose rigid molecules simply based on atomic numbers, molecular coordinates, and connectivity. The algorithm is further developed to enable handling rotations around single bonds; in this way, common structural features, which were not properly aligned due to conformational causes, can be brought together, thus improving the molecular similarity picture of the final alignment. The present procedure, implemented in Fortran 90 and named TGSA-Flex, is deeply detailed and tested over four molecular sets: amino acids, nordihydroguaiaretic acid (NDGA) derivatives, HIV-1 protease inhibitors, and 1-[2-hydroxyethoxy)methyl]-6-(phenylthio)thymine (HEPT) derivatives. TGSA-Flex performance is evaluated by means of computational time, number of superposed atoms (also comparing it with respect to the rigid approach), and index of fit between the compared structures.     

Semiclassical $$\bar \partial $$ -Method: Generating Equations for Dispersionless Integrable Hierarchies

We use the semiclassical -dressing method to derive compact generating equations for dispersionless hierarchies. The considered illustrative examples are the dispersionless Kadomtsev–Petviashvili and two-dimensional Toda lattice hierarchies.