同轴电喷法制备PCL-蛋清体系复合微胶囊

以鸡蛋的卵清蛋白作为蛋白质药物模板、生物可降解材料聚己内酯(PCL)为药物载体模板,采用同轴电喷法制备PCL-蛋清体系的复合微球.研究了电导率、黏度对于电喷微球成型的影响.核壳溶液推进速率比、电压、溶液质量分数和接收距离等对于所得微球表面形态和结构的影响.利用扫描电子显微镜(SEM)研究了微球的表面形态,用荧光显微镜表征了微球的包覆模式.结果表明:同轴电喷法可以制备PCL-蛋清体系的复合结构微胶囊,其中推进速率比对微球形貌、粒径及其分布的影响比较明显,当PCL与蛋清溶液推进速率比大于10时,将出现具有包覆结构的微球.     

Initiation of Light Pulses by a Coaxial H‐Compressed Discharge

An optimum configuration of the discharge channel of a coaxial Hcompressed discharge is determined to exclude the screening influence of an envelope on discharge radiation in the UV region of a spectrum. It is shown that the use of an Hcompressed discharge of coaxial shape makes it possible to increase the radiation yield in the UV spectrum as compared to a plane shape at the same parameters of electric power supply.     

Use of an injection port for thermochemolysis–gas chromatography/mass spectrometry: Rapid profiling of biomaterials

A simple and direct approach was developed for thermochemolytic analysis of a wide range of biomolecules present in plant materials using an injection port of a gas chromatograph/mass spectrometer (GC/MS) and a novel solids injector consisting of a coiled stainless steel wire placed inside a modified needle syringe. Optimum thermochemolysis (or Thermally Assisted Hydrolysis/Methylation) was achieved by using a suitable methanolic solution of trimethylsulfonium hydroxide (TMSH) or tetramethylammonium hydroxide (TMAH) with an injection port temperature of 350 °C. Intact, methylated flavonoids, saccharides, phenolic and fatty acids, lignin dimers and diterpene resin acids were identified. Samples include tea leaves, hemicelluloses, lignin isolates and herbal medicines. Unexpected chromatographic results using TMAH reagent revealed the presence of intact methylated trisaccharides (658 Da) and structurally informative dimer lignin markers.     

Multifarious injection chamber for molecular structure study (MICOSS) system: development and application for serial femtosecond crystallography at Pohang Accelerator Laboratory X‐ray Free‐Electron Laser

The multifarious injection chamber for molecular structure study (MICOSS) experimental system has been developed at the Pohang Accelerator Laboratory X‐ray Free‐Electron Laser for conducting serial femtosecond crystallography. This system comprises several instruments such as a dedicated sample chamber, sample injectors, sample environment diagnostic system and detector stage for convenient distance manipulation. Serial femtosecond crystallography experiments of lysozyme crystals have been conducted successfully. The diffraction peaks have reached to ～1.8 Å resolution at the photon energy of 9.785 keV.     

再谈"三维导体"的自感系数

由公式ε＝Ｌ│ｄＩ／ｄｔ│出发，只要求出“三维导体”中的等效自感电动势，即可求得自感系数Ｌ，并以无限长同轴电缆自感系数的求解为例加以证明。     

光纤—自聚焦棒—反射器耦合系统的后向耦合系数

用光线矩阵方法推导了光纤-自聚焦棒-反射器在共轴耦合情况下的后向耦合系数;分析了它与耦合系统结构参数之间的关系.用计算机模拟画出了反射器为平面镜的系统的后向耦合系数和后向耦合损耗的曲线分布,计算曲线与实验结果大致符合.     

强流相对论电子束的数值模拟

我们研制了CEBQ程序和ENVLOP程序，模拟稳态相对论电子束在二极管区的产生和加速，以及电子束在阳极通道内的传输过程。CEBQ程序模拟二极管区电子轨道，当阳极电压为1．5MV时，阴极总发射电流为17．9kA，进入阳极通道内的传输电流为4．3kA，阳极入口处D=4cm的束发射度为24．9cm．mrad。ENVLOP程序使用线性近似下的包络方程，描述电子束包络在螺旋管引导磁场作用下的变化，讨论了外加引导磁场对包络的影响。计算结果表明，在合适引导磁场作用下，束包络起伏较小，进入阳极通道的束流(4．3kA)能全部通过。     

LIA组元的脉冲功率调制系统研制

本文介绍一种以加速组元为终端负载的纳秒脉冲功率系统。获得的加速间隙电压为350kV，90ns(半高宽)，波形上升时间为30ns；Blumlein主开关工作电压大于280kV，抖动小予1.5ns(均方根值)。对同轴场畸变开关性能的进一步改善作了必要的讨论，提出了用等场强原则偏置触发极，比通常采用自然中位面方法，可使开关工作电压提高8．7％。     

五轴加工中心范成铣磨离轴非球面研究

离轴非球面作为非球面的一部分,是空间光学系统、天文学和高精度测量系统不可或缺的光学器件.针对空间光学对离轴非球面光学元件制造技术的重大需求,开展了离轴非球面反射镜的精密铣磨加工技术研究.分析了五轴联动范成法铣磨离轴非球面的原理,将离轴非球面所在的同轴母镜离散为一系列不同半径的球面环带,将工件坐标系建立在待加工离轴非球面...     

直接观测法塞曼效应实验系统的优化调整

提出了塞曼效应实验仪调整中系统优化的理念,给出了直接观测法塞曼效应实验系统的优化方法.