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171.
In this paper, we investigate the existence of finitely optimal solutions for the Lagrange problem of optimal control defined on [0, ) under weaker convexity and seminormality hypotheses than those of previous authors. The notion of finite optimality has been introduced into the literature as the weakest of a hierarchy of types of optimality that have been defined to permit the study of Lagrange problems, arising in mathematical economics, whose cost functions either diverge or are not bounded below. Our method of proof requires us to analyze the continuous dependence of finite-interval Lagrange problems with respect to a prescribed terminal condition. Once this is done, we show that a finitely optimal solution can be obtained as the limit of a sequence of solutions to a sequence of corresponding finite-horizon optimal control problems. Our results utilize the convexity and seminormality hypotheses which are now classical in the existence theory of optimal control.This research forms part of the author's doctoral dissertation written at the University of Delaware, Newark, Delaware under the supervision of Professor Thomas S. Angell.  相似文献   
172.
In this paper, on the basis of Young's method (Ref. 1), sufficient conditions for a strong relative minimum in an optimal control problem are given. Young's method generalizes geodesic coverings and the simplest Hilbert integral from the standard variational calculus. This paper carries Young's method over to nonparametric problems.  相似文献   
173.
为研制司帕沙星软膏,建立其含量测定方法。用差示紫外分光光度法在306nm外测定司帕沙星的含量。平均回收率为99.98%,RSD为0.72%,线性范围15.62-40.14μg/ml。该法简便、准确、快捷。  相似文献   
174.
用转换器和IBMPC/XT微机与Dionex2020i型离子色谱仪连接组成自动控制与数据处理系统,转换器由8031及8255等芯片组成,其功能是采集数据和转送数据,软件由汇编及C语言编制。这套新系统增加了注入/记录同步,分级梯度淋洗,自动连续进样等功能以及很强的数据处理能力。  相似文献   
175.
Chromatographic purification of the alcoholic extract from the aerial parts of the Saudi plant Nuxia oppositifolia (Hochst.), Benth., resulted in five isolated phenolic compounds. Two flavones, hispidulin (1) and jaceosidin (2), and the phenylethanoid glycosides, verbascoside (3), isoverbascoside (4), and conandroside (5), were identified and their chemical structures were determined by spectroscopic analyses. The insecticidal activity of compounds 1 and 2, in addition to 11 compounds isolated in a previous research (6–16), was evaluated against the Yellow Fever mosquito, Aedes aegypti. Four compounds displayed adulticidal activity with LD50 values of 2–2.3 μg/mosquito. Free radical scavenging properties of the plant extracts and compounds (1–5) were evaluated by measuring the 1,1-diphenyl-2-picrylhydrazyl radical (DPPH) and 2,2′-azino-bis (3-ethylbenzothiazoline-6-sulfonate radical cation (ABTS•+) scavenging activity. All compounds exhibited notable activity, compared with the positive control, l-Ascorbic acid. This study suggests that N. oppositifolia could be a promising source of secondary metabolites, some with lethal adulticidal effect against Ae. aegypti.  相似文献   
176.
中药配方颗粒红外光谱法的快速鉴别   总被引:14,自引:0,他引:14  
周群  李静  孙素琴  梁曦云 《分析化学》2003,31(3):292-295
采用红外光谱法对中药配方颗粒及其辅料进行了鉴别研究。结果表明:不同生产厂商的配方颗粒中所添加的辅料类型及用量有较大差别;不同种的配方颗粒在辅料含量较低的情况下有较明显的指纹性,而辅料含量较高时,采用差谱技术可以提高谱图的指纹性,达到中药配方颗粒--鉴别的目的。该法简便、快速、可靠,是中药配方颗粒宏观质控的一个强有力的手段。  相似文献   
177.
缓慢炭化部分氧化对制备煤质活性炭的影响   总被引:5,自引:0,他引:5  
研究了炭化升温速度、炭化低温区引入空气部分氧化对活性炭制备过程中炭化阶段、炭化物结构、活性炭性能等的影响。结果表明,炭化时低温部分氧化可提高炭化物得率,使炭化物微晶的d002值升高和Lc值减小;而较慢的炭化升温速度有利于制备优质活性炭。缓慢炭化、部分氧化可以在一定程度上控制炭化路径,使炭化向生成取向性差、难石墨化、各向同性、呒定形炭多的炭化物的方向进行;并讨论了它们控制炭化的作用机理。以此为指导,  相似文献   
178.
The structure of iron oxide was controlled by regulating the hydrolytic polymerization of aquo iron complexes with organic polydentate ligands such as diols. Iron oxides were prepared by calcining the precursor polymers obtained from iron nitrate nonahydrate and diols. When the diols were 1,2-pentanediol, 1,2-hexanediol and 1,2-octanediol, α-Fe2O3 with corundum structure appeared exclusively or as the main crystalline phase, in spite of the amount of diol used and the calcination temperature. In the case of 1,2-decanediol and 1,2-dodecanediol, when five moles of the diols were used to one mole of iron nitrate and the calcination temperatures were below 400°C, ψ-Fe2O3 with spinel structure appeared as the main phase and, when less than five moles of the diols were used, α-Fe2O3 appeared exclusively or as the main phase, irrespective of the calcination temperature. This tendency was also observed in thin films. Thus, a transparent magnetic film composed of γ-Fe2O3 could be prepared by applying a benzene solution of the iron polymer, obtained with 5 equivalents of 1,2-decanediol, on quartz and calcining the gel film at 350°C.  相似文献   
179.
 Noble metal nanoparticles were prepared by the in situ reduction of the respective metal salt precursors in the presence of various protective polymers. Transmission electron microscopy (TEM) has been used to determine the particle shapes and morphologies. These are strongly influenced by the reduction methods and conditions chosen, but the choice of the protective polymer is equally important for controlling the particle morphologies and for the stabilization of the colloids. A whole spectrum of nanoparticle morphologies and shapes was obtained, ranging from nanoagglomerates which are nevertheless well-defined and well-stabilized to nanosized single crystals with triangular shape. Received: 2 February 1998 Accepted: 29 May 1998  相似文献   
180.
利用商品化ITO玻璃导电层的温阻效应, 无需任何微加工手段, 实现了自加热和传感的芯片温度自动程序控制, 最大程度地减小了传感滞后对温度控制稳定性的影响, 温度控制的稳定性达到了0.2 ℃, 升温速度最快可达20 ℃/s以上, 在冷却风扇辅助下降温速度最快达到了8 ℃/s. 芯片温控单元的引线从传统的两对(一对用于传感, 一对用于加热)减少为一对. 通过在该芯片上直接构建多个开放微池反应器的方法成功地实现了λDNA 157 bp片段的并行扩增. 将该芯片置于倒置荧光显微镜样品台上, 以蓝色(575 nm)发光二极管为光源, 以光电倍增管为检测手段检测了dsDNA和SYBR Green Ⅰ嵌合物的荧光强度随温度的实时变化曲线.  相似文献   
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