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61.
X射线递变能量成像是依次获取复杂结构件在递变能量下的局部有效信息,并通过多谱融合获取完整结构信息。但是目前的能量选择主要以人工设定管电压步进为主,无法匹配检测对象的有效厚度变化率,成像效率及射线利用率较低。基于递变能量成像规律,提出一种最佳X射线管电压预测算法。该方法通过对检测物体进行变能量预扫描,提取图像序列中有效厚度(高质量区域)和临近厚度(预测区域),建立有效厚度的图像灰度与管电压、X射线光谱之间的物理模型,及临近厚度灰度差与电压的函数模型,进而得到临近厚度最佳成像时的能量预测模型。通过模型求解,实现了能量的自适应预测。以不同厚度钢块为对象,利用该算法逐一预测各个厚度钢块最佳成像时的管电压,并与实际值对比。实验结果显示,在低能时可跨3~4 mm准确预测,高能时可跨7~10 mm预测,精度可以达到95%以上。 相似文献
62.
Image deconvolution analyses showed that reversion of S-Al2CuMg precipitates occurred in an Al–Cu–Mg alloy during high-resolution transmission electron microscopy observations. A fraction of Mg and Cu atoms in the precipitates diffused into Al matrix due to electron beam irradiation at 300 kV, resulting in structural/chemical reversion of the precipitates. The structural reversion of the S-Al2CuMg precipitates is closely related with irradiation-induced displacement of atoms. The strong attraction between Cu and Mg atoms might assist the sub-threshold displacement of Cu atoms. One transitional structure is determined to be S′′-Al10Cu3Mg3, a precursor of S-Al2CuMg. Two other transitional structures, Al3CuMg and Al18Cu5Mg5 which have the same lattice parameters of a = c = 0.405 nm as that of S′′-Al10Cu3Mg3, but different b values, are suggested. 相似文献
63.
J.L. Gunjakar 《Applied Surface Science》2008,254(18):5844-5848
The present investigation is related to the deposition of single-phase nano-sheets spinel nickel ferrite (NiFe2O4) thin films onto glass substrates using a chemical method. Nano-sheets nickel ferrite films were deposited from an alkaline bath containing Ni2+ and Fe2+ ions. The films were characterized for their structural, surface morphological and electrical properties by means of X-ray diffraction (XRD), transmission electron microscope (TEM), Fourier transform infrared spectroscopy (FT-IR), scanning electron microscopy (SEM), and two-point probe electrical resistivity techniques. The X-ray diffraction pattern showed that NiFe2O4 nano-sheets are oriented along (3 1 1) plane. The FT-IR spectra of NiFe2O4 films showed strong absorption peaks around 600 and 400 cm−1 which are typical for cubic spinel crystal structure. Microstructural study of NiFe2O4 film revealed nano-sheet like morphology with average sheet thickness of 30 nm. The room temperature electrical resistivity of the NiFe2O4 nano-sheets was 107 Ω cm. 相似文献
64.
D.M. Rajkumar M. Manivel RajaR. Gopalan V. Chandrasekaran 《Journal of magnetism and magnetic materials》2008
Evolution of structure and magnetocaloric properties in ball-milled Gd5Si2Ge2 and Gd5Si2Ge2/0.1 wt% Fe nanostructured powders were investigated. The high-energy ball-milled powders were composed of very fine grains (70–80 nm). Magnetization decreased with milling time due to decrease in the grain size and randomization of the magnetic moments at the surface. The magnetic entropy change (ΔSM) was calculated from the isothermal magnetization curves and a maximum value of 0.45 J/kg K was obtained for 32 h milled Gd5Si2Ge2 alloy powder for a magnetic field change of 2 T while it was still low in Fe-contained alloy powders. The thermo-magnetic measurements revealed that the milled powders display distribution of magnetic transitions, which is desirable for practical magnetic refrigerant to cover a wide temperature span. 相似文献
65.
66.
Ailin Xia Chuangui JinDexin Du Guohui Zhu 《Journal of magnetism and magnetic materials》2011,323(12):1682-1685
We prepared NiZnCu ferrite powders with nominal composition Ni0.4−xZn0.6CuxFe2O4 (x=0-0.2) via chemical coprecipitation method with NaOH and Na2CO3 as coprecipitators. The structural and magnetic properties of these compounds were studied and compared. It is found that all the specimens exhibit single-phase structure after annealing. The saturation magnetization of specimens with NaOH as coprecipitator is lower than that with Na2CO3 as coprecipitator. It is also found that the growth of grains is hindered for specimens using Na2CO3 as coprecipitator. 相似文献
67.
Glasses in the system Ge-Se-S were prepared with different Se/S ratios in order to investigate the compositional dependence of selected physical properties. We report the results of a systematic study examining the UV-vis transmission, dc electrical conductivity and X-ray diffraction of the system Ge(SxSe1−x)2 with x=0, 0.1, 0.4 and 1.0 where replacement of S by Se was made. The changes in the optical energy gap, Eg, (from 1.95 to 2.43 eV) and band tail width, Ee, (from 103 to 243 meV) behave contrarily to the change in refractive index, n, (from 2.3 to 2) with the progressive replacement of S by Se. This behavior was discussed and interpreted with the changes in cohesive energy. The analysis of defects in the prepared films was carried out by the examination of activation energies obtained from dc electrical conductivity. The analysis of the X-ray diffraction pattern revealed a remarkable reduction in the intensity of the first and second diffraction peaks with the progressive replacement of S content, which confirms a change in the intermediate range order structure: reorganization of the structural properties. 相似文献
68.
69.
B. Ghebouli M.A. Ghebouli T. Chihi M. Fatmi S. Boucetta M. Reffas 《Solid State Communications》2009,149(47-48):2244-2249
We present structural, elastic, electronic and optical properties of the perovskites SrMO3 (M=Ti, and Sn) for different pressure. The computational method is based on the pseudo-potential plane wave method (PP-PW). The exchange-correlation energy is described in the generalized gradient approximation (GGA). The calculated equilibrium lattice parameters are in reasonable agreement with the available experimental data. This work shows that the perovskites SrTiO3, and SrSnO3 are mechanically stable and present an indirect band gaps at the Fermi level. Applied pressure does not change the shape of the total valence electronic charge density and most of the electronic charge density is shifted toward O atom. Furthermore, in order to understand the optical properties of SrMO3, the dielectric function, absorption coefficient, optical reflectivity, refractive index, extinction coefficient and electron energy-loss are calculated for radiation up to 80 eV. The enhancement of pressure decreases the dielectric function and refractive indices of SrTiO3 and SrSnO3. 相似文献
70.