具有区域极点约束的柔性梁鲁棒H∞振动主动控制

本文基于H∞控制理论研究了传感器和作动器非同位配置情况下,柔性悬臂梁的多模态振动抑制问题。采用频域辨识方法获取低阶名义模型,合理选取加性不确定权函数和性能权函数,将鲁棒H∞控制问题转化为标准H∞控制问题。为了避免H∞控制器设计过程中产生的零极点对消问题,在求解过程中引入区域极点约束。比较了鲁棒H∞控制器和不考虑高阶未建模动态的非鲁棒H∞控制器的控制效果,实验结果表明,设计的鲁棒H∞控制器能够有效抑制柔性梁的前三阶模态振动,而且不会发生溢出问题。     

利用偏置磁极周期会切磁铁产生边聚焦场

利用理论分析和数值计算的方法,研究了偏置磁极周期会切磁铁产生的、可用于带状电子束宽边聚焦的边聚焦场。结果表明:增加偏置长度,减小电子束通道宽度,增大磁极轴向长度可以在基本不改变边聚焦场在x方向上分布特性的前提下提高幅值;增大电子束通道的高度,增大磁极厚度均可以减小边聚焦场在x方向上分布曲线的曲率,但同时其幅值也会降低,该降低可利用前述方法予以补偿。在对带状电子束宽边聚焦进行束匹配时,可以先进行曲率匹配,再进行幅值匹配。在进行参数选择时,应合理选择束通道高度和磁极厚度的取值,以避免束通道内的边聚焦场在x方向上的分布出现曲率反向。     

浅析CTS系统在化探中的应用

主要介绍CTS（计算机译谱系统）在化探多元素光谱分析中的应用以及如何建立化探多元素分析方法文件。     

Some remarks on X(6900)

The analysis of the LHCb data on \begin{document}$X(6900)$\end{document} found in the di-\begin{document}$J/\psi$\end{document} system was performed using a momentum-dependent Flatté-like parameterization. The use of the pole counting rule and spectral density function sum rule provides consistent evidence that both confining and molecular states are possible. Alternatively, the nature of \begin{document}$X(6900)$\end{document} cannot be distinguished if only the di-\begin{document}$J/\psi$\end{document} experimental data with current statistics are available. Nevertheless, we found that the lowest state in the di-\begin{document}$J/\psi$\end{document} system likely has the same quantum numbers as \begin{document}$X(6900)$\end{document}, and \begin{document}$X(6900)$\end{document} is probably not interpreted as a \begin{document}$J/\psi-\psi(2S)$\end{document} molecular state.     

Rapid Determination of Phenolic Compounds in Water Samples: Development of a Paper‐based Nanobiosensor Modified with Functionalized Silica Nanoparticles and Potato Tissue

In this study, we present a fast, simple, low‐cost and disposable method for determination of phenolic content in water samples, using a paper based polyphenol oxidase biosensor. The propylamine functionalized silica nanoparticles was dropped onto a paper sheet. After drying at room temperature, the potato tissue extract including polyphenol oxidase was immobilized on the paper via physical and chemical adsorption. The modified paper was placed on the top of the graphite screen printed electrode. To construct of an electrochemical nanobiosensor, the electrochemical behavior of the modified electrode in different steps was investigated by cyclic voltammetry and electrochemical impedance spectroscopy methods. After being optimized the effective parameters, the changes in the biosensor electrochemical response vs. to the different concentrations of the substrate (phenol solution) were monitored by differential pulse voltammetry and amperometry methods. The linear relationships for phenol detection were obtained in the concentration ranges of 0.01–160 μM and 0.1–300 μM with a detection limit of 0.007 μM and 0.042 μM with DPV and amperometry methods, respectively. This method was successfully used in the voltammetric determination of the phenol content in the real samples, like the river water and the wastewater of wood factory.     

A characterization of generalized poles of generalized Nevanlinna functions

Generalized poles of a generalized Nevanlinna function Q ∈ ??_κ (??) are defined in terms of the operator representation of Q . In this paper those generalized poles that are not of positive type and their degrees of non‐positivity are characterized analytically by means of pole cancellation functions. (© 2006 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim)     

Analytical methods to determine cocaine contamination of banknotes from around the world

The presence of cocaine in a significant number of UK pounds (Xxxx), Euros (€) and North American banknotes ($) in general circulation requires appropriate tools to do determinations. This article discusses the-state-of-the-art in the analysis of cocaine on banknotes. We summarize the usual extraction methods of currency samples and compare them, especially with respect to avoiding sample damage. We critically discuss analytical methods, namely gas chromatography (GC) and liquid chromatography (LC), capillary electrophoresis (CE), immunoassay, thermal desorption tandem mass spectrometry (TD-MS²) and ion-mobility spectrometry (IMS). We also review cocaine levels on banknotes around the world and their possible relationship with drug consumption.     

Thermodynamic characteristics of the activity of selected chromatographic sorbents

Summary The possibility of comparing various chromatographic sorbents in respect of their activity is discussed utilizing a simple thermodynamic approach presented earlier.     

An XPS round robin investigation on analysis of wood pulp fibres and filter paper

X-ray photoelectron spectroscopy (XPS) has been applied to pulp and paper research for decades. However, there has been no attempt to standardise or even systematically compare experimental and analysis procedures, even though it is known that fibrous, nature-derived and insulating fibre materials pose remarkable challenges to reliable surface analysis. The experimental problems are mainly linked with neutralisation, energy resolution, contamination and X-ray induced degradation.We have tested applicability, reliability and reproducibility of XPS analysis on real pulp samples with varying lignin and extractives contents in a small round robin investigation. We also tested the instrumental set-ups with an acetone-extracted filter paper, used as a reference sample. The data, collected at four different laboratories with state-of-the-art instruments indicate that reproducible results can be obtained, despite minor differences in experimental and analysis procedures. However, we found that a specified sample handling procedure and limited X-ray exposure are crucial for reproducible, reliable data.Based on the round robin data we recommend dose restricted monochromatic measurements, a cellulosic in situ reference and a consistent sample handling procedure. The data confirms that a paper-based reference material and the correlation of high-resolution C 1s data with O/C atomic ratios can be used in testing instruments and experimental set-ups for pulp and paper materials.