The machining process is primarily used to remove material using cutting tools. Any variation in tool state affects the quality of a finished job and causes disturbances. So, a tool monitoring scheme (TMS) for categorization and supervision of failures has become the utmost priority. To respond, traditional TMS followed by the machine learning (ML) analysis is advocated in this paper. Classification in ML is supervised based learning method wherein the ML algorithm learn from the training data input fed to it and then employ this model to categorize the new datasets for precise prediction of a class and observation. In the current study, investigation on the single point cutting tool is carried out while turning a stainless steel (SS) workpeice on the manual lathe trainer. The vibrations developed during this activity are examined for failure-free and various failure states of a tool. The statistical modeling is then incorporated to trace vital signs from vibration signals. The multiple-binary-rule-based model for categorization is designed using the decision tree. Lastly, various tree-based algorithms are used for the categorization of tool conditions. The Random Forest offered the highest classification accuracy, i.e., 92.6%.
Carotenoids are an essential component of cashew and can be used in pharmaceuticals, cosmetics, natural pigment, food additives, among other applications. The present work focuses on optimizing and comparing conventional and ultrasound-assisted extraction methods. Every optimization step took place with a 1:1 (w:w) mixture of yellow and red cashew apples lyophilized and ground in a cryogenic mill. A Simplex-centroid design was applied for both methods, and the solvents acetone, methanol, ethanol, and petroleum ether were evaluated. After choosing the extractor solvent, a central composite design was applied to optimize the sample mass (59–201 mg) and extraction time (6–34 min). The optimum conditions for the extractor solvent were 38% acetone, 30% ethanol, and 32% petroleum ether for CE and a mixture of 44% acetone and 56% methanol for UAE. The best experimental conditions for UAE were a sonication time of 19 min and a sample mass of 153 mg, while the CE was 23 min and 136 mg. Comparing red and yellow cashews, red cashews showed a higher carotenoid content in both methodologies. The UAE methodology was ca. 21% faster, presented a more straightforward composition of extracting solution, showed an average yield of superior carotenoid content in all samples compared to CE. Therefore, UAE has demonstrated a simple, efficient, fast, low-cost adjustment methodology and a reliable alternative for other applications involving these bioactive compounds in the studied or similar matrix. 相似文献
ABSTRACTIn this paper, lanthanum was used as a chemical modifier for the direct determination of erbium by high-resolution continuum source electrothermal atomic absorption spectrometry. A two-step experimental design was used for optimization, first a full factorial design was conducted for identification of significant factors, and then a central composite design was carried out for final optimization of the significant factors. The optimum parameters were obtained as follows: atomization temperature of 2500°C, pyrolysis temperature of 1600°C, and pyrolysis time of 10?s in the presence of lanthanum as a chemical modifier. Under optimum conditions, the characteristic mass, limit of detection, and limit of quantification were 29?pg, 0.71, and 2.4?µg?L?1, respectively. The precision of the method, estimated as the relative standard deviation for 10 replicate measurements of 50?µg?L?1 of erbium, was 1.8%. The optimized method was applied to determine erbium content in sediments and rock samples. The determined values of erbium in sediment certified reference materials were in satisfactory agreement with the certified values according to the t-test for a 95% confidence level. 相似文献
A numerical/experimental inverse procedure was employed to estimate the temperature-dependent thermal conductivity of a solid body in which 1D heat conduction in a top heated cylindrical sample is assumed. The emphasis is focused on the issue of sensitivity of results to selected assumptions made in inverse calculations. It has been found that the accuracy of heat capacity evaluation brings the largest contribution to final errors (up to 74%). Density accounts for one-fourth to one-third of the total error of determination. The failure to ensure unidirectional heat conduction in a sample during an experiment is important only at elevated temperatures. 相似文献