小型化超导接收前端在雷达中的应用分析

超导接收前端与常规接收前端相比有着极低的噪声系数和极高的频率选择制能力。文中介绍了超导接收前端的技术特点,分析了超导接收前端对于雷达系统性能的提升能力,此外还分析了小型化超导接收前端在雷达领域中应用需要改进的一些问题,并指出了解决这些问题的关键技术。     

冲击压缩下氧化铝陶瓷中破坏阵面的传播

进行了平面冲击波压缩下氧化铝陶瓷中破坏阵面的实验测试和理论探索. 通过氧 化铝陶瓷的平板碰撞实验,借助VISAR测试系统测量了试件自由面的质点速度历程,并对回 收试件进行了电镜扫描观察. 质点自由面速度历程曲线表明,氧化铝陶瓷材料中存在破坏阵 面的传播. 考察了破坏阵面的传播特性,给出了陶瓷材料的动态破坏模型,并对破坏阵面的 传播进行了数值分析.     

Sensitivity comparison of gas chromatography–mass spectrometry with Cold EI and standard EI

Gas chromatography–mass spectrometry (GC–MS) with Cold EI is based on interfacing GC and MS with supersonic molecular beams (SMBs) along with electron ionization of vibrationally cold sample compounds in SMB in a fly-through ion source (hence the name Cold EI). Cold EI improves all the central performance aspects of GC–MS, and in this paper, we focus on its improvement of signal-to-noise ratio (S/N) and limits of detection (LODs). We found that the harder the compound for analysis with standard EI, the greater the Cold EI gain in S/N and LOD. The lower LOD and higher S/N of Cold EI emerge from a few reasons: (a) similar ionization yield as standard EI, (b) enhanced abundance of molecular ions, (c) elimination of vacuum background noise, (d) elimination of ion source-related peak tailing and degradation, (e) ability to lower the elution temperatures via the use of high column flow rates, and (f) greater range of thermally labile and low-volatility compounds that can be analyzed. We demonstrate the superior S/N and lower LOD of Cold EI versus standard EI in a range of compounds, from the simple-to-analyze octafluoronaphthalene all the way to reserpine and an organo-metallic compound that cannot be analyzed by standard EI. These compounds include methyl stearate, cholesterol, n-C₃₂H₆₆, large polycyclic aromatic hydrocarbons, dioctyl phthalates, diundecyl phthalate, pentachlorophenol, benzidine, lambda-cyhalothrin, and methidathion. The significantly lower Cold EI LODs that can be over 1000 times better than in standard EI further result in far superior response linearity and greater measurement dynamic range.