A Wide Band Strong Acoustic Absorption in a Locally Network Anechoic Coating

Composite materials with interpenetrating network structures usually exhibit unexpected merit due to the cooperative interaction. Locally resonant phononic crystals （LRPC） exhibit excellent sound attenuation performance based on a periodical arrangement of sound wave scatters. Inspired by the interpenetrating network structure and the LRPC concept, we develop a locally network anechoic coating （LNAC） that can achieve a wide band of underwater strong acoustic absorption. The experimental results show that the LNAC possesses an excellent underwater acoustic absorbing capacity in a wide frequency range. Moreover, in order to investigate the impact of the interpenetrating network structure, we fabricate a faultage structure sample and the network is disconnected by hard polyurethane （PU）. The experimental comparison between the LNAC and the fanltage structure sample shows that the interpenetrating network structure of the LNAC plays an important role in achieving a wide band strong acoustic absorption.     

Experimental measurement of the nonlinearities of electrodynamic microphones

This paper presents an experimental way of characterizing the nonlinearities of electrodynamic microphones used as acoustical sources. This functioning occurs for reciprocal calibration techniques. For this purpose, its electrical impedance is measured with a Wayne Kerr wedge which has an excellent precision. Moreover, it can be noted that the Thiele and Small model is used to characterize its electrical impedance. Furthermore, an experimental method based on Simplex algorithm allows us to construct polynomial laws which describe the dependence of the Thiele and Small parameters with the input voltage. The nonlinear variations obtained allow us to determine the nonlinear differential equation of the electrodynamic microphone. Then, this equation is solved numerically in order to confirm the accuracy of the polynomial laws obtained by the Simplex algorithm. The distortions are measured with a laser Doppler velocimeter and compared with the ones obtained by the numerical solving of the nonlinear differential equation. The experimental displacement spectrum is consistent with the theoretical one.     

Time-varying non linear modeling of electrodynamic loudspeakers

This paper deals with the time-varying nonlinear analytical modeling of the electrodynamic loudspeaker. We propose a model which takes into account the variations of Small signal parameters. The six Small signal parameters (R_e, L_e, Bl, R_ms, M_ms, C_ms) depend on both time and input current. The electrodynamic loudspeaker is characterized by the electrical impedance which, precisely measured, allows us to construct polynomial functions for each Small signal parameter. By using this analytical model, we propose to compare two identical electrodynamic loudspeakers. One of them is supposed to be run in and the other one is not. The experimental methodology is based on a precise measurement. In all the paper, the time scale is assumed to be much longer than one period of the harmonic excitation.     

Weighted pseudo-almost periodic solutions to a neutral delay integral equation of advanced type

This paper studies suitable sufficient conditions to ensure the existence and uniqueness of weighted pseudo-almost periodic solutions to a neutral delay integral equation of advanced type introduced by T.A. Burton in the literature. The abstract results are then utilized to characterize weighted pseudo-almost periodic solutions to the well-known logistic equation.     

A measurable-group-theoretic solution to von Neumann’s problem

We give a positive answer, in the measurable-group-theory context, to von Neumann’s problem of knowing whether a non-amenable countable discrete group contains a non-cyclic free subgroup. We also get an embedding result of the free-group von Neumann factor into restricted wreath product factors. D. Gaboriau’s research was supported by CNRS. R. Lyons’ research was supported partially by NSF grant DMS-0705518 and Microsoft Research.     

-extension of Lie triple systems

In this paper, we introduce the notion of T^*-extension of a Lie triple system. Then we show that T^*-extension is compatible with nilpotency, solvability, and it preserves in certain sense the decomposition properties. In addition, we investigate the equivalence of T^*-extensions using cohomology. Finally, we show that every finite-dimensional nilpotent metrised Lie triple system over an algebraically closed field is the T^*-extension of an appropriate quotient system.     

Fractional and Hypersingular Operators in Variable Exponent Spaces on Metric Measure Spaces

We prove the continuity of potential type operators and hypersingular operators in variable Lebesgue and Sobolev spaces on a metric measure space (Χ, d, μ). Two variants of such operators are considered, according to the regularity admitted on the measure μ.     

吡咯腙对溶酶体中Hg2+的荧光成像

合成了一种新的吡咯腙探针1,用于Hg^2+的比色和荧光开启检测。探针1对Hg^2+的检测限为45 nmol·L^-1,缔合常数为5.78×10⁸ L·mol^-1。值得注意的是,工作pH范围为4.0~10.0。Job曲线和MS数据证实探针与Hg^2+形成1:1的配合物。通过¹H NMR、时间分辨荧光光谱和密度泛函理论(DFT)计算系统研究了探针与Hg^2+的配位模式。此外,由于吗啉基团的存在,探针可以检测HeLa细胞溶酶体中的Hg^2+。     

固定化新月菱形藻的制备及其对N、P吸收的影响

为优化固定化新月菱形藻(Nitzschia closterium)在污水中去氮、磷的效果, 以褐藻酸钠为固定化载体, 采用单因子试验方法, 研究了不同包埋藻细胞密度(0、0.27×107、0.81×107、1.35×107、1.89×107、2.43×107 cells?mL-1), 不同藻球直径(2.5、3.0、3.5、4.0mm), 3% CaCl2溶液不同加固时间(0、1、2、4、6、8h)、不同藻球用量(0、7.5、15.0、22.5、30.0、37.5g?L-1)和不同加固时间下反复使用次数对氮、磷的去除效果. 结果表明: 包埋藻细胞密度为1.35×107 cells?ml-1时单位藻细胞去除NH4+-N和PO43--P的效果较好. 藻球规格对NH4+-N和PO43--P去除效率的影响不显著(P>0.05). CaCl2加固时间2~8h对藻球中藻细胞生长、NH4+-N和PO43--P去除率没有显著影响(P>0.05), 但均显著高于加固1h, 未经加固的藻球极易破损. 藻球投放质量越大, NH4+-N和PO43--P的去除速度越快, 投放量为30g?L-1, 培养9d后, NH4+-N和PO43--P去除率可达80%以上. 固定化藻球反复使用3次以上, 其NH4+-N和PO43--P的去除效率下降. 由此得出: 固定化新月菱形藻球包埋藻细胞密度以1.35×107 cells?mL-1, 藻球直径3.5mm为佳; 藻球制作时在3% CaCl2溶液中加固最佳时间为2h; 藻球用量为30g?L-1; 对藻球定期(9d)进行加固, 有利于增加藻球使用寿命, 并保持其较好的氮、磷去除率.     

2,5-噻吩二甲酸与菲咯啉构筑的稀土配合物:晶体结构,荧光性质和对Cu2+离子的荧光传感

稀土硝酸盐和2,5-噻吩二甲酸与菲咯啉在水热反应条件下合成了3个新的配合物,[Ln(2,5-tdc)1.5(phen)(H2O)]n(Ln=Gd(1),Tb(2),Dy(3);2,5-tdc=2,5-噻吩二甲酸根,phen=菲咯啉)。通过X射线单晶衍射确定了它们的晶体结构。配合物1~3为同构的2D网络结构。配合物1在340 nm激发下出现最大发射中心位于366和387 nm的宽峰,可归属于配体的π*-π跃迁发射。配合物2在365 nm紫外灯照射下发绿光,其荧光发射光谱中出现了4个尖峰,位于491、545、588和620 nm处,对应于Tb3+的5D4→7FJ(J=6~3)跃迁。配合物2的荧光寿命显示为单指数衰减,其值为(0.123±0.005)ms。配合物3的发射光谱中出现了2个尖峰,位于482和575 nm处,分别对应于Dy3+的4F5/2→6H15/2和4F5/2→6H13/2跃迁。另外,研究了配合物2的荧光传感能力,该配合物可作为荧光探针检测水溶液中的Cu2+离子。