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41.
Florence Burdin Pascal Guiraud Anne‐Marie Wilhelm Henri Delmas 《Particle & Particle Systems Characterization》2002,19(2):73-83
Knowledge of the acoustic cavitation cloud would be useful for improving ultrasound reactor design. Among the characterisation techniques, few are adapted to bubble investigations in an intense ultrasound field. Some problems raised by these measurements result from interactions between the acoustic pressure wave and the measuring light wave. This paper reports the implementation of the laser diffraction technique to determine the size and volume concentration of bubbles generated by a dipping horn operating at 20 kHz. Measurements were performed with a Malvern 2600 instrument. The size distribution, deduced from the diffraction pattern scattered by the bubble cloud crossed by a laser beam, is disturbed by the acoustic pressure wave involving deviation of a light beam at low diffusion angles (acousto‐optic effect). A bubble size correction procedure based on the subtraction of the light energy due to the ultrasound wave is described. The size measurements, and thus the correction procedure, were validated by a second laser technique based on a different measuring principle: phase Doppler interferometry. The measurement reliability was further confirmed by an original application of laser diffraction based on measurements performed just after sonication. These three methods lead to a mean bubble size (Sauter mean diameter) of about 10 μm at a high ultrasound power input. Concerning the void fraction, only measurements achieved after sonication and by laser diffraction predict a correct estimation of this parameter. 相似文献
42.
43.
W. Kockelmann M. Hofmann O. Moze S.J. Kennedy K.H.J. Buschow 《The European Physical Journal B - Condensed Matter and Complex Systems》2002,30(1):25-32
The element distributions and the magnetic ordering behaviour of compounds RNi10Si2 (R
=
Tb, Dy, Ho, Er, Tm) have been studied by neutron powder diffraction down to temperatures of 1.6 K. The compounds crystallize
in an ordered variant of the ThMn12 structure type in the tetragonal space group P4/nmm. An ordered 1:1 distribution of Ni and Si on sites 4d and 4e, respectively,
corresponds to a modulation vector [0, 0, 1] with respect to the space group I4/mmm of the ThMn12 structure. TbNi10Si2 orders antiferromagnetically below T
N
= 4.5 K with a magnetic propagation vector of [0, 0, 1/2]. The magnetic Tb moments, 8.97(2) /Tb atom at 1.6 K, are aligned along the c-axis. The Ni sites in TbNi10Si2 do not carry any ordered magnetic moments. The compounds with R
=
Dy, Ho, Er, and Tm are paramagnetic down to 1.6 K and 3.0 K, respectively.
Received 10 July 2002 / Received in final form 12 September 2002 Published online 29 October 2002 相似文献
44.
Richard P. Fischer Arne W. Fliflet 《International Journal of Infrared and Millimeter Waves》2002,23(9):1297-1313
This paper presents the design and test of asymmetric quasioptical resonators for gyrotron applications, where most of the diffraction output coupling comes from the smaller of two mirrors. A computer code based on scalar diffraction theory is used to calculate the resonator losses and the electric field near the mirrors. Resonators with mirror separations approaching confocal have reduced side lobes in the diffraction patterns, which should allow for better power transmission and focusing. Cold tests have been performed at 94 and 141 GHz to measure the quality factor of the asymmetric resonators as a function of mirror separation and mirror misalignment. Typical resonator parameters include 65 cm mirror separation, 1-3% output coupling and 85% of the losses from the small mirror. A half-symmetric resonator with one flat and one curved mirror has also been investigated. The calculated values of Q are in reasonably good agreement with the cold test measurements. 相似文献
45.
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49.
用X射线衍射(XRD)技术和显微Raman散射方法对金属有机化学气相沉积(MOCVD)法生长的六方相InxGa1-xN薄膜样品进行了研究,观察到了相分离现象和LO声子-等离子耦合模(LPP+),讨论了InxGa1-xN的A1(LO)模被屏蔽的主要物理机制.同时,对Raman谱中E2和A1(TO)声子模进行了分析和讨论.在InxGa1-xN样品的低温Raman谱中还观察到单电子跃迁产生的Raman散射信号.
关键词:
Raman散射
X射线衍射
相分离
应力
LO声子-等离子耦合 相似文献
50.
A.R. Phani M. PassacantandoS. Santucci 《Journal of Physics and Chemistry of Solids》2002,63(3):383-392
Crack free, dense and transparent CdTiO3 thin films have been prepared by sol-gel technique using titanium butoxide and cadmium acetate. The formation of the CdTiO3 phase started from 500°C annealing temperature onwards. The complete orthorhombic structure of CdTiO3 was formed on Silicon (100) substrate at an annealing temperature of 600°C for 5 h. As the annealing temperature increased from 600 to 700°C, we have observed the cadmium silicate phase at the interface of Si and CdTiO3 phase. Structural, morphological and elemental evolution of these CdTiO3 thin films produced by sol-gel synthesis were characterised by grazing incidence X-ray diffraction (GIXRD), tapping mode atomic force microscopy (TMAFM), scanning electron microscopy (SEM) and X-ray photoelectron spectroscopy (XPS) respectively. 相似文献