多波长线性回归法测定脑宁片的含量

本文采用多波长线性回归法测定脑宁片的含量。计算程序采用BASIC语言编制。氨基比林和咖啡因的回收率和相对标准偏差分别为98.03%-100.9%,1.0%-和97.77%-99.39%,0.61%。本法不经分离直接测定脑宁片中二组分的含量,方法简便、快速、结果满意。     

长周期光纤光栅:原理、制备与应用

较全面介绍了长周期光纤光栅。对比Bragg光纤光栅说明了长周期光纤光栅的特点。对其耦合机理进行了分析 ,阐明了波长选择损耗特性。介绍了长周期光纤光栅的制备方法 ,大致分之为基于非形变的制备方法和基于形变的制备方法。详细阐述其在通信、传感领域的应用 ,尤其是新型应用 :带通滤波、光上下路复用、光纤光源、偏振器件、新型传感等。并针对长周期光纤光栅对温度、应力、外部折射率敏感的特性 ,探讨了调谐性以及温度稳定性的方案     

Breakdown Pattern of Hydrocarbons by Laser Breakdown Time-of-flight Mass Spectrometry

The laser breakdown time-of-flight mass spectrometry was developed and applied to detect the breakdown patterns of hydrocarbons that are significant to improve the detectability of heavy metals compounded in various mixtures such as particles and hydrocarbons. The laser wavelength dependence of this method was evaluated using 1064, 532, and 266 nm laser outputs. Breakdown processes using 1064 and 532 nm outputs showed less interference of fragmentation for the detection of various heavy metals. The method was applied to various hydrocarbons and it showed the possibility of categorization of hydrocarbon groups using the pattern of breakdown products.     

Dual Wavelength Spectrophotometry. Determination of 1,2,4-Benzenetricarboxylic Acid and Benzenepentacarboxylic Acid

Dual wavelength ultraviolet spectrophotometry was utilized for the determination of 1,2,4-benzenetricarboxylic and benzenepentacarboxylic acids in their simultaneous solution.     

用于全光波长转换的外腔半导体激光器的注入电流选择

实验研究了注入光对光纤光栅外腔半导体激光器阈值电流的影响,给出了可同时获得高消光比和高转换速率的注入电流范围。采用载流子消耗机抽对实验结果进行了实性分析。     

用统一耦合模理论分析含布拉格光栅的对称光纤耦合器的传输特性

利用由麦克斯韦方程组直接导出的统一耦合模理论分析各类型的含布拉格光栅的对称光纤耦合器的传输特性。与以前发表的分析方法不同,对于含布拉格光栅的耦合区域,统一耦合模型理论同时考虑了布拉格光栅和耦合的耦合作用。模拟结果证明它能精确地模拟和解释各种类型的含布拉格光栅的对称光纤耦合器的有关实验现象。     

宽带消波长依存波导耦合器的统计优化设计

提出了一种适合于宽带消波长依存波导耦合器的统计优化设计方法。使用该方法 ,在 12 80nm～ 165 0nm带域内 ,对Si基SiO2 光波导作了包括偏振变动优化在内的 5 0 %和 2 0 %功率耦合比的消波长依存波导耦合器的设计。两个器件经三维波束传播法 (BPM)模拟运行验证 ,结果表明 ,在 370nm宽带内 ,两个直交偏振态均实现了功率耦合比为 (5 0± 2 .1) %和 (2 0± 1.4) %、偏振变动量分别小于 0 .65 %和 0 .2 0 %的良好特性     

Details of Structure Formation During the Induction Period of Spinodal-Type Polymer Crystallization

An unexpected type of primary crystal nucleation is described, involving spinodal decomposition (SD) type microphase separation due to the orientation fluctuations of rigid segments prior to crystal nucleation. This type of mechanism was found by the present authors about 10 years ago, and recently, it was theoretically revealed by Olmsted et al. to be one of three types of primary crystal nucleation: the well-known homogeneous crystal nucleation directly from the liquid–crystal coexistence domain, which occurs at higher temperatures above the binodal temperature T _b , crystal nucleation after binodal microphase separation between T _b and spinodal temperature T _s , and that after SD below T _s . The detailed experimental results for the spinodal-type crystal nucleation, especially the temperature dependence of characteristic wavelength in SD, are explained as well.     

相关分析与谱分析在表面形貌研究中的应用

本文通过对表面形貌进行相关分析与谱分析,提出了相对波度和有效波度、相对波长和有效波长的概念,并且指出相关分析与谱分析是研究表面形貌润滑效应的有力工具。作者认为,当相对波度为有效波度时,应当同时考虑波长和幅值的摩擦学效应;当相对波度为高频的粗糙度时,只需考虑表面形貌的幅值效应。     

Electric field‐induced birefringence,optical rotatory power and conoscopic measurements of a chiral antiferroelectric smectic liquid crystal

Using a photoelastic modulator‐based novel set‐up, the electric field‐induced in‐plane birefringence and the optical rotatory power (ORP) were measured of an antiferroelectric liquid crystalline compound (12OF1M7) in its various phases using 30 µm homeotropic cells. Some specific signatures of the in‐plane birefringence and of the ORP for the various phases are being established. A relatively small threshold field is needed for the unwinding process of the antiferroelectric phase with a unit cell of four layers [SmC_A*(1/2)] compared with that for two layers [SmC_A*(0)]. On application of the electric field on the high temperature side of the SmC_A*(1/2) phase (80.1–81.5°C), a field‐induced phase transition is shown to occur directly to the SmC* phase, whereas on the lower temperature side (79.4–80.1°C) the transition takes place to SmC* via the SmC_A*(1/3) phase. The in‐plane birefringence exhibits a critical power law dependence for the SmC*–SmA transition. The ORP changes sign within the temperature range of the phase with a unit cell of three layers, reflecting a change in the handedness during this phase. Using tilted conoscopy, the results for the biaxiality and the apparent tilt angle for a smectic liquid crystal with a tilt angle greater than 18° in the ferroelectric phase are reported. The biaxiality implies the difference in the refractive indices between the two minor axes of the refractive index ellipsoid. The optical transmittance at visible and IR wavelengths for free‐standing films reveal characteristic reflection bands for these phases. The modulated structures of the reflected bands appear just above the SmC_A* phase and below SmC_A*(1/3); these are possibly due to an easy deformation of the phase by the surfaces.