一种适于自适应光学的旋转软刀口波面传感器的研究

利用傅里叶光学理论,证明了一种新型波面传感器——旋转软刀口波面传感器的概念.在经典刀口法的刀口区,以渐变透过率代替突变透过率函数,在光瞳象面上可获得反映光瞳面位置待测波面位相梯度及位相梯度方向的调制信号.文中给出了实验结果和讨论.     

Study on thermal decomposition of polymers by evolved gas analysis using photoionization mass spectrometry (EGA-PIMS)

Photoionization mass spectrometry (PIMS) with vacuum ultraviolet (VUV) light source provides an efficient and fragmentation-free method for the soft ionization of gaseous compounds, in order to facilitate an understanding of thermal decomposition behavior and chemical composition of polymeric materials. The PIMS was applied to the evolved gas analysis (EGA) system equipped with a skimmer interface which is constituted based upon a jet separator principle between a vacuum MS chamber and an atmospheric sample chamber in a furnace. A photoionization source with a deuterium (D₂) lamp was closely installed to the vacuum ionization chamber of a mass spectrometer to improve the ionization efficiency. The thermal decomposition of typical polymers in inert gas atmosphere was investigated by the EGA-PIMS and the resulting PI mass spectrum was characterized satisfactorily by only the parent ions with no contribution as a result of fragmentation during the ionization. The results suggested that the EGA-PIMS was an especially powerful and desirable in situ thermal analysis method for polymeric materials which evolve organic gases simultaneously and concurrently. The combination of EGA equipped with skimmer interface with no change of evolved gaseous species and PIMS with fragmentation-free during the ionization is described briefly, and the effective results are presented by comparing with EGA using conventional electron impact ionization mass spectrometry.     

合肥同步辐射软X射线显微术研究

合肥国家同步辐射实验室首期建设的光束线之一用于软Ｘ射线显微成像研究。实验站现已装置初型的扫描透射Ｘ射线显微镜，并正在进行亲一代的扫描显微建设，同时还使同步辐射光进行接触软Ｘ射线呈微成像研究，并对选取的一些生物样品进行了成像试验。本文介绍了合肥同步辐射光源上软Ｘ射线显微术实验线站的建设及完成的一些实验结果。     

软体连续机械臂动力学建模与仿真

由于软体机械臂的质量是沿臂的长度连续分布,因此采用拉格朗日方法建立软体机械臂的动力学模型时,涉及计算复杂的积分运算,采用离散化的集中质量模型降低了计算的复杂性,但准确性不足.为了提高软体机械臂动力学建模与仿真的准确度和计算效率,本文采用模态方法对软体机械臂进行运动学描述,并从能量的角度分析软体机械臂动力学特性,研究发现...     

Stimuli‐Responsive Theragrippers for Chemomechanical Controlled Release

We report on a therapeutic approach using thermo‐responsive multi‐fingered drug eluting devices. These therapeutic grippers referred to as theragrippers are shaped using photolithographic patterning and are composed of rigid poly(propylene fumarate) segments and stimuli‐responsive poly(N‐isopropylacrylamide‐co‐acrylic acid) hinges. They close above 32 °C allowing them to spontaneously grip onto tissue when introduced from a cold state into the body. Due to porosity in the grippers, theragrippers could also be loaded with fluorescent dyes and commercial drugs such as mesalamine and doxorubicin, which eluted from the grippers for up to seven days with first order release kinetics. In an in vitro model, theragrippers enhanced delivery of doxorubicin as compared to a control patch. We also released theragrippers into a live pig and visualized release of dye in the stomach. The design of such tissue gripping drug delivery devices offers an effective strategy for sustained release of drugs with immediate applicability in the gastrointestinal tract.     

Imaging Magnetic Domain Structures with Soft X-Ray Microscopy

The current achievements in magnetic transmission soft X-ray microscopy will be reviewed. The magnetic contrast is given by X-ray magnetic circular dichroism (X-MCD), i.e., the dependence of the absorption coefficient of circularly polarized X rays on the projection of the magnetization in a ferromagnetic system onto the photon propagation direction. X-MCD contrast can reach, e.g., at L_2,3 edges in transition metals, large values up to 50%. Combined with a soft X-ray microscope where Fresnel zone plates acting as optical elements provide a lateral resolution down at 25 nm, it allows for imaging magnetic microstructures. Specific features of this photon-based technique are the recording of images in varying external magnetic fields, an inherent chemical specificity, a high sensitivity to thin magnetic layers, due to the large contrast, and the possibility to distinguish between in-plane and out-of plane contributions. In this report, recent results obtained with the XM-1 microscope at the ALS (Berkeley/CA) demonstrate the broad applicability of this novel experimental technique to both fundamental and technological relevant issues in nanomagnetism. The future potential will be briefly outlined.     

激光等离子体脉冲软X光标定源

利用神光Ⅱ上激光与等离子体相互作用得到的软X光,建立了基于多层镜的四通道软X光单色器系统。研究了光源的性能,测量了光源强度、单色器系统稳定性、相应通道的一致性。研究表明,采用多层镜作为脉冲光源的分光元件,可以得到具有较好单色性的强脉冲软X 光标定源。光源的光子能量为253 eV和820 eV,两能道的光源强度分别为1.8×1019 photon/(s·cm2)和3.2×1019 photon/(s·cm2)。在该标定源上可以实现XRD、平面镜、多层镜、透射光栅和滤片的标定。     

泡沫流体的剪应力与法向应力差

本文在同时考虑表面张力与粘性力的情况下,以三维模型—长菱形十二面体及泡沫的应力张量表达式为基础,得出了泡沫的剪应力及法向应力差表达式,并通过计算机进行了求解,讨论了泡沫粘度、泡沫大小等因素对剪应力及法向应力差的影响。 实验使用了 RMS-605 大型流交仪、RV-2 流变仪及毛细管流变仪测定泡沫流变特性。消除了表面滑移影响后得到的剪应力与法向应力表数据与理论结果较接近,说明理论模型具有一定的实用价值。     

高温下轻质泡沫铝动态力学性能实验

对传统的分离式Hopkinson压杆装置加以改进,设计了一种长杆直接撞击Hopkinson杆的实验方案,检测出低波阻抗材料在高温动态加载下的应力均匀性。对轻质泡沫铝材料的实验表明,在同一撞击速度下,温度越高,试件两端的应力均匀性越差,增加温度与提高撞击速度均会导致泡沫铝材料冲击端与支撑端的应力不均匀性。根据高温下应力均匀性的实验结果,确定高温下试件均匀变形对应的冲击速度,再通过传统的分离式Hopkinson压杆实验得出泡沫铝在高温动态下的力学性能。