平台石墨炉原子吸收测磷的方法研究

研究了平台石墨炉原子吸收测定磷的方法,表明以氯化钯和硝酸钙的混合液作为基体改进剂测定生物样品中的磷效果最好,方法特征量为8×10~(-9)g,工作曲线线性范围为0～0.400吸光度,精密度好,抗干扰能力强,方法简单,利用标准曲线即可测定生物样品中磷。     

具有非局部边界条件的奇摄动反应扩散问题

本文研究了一类具有非局部边界条件的奇摄动反应扩散初始边值问题．在适当的条件下，利用比较定理讨论了问题解的渐近性态．     

Regularization of singular systems of linear algebraic equations by shifts

Regularization of singular systems of linear algebraic equations by shifts is examined. New equivalent conditions for the shift regularizability of such systems are derived.     

On parametric instability of viscous two-layer fluid in a vessel with a permeable bottom

A linear problem of parametric oscillations of a low-viscous two-layer fluid in a closed vessel partially filled with a porous medium is studied. An asymptotic solution is constructed on the basis of combined application of boundary functions and averaging methods. Approximate formulas for boundaries of instability domains in the case of subharmonic and harmonic resonances are derived.     

Fixed-sign solutions for a system of singular focal boundary value problems

We consider a system of focal boundary value problems where the nonlinearities may be singular in the independent variable and may also be singular in the dependent arguments. Using Schauder fixed point theorem, we establish criteria such that the system of boundary value problems has at least one fixed-sign solution.     

The construction of infinite families of any k-tight optimal and singular k-tight optimal directed double loop networks

The double loop network(DLN)is a circulant digraph with n nodes and outdegree 2.It is an important topological structure of computer interconnection networks and has been widely used in the designing of local area networks and distributed systems.Given the number n of nodes,how to construct a DLN which has minimum diameter?This problem has attracted great attention.A related and longtime unsolved problem is:for any given non-negative integer k,is there an infinite family of k-tight optimal DLN?In this paper,two main results are obtained:(1)for any k≥0,the infinite families of k-tight optimal DLN can be constructed,where the number n(k,e,c)of their nodes is a polynomial of degree 2 in e with integral coefficients containing a parameter c.(2)for any k≥0, an infinite family of singular k-tight optimal DLN can be constructed.     

L~p Estimates for Hyperbolic Singular Integral Operators

In this paper, we prove Lp-boundedness of hyperbolic singular integral operators for kernels satisfying weakened regularity conditions, where 1相似文献   

类奇异积分和交换子在广义Morrey空间上的有界性

The generalized Morrey spaces are introduced under the hypothesis that Rn is endowed with the general parabolic metric , and the boundedness properties are established in generalized Morrey spaces for a class of singular integral operators, which include Calderon-Zygmund singular integrals and their commutators with BMO.     

四阶微分方程奇异边值问题的正解

本文利用锥上的不动点指数理论,在更一般的边界条件下讨论了一类四阶奇异边值问题正解的存在性并给出了应用．     

New methodologies in trace analysis of volatile organic compounds

Two methods for sampling and concentration of volatile organic compounds are reported. In the first method, traps coated with a very thick film (ca. 100 μm) of cross-linked silicone stationary phase are employed. Such thick films can be prepared with a modified dynamic coating procedure, which is briefly described. The low phase ratio traps can be utilized for enrichment of volatiles from gaseous as well as aqueous matrices. The second technique is based on chromatographic evaporation of a solvent in a capillary tube, where the process is sustained by a repeated sample injection and a cyclic flow reversal. In this way, large solvent volumes can be handled by a small volume system. Under optimal conditions, when using a solvent barrier, quantitative recovery is possible even for compounds of comparatively high volatility. Another important application of the technique is extraction of trace components from gases such as headspace samples, polluted air, etc.