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101.
D. N. Olennikov L. M. Tankhaeva G. G. Nikolaeva A. V. Tsyrenzhapov S. M. Nikolaev G. V. Chekhirova 《Chemistry of Natural Compounds》2004,40(1):1-5
Leaves of Cacalia hastate L. (Asteraceae) were composed of free sugars, water-soluble polysaccharides (arabinogalactan type), pectinic substances, hemicelluloses, and cellulose. The hypoglycemic activity was determined for the water-soluble polysaccharides and pectinic substances. 相似文献
102.
As a potential anticarcinogenic agent, polysaccharides from Cordyceps sinensis have been demonstrated to possess strong antioxidation activity. The aim of the present research was to study the optimal
medium to produce polysaccharides of C. sinensis by using response surface methodology (RSM). The composition of optimized medium for polysaccharide production calculated
from the regression model of RSM was 6.17% sucrose, 0.53% corn steep powder, 0.5% (NH4)2HPO4, and 0.15% KH2PO4 at pH 4.44, with a predicted maximum polysaccharide production of 3.17 g/L. When applying this optimal medium, the maximum
polysaccharide production was 3.05 and 3.21 g/L in a shake flask and a 5-L jar fermentor, respectively. When the pH was controlled
at a higher level such as pH 5.0, both cell growth and polysaccharide production were inhibited. A low pH of 2.85 was required
for maximum production of polysaccharides. 相似文献
103.
海水小球藻中多糖的提取及其单糖组成的气相色谱-质谱分析 总被引:6,自引:0,他引:6
在温度为70℃、功率为600 W、提取时间为30 m in的条件下,海水小球藻中的多糖可以得到较好的提取。经过优化,当超声波作用时间为90 m in、超声波功率为300 W、水解液为1 mol/L乙酸时,小球藻多糖的超声水解效果最好。碱提、水提、酸提海水小球藻多糖中的单糖组成,经过GC-MS分析,它们的单糖组成各不相同。碱提粗多糖中所含单糖为鼠李糖、L-岩藻糖、D-阿拉伯糖、D( )-木糖、D-甘露糖、D-葡萄糖、D-半乳糖,各单糖百分含量分别为20.68%、0.32%、1.0%、2.20%、4.58%、50.28%、20.91%(W/W);水提海水小球藻粗多糖中含鼠李糖、核糖、岩藻糖、阿拉伯糖、木糖、甘露糖、葡萄糖、半乳糖8种单糖,它们百分比分别为2.32、2.36、0.24、0.89、0.56、3.44、78.21、11.99%(W/W);酸提粗多糖中所含单糖为鼠李糖、核糖、岩藻糖、阿拉伯糖、木糖、甘露糖、葡萄糖、半乳糖,各单糖百分含量分别为2.75、1.75、0.23、1.04、0.61、5.99、74.33、13.30%(W/W)。本实验所建立的微波辅助提取、超声水解多糖、GC-MS分析多糖中的单糖组成等方法,具有简便、快速、准确的特点。可用于海藻和其它植物中的多糖研究。 相似文献
104.
105.
Various natural and modified polysaccharides (i.e. arabic gum, tragacanth gum, xanthan gum, sodium alginate, chitosan, sodium carboxymethyl cellulose, hydroxyethyl cellulose, methyl cellulose) were modified using ceric-initiated graft polymerization of acrylonitrile under inert atmosphere. Grafting was confirmed using spectral (FT-IR) proofs. The grafting parameters were determined by conventional methods. Thermal characteristics of the homopolymer-free copolymers were studied using differential scanning calorimetry (DSC) and thermogravimetric analysis (TGA) under nitrogen atmosphere. The major thermal transitions as well as the activation energy of the major decomposition stages were investigated. The polyacrylonitrile (PAN)-grafted polysaccharides were recognized to be thermally stable more than the corresponding non-grafted substrates, although they begin to decompose at relatively lower temperatures than the non-grafted counterparts. Copyright © 2003 John Wiley & Sons, Ltd. 相似文献
106.
K. Turdumambetov Z. Bekmuratov D. A. Rakhimov M. Kh. Malikova 《Chemistry of Natural Compounds》2007,43(1):1-4
Structures of glucofructans isolated from Cousinii radians roots were studied by methylation, periodate oxidation, and IR and 13C NMR spectroscopies. It was found that fructofuranose units were bonded to each other by inulin-type β-(2→1)-gylcoside bonds.
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Translated from Khimiya Prirodnykh Soedinenii, No. 1, pp. 3–5, January–February, 2007. 相似文献
107.
Studies on the Peptides and Polysaccharides in Pollen 总被引:1,自引:0,他引:1
The peptides RP3I and PSPP1-4 were purified from the rape and the Papaver Somniferunpollens, respectively. Their sequences and physiological activities were determined and synthesized ex-cept PSPP1. The polysaccharides TAA-C and CPA-E were obtained from Typha Angustifilia andCodonopsis Pilosula pollens, respectively. Their partial characterization and structures were studied. 相似文献
108.
A. Alcantara A. Ballesteros J. V. Sinisterra 《Applied biochemistry and biotechnology》1990,26(3):297-310
Improvement have been made in a simplified procedure we previously reported (J.Mol.Catal. (1986),38,227 for the activation
of tosyl chloride of supports possessing primary hydroxyl groups. The method is simple, can be completed in less than 90 min,
yields a broad range of activation degrees, and, since it involves no toxic reagents, may be used for preparing immobilized
enzymes to be utilized in food manufacturing and processing. The immobilization ofStophylococcal Nuclease has been carried out by this method. The insolubilized derivatives are more active than the native enzyme in the hydrolysis
of DNA. The thermal stability of nuclease derivatives is greater than that of the native enzyme. These derivatives remain
active at 50°C, and the native enzyme, 39°C. The insolubilized nuclease is more stable against organic solvents such as, dimethylsulfoxide
(DMSO) or tetrahydroduran (THF) than the native enzyme. 相似文献
109.
110.
D. A. Rakhimov T. N. Kholmuradova R. Sh. Shoyakubov 《Chemistry of Natural Compounds》2006,42(3):259-261
It was established by studying carbohydrates of Iris pseudacorus during vegetative periods that the content of water-soluble polysaccharides in the rhizomes and roots is greatest during
seed ripening; of pectinic substances, during budding. Glycomannan was isolated from seeds.
__________
Translated from Khimiya Prirodnykh Soedinenii, No. 3, pp. 216–217, May–June, 2006. 相似文献