A New Pathway to Synthesize Cyclomercurated Ferrocenylimines Containing Heterocyclic Ring

The cyclomercurated ferrocenylimines containing heterocyclic ring were prepared by the condensation of cyclomercuration of acylferrocene with the appropriate heterocyclic amine.This procedure provides an efficient method for the synthesis of cyclomerucurated ferrocenylimines containing heterocyclic ring which are difficultly synthesized by the conventional method.The reaction mechanism is proposed.     

应用参数假设检验分析特异功能是否存在

本文应用参数假设检验知识分析“特异功能”者是否有特异功能。     

迈克耳逊干涉仪的彩色光环的调节与拍摄

本文介绍了迈克耳逊干涉仪的彩色光环的产生机理、快速调节与拍摄方法。     

SXDG-1型汽车前照灯全自动检测仪的微机控制

SXDG—1型汽车前照灯全自动检测仪是用于检测汽车前照大灯光轴的偏斜情况及发光强度并进行定量检验的专用设备。它可以自动测出有关参数,并予以数字显示和打印输出。本文介绍了该仪器的主要性能、工作原理及微机控制系统(包括硬件结构和软件设计思想等)。     

关于NF-环的构造

研究了无限的ＮＦ－环及有限的ＮＦ－环，并且给出了有限ＮＦ－环的构造．     

Factorisation in the ring of exponential polynomials

We study factorisation in the ring of exponential polynomials and provide a proof of Ritt's factorisation theorem in modern notation and so generalised as to deal with polynomial coefficients as well as with several variables. We do this in the more general context of a group ring of a divisible torsion-free ordered abelian group over a unique factorisation domain.

     

Supersemiprime Rings and Supersemiprime Radical

§1.　IntroductionInthisrecentyears,theprimeringswithspecialpropertieshavebeenstudiedsomeau-thors,forexample,N.T.Groenewaldintroducedthecompletelyprimeringsandthecompletelyrimeradicalin[1].D.HandelmanandJ.Lawrencediscussedthestronglyprimeringsandthestronglyprimeradicalin[2].S.Veldsmanstudiedthesuperprimeringsandthesuperprimeradicalin[3].ZhangXianjunintroducedtheAbsolutelysemiprimeringsandtheabsolutelysemiprimeradicalandsoon.Theaimofthispaperistostudythesemiprimeringswithspecialpropertiesan…     

用频域法实现圆环形目标物的计数

研究了用频域法实现圆环形目标物计数的方法。对空域中含有圆环形目标物的二值图像，经傅里叶变换后在频域内进行滤波，再经傅里叶反变换后取一阈值进行处理，则对应于圆环形目标物即变为一个实心体，然后对实心体进行计数即可实现对圆环形目标物的计数。对该方法进行了数学描述，并分别用模拟图像和实际图像进行了实验。结果表明，该方法消除噪声的效果好，对部分封闭圆的检测同样有效，且可用于目标物有粘连的情况。该方法对圆环形目标物的尺寸相差不大的情况更为有效。     

Exchange环的K0群的正向凸子群格

本文证明了：(1)Exchange环R的K0群的正向凸子群格同构于R的稳定余有限半本原理想格；(2)稳定有限、半本原的exchange环R是单的当且仅当它是K0-单的并且满足逼近弱s^*—可比性，推广了Goodearl，Ara等人的结果。     

Synthesis,characterization, and micellization of an epoxy‐based amphiphilic diblock copolymer of ϵ‐caprolactone and glycidyl methacrylate by enzymatic ring‐opening polymerization and atom transfer radical polymerization

Amphiphilic diblock copolymer polycaprolactone‐block‐poly(glycidyl methacrylate) (PCL‐b‐PGMA) was synthesized via enzymatic ring‐opening polymerization (eROP) and atom transfer radical polymerization (ATRP). Methanol first initiated eROP of ?‐caprolactone (?‐CL) in the presence of biocatalyst Novozyme‐435 under anhydrous conditions. The resulting monohydroxyl‐terminated polycaprolactone (PCL–OH) was subsequently converted to a bromine‐ended macroinitiator (PCL–Br) for ATRP by esterification with α‐bromopropionyl bromide. PCL‐b‐PGMA diblock copolymers were synthesized in a subsequent ATRP of glycidyl methacrylate (GMA). A kinetic analysis of ATRP indicated a living/controlled radical process. The macromolecular structures were characterized for PCL–OH, PCL–Br, and the block copolymers by means of nuclear magnetic resonance, gel permeation chromatography, and infrared spectroscopy. Differential scanning calorimetry and wide‐angle X‐ray diffraction analyses indicated that the copolymer composition (?‐CL/GMA) had a great influence on the thermal properties. The well‐defined, amphiphilic diblock copolymer PCL‐b‐PGMA self‐assembled into nanoscale micelles in aqueous solutions, as investigated by dynamic light scattering and transmission electron microscopy. © 2007 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 45: 5037–5049, 2007